CH439759A - Verfahren zur Herstellung von pulver- oder perlförmigen Kondensationsprodukten aus 2-wertigen phenolischen Verbindungen und Epihalogenhydrinen - Google Patents

Verfahren zur Herstellung von pulver- oder perlförmigen Kondensationsprodukten aus 2-wertigen phenolischen Verbindungen und Epihalogenhydrinen

Info

Publication number: CH439759A
Authority: CH; Switzerland
Prior art keywords: sep; condensation products; epihalohydrins; reaction; production
Prior art date: 1964-01-28

Application number

CH103265A

Other languages

German (de)

English (en)

Inventor

Paul Dr Janssen

Hermann Dr Richtzenhain

Wilhelm Dr Vogt

Original Assignee

Dynamit Nobel Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1964-01-28

Filing date

1965-01-25

Publication date

1967-07-15

1965-01-25 Application filed by Dynamit Nobel Ag filed Critical Dynamit Nobel Ag

1967-07-15 Publication of CH439759A publication Critical patent/CH439759A/de

Links

239000007859 condensation product Substances 0.000 title claims description 35
238000000034 method Methods 0.000 title claims description 22
150000002989 phenols Chemical class 0.000 title claims description 20
238000004519 manufacturing process Methods 0.000 title claims description 11
239000000843 powder Substances 0.000 title claims description 6
238000006243 chemical reaction Methods 0.000 claims description 21
239000003995 emulsifying agent Substances 0.000 claims description 14
125000003700 epoxy group Chemical group 0.000 claims description 14
238000009833 condensation Methods 0.000 claims description 12
230000005494 condensation Effects 0.000 claims description 12
150000001875 compounds Chemical class 0.000 claims description 9
239000000084 colloidal system Substances 0.000 claims description 7
230000001681 protective effect Effects 0.000 claims description 7
239000003513 alkali Substances 0.000 claims description 6
239000003795 chemical substances by application Substances 0.000 claims description 5
125000003118 aryl group Chemical group 0.000 claims description 3
239000001257 hydrogen Substances 0.000 claims description 3
229910052739 hydrogen Inorganic materials 0.000 claims description 3
125000000217 alkyl group Chemical group 0.000 claims description 2
125000000753 cycloalkyl group Chemical group 0.000 claims description 2
125000004435 hydrogen atom Chemical class [H]* 0.000 claims description 2
125000005429 oxyalkyl group Chemical group 0.000 claims description 2
239000000725 suspension Substances 0.000 claims description 2
125000004001 thioalkyl group Chemical group 0.000 claims description 2
125000004103 aminoalkyl group Chemical group 0.000 claims 1
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 21
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 17
239000000047 product Substances 0.000 description 14
239000002904 solvent Substances 0.000 description 14
239000000243 solution Substances 0.000 description 13
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 12
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 10
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 10
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 8
230000035484 reaction time Effects 0.000 description 7
235000011121 sodium hydroxide Nutrition 0.000 description 7
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 6
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 6
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 6
BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 5
239000004593 Epoxy Substances 0.000 description 5
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 5
150000001412 amines Chemical class 0.000 description 5
229910021529 ammonia Inorganic materials 0.000 description 5
239000007795 chemical reaction product Substances 0.000 description 4
235000011007 phosphoric acid Nutrition 0.000 description 4
229920000647 polyepoxide Polymers 0.000 description 4
238000005406 washing Methods 0.000 description 4
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
-1 alkyl aromatic sulfonic acids Chemical class 0.000 description 3
239000000460 chlorine Substances 0.000 description 3
229910052801 chlorine Inorganic materials 0.000 description 3
239000011248 coating agent Substances 0.000 description 3
238000000576 coating method Methods 0.000 description 3
239000012153 distilled water Substances 0.000 description 3
239000003822 epoxy resin Substances 0.000 description 3
238000002474 experimental method Methods 0.000 description 3
239000000706 filtrate Substances 0.000 description 3
LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 3
YLGXILFCIXHCMC-JHGZEJCSSA-N methyl cellulose Chemical compound COC1C(OC)C(OC)C(COC)O[C@H]1O[C@H]1C(OC)C(OC)C(OC)OC1COC YLGXILFCIXHCMC-JHGZEJCSSA-N 0.000 description 3
239000000203 mixture Substances 0.000 description 3
230000007935 neutral effect Effects 0.000 description 3
229920001983 poloxamer Polymers 0.000 description 3
229920000570 polyether Polymers 0.000 description 3
238000002360 preparation method Methods 0.000 description 3
150000003141 primary amines Chemical class 0.000 description 3
239000011541 reaction mixture Substances 0.000 description 3
150000003335 secondary amines Chemical class 0.000 description 3
238000003756 stirring Methods 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
SLABEOONBHLKSD-UHFFFAOYSA-N O=S1(=O)C(C=C2)=CC=C2OOC2=CC=C1C=C2 Chemical compound O=S1(=O)C(C=C2)=CC=C2OOC2=CC=C1C=C2 SLABEOONBHLKSD-UHFFFAOYSA-N 0.000 description 2
239000004721 Polyphenylene oxide Substances 0.000 description 2
GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 2
125000001931 aliphatic group Chemical group 0.000 description 2
229910000147 aluminium phosphate Inorganic materials 0.000 description 2
238000013459 approach Methods 0.000 description 2
239000001913 cellulose Substances 0.000 description 2
229920002678 cellulose Polymers 0.000 description 2
239000012084 conversion product Substances 0.000 description 2
238000001816 cooling Methods 0.000 description 2
MIHINWMALJZIBX-UHFFFAOYSA-N cyclohexa-2,4-dien-1-ol Chemical class OC1CC=CC=C1 MIHINWMALJZIBX-UHFFFAOYSA-N 0.000 description 2
239000012535 impurity Substances 0.000 description 2
238000002955 isolation Methods 0.000 description 2
239000011049 pearl Substances 0.000 description 2
239000001294 propane Substances 0.000 description 2
238000010992 reflux Methods 0.000 description 2
229920005989 resin Polymers 0.000 description 2
239000011347 resin Substances 0.000 description 2
229920001169 thermoplastic Polymers 0.000 description 2
239000004416 thermosoftening plastic Substances 0.000 description 2
229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 description 1
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
239000005977 Ethylene Substances 0.000 description 1
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
229930194542 Keto Natural products 0.000 description 1
229920000881 Modified starch Polymers 0.000 description 1
RVGRUAULSDPKGF-UHFFFAOYSA-N Poloxamer Chemical compound C1CO1.CC1CO1 RVGRUAULSDPKGF-UHFFFAOYSA-N 0.000 description 1
229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
239000004372 Polyvinyl alcohol Substances 0.000 description 1
229920002359 Tetronic® Polymers 0.000 description 1
239000000654 additive Substances 0.000 description 1
230000000996 additive effect Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
229910001508 alkali metal halide Inorganic materials 0.000 description 1
150000008045 alkali metal halides Chemical class 0.000 description 1
150000008044 alkali metal hydroxides Chemical class 0.000 description 1
239000012670 alkaline solution Substances 0.000 description 1
125000003277 amino group Chemical group 0.000 description 1
150000001450 anions Chemical group 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
238000009835 boiling Methods 0.000 description 1
239000001768 carboxy methyl cellulose Substances 0.000 description 1
235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
239000008112 carboxymethyl-cellulose Substances 0.000 description 1
150000003945 chlorohydrins Chemical class 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
230000003750 conditioning effect Effects 0.000 description 1
125000004122 cyclic group Chemical group 0.000 description 1
229940075894 denatured ethanol Drugs 0.000 description 1
150000004985 diamines Chemical class 0.000 description 1
235000014113 dietary fatty acids Nutrition 0.000 description 1
ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 1
HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 description 1
GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical class C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 description 1
LVTYICIALWPMFW-UHFFFAOYSA-N diisopropanolamine Chemical compound CC(O)CNCC(C)O LVTYICIALWPMFW-UHFFFAOYSA-N 0.000 description 1
229940043276 diisopropanolamine Drugs 0.000 description 1
238000004821 distillation Methods 0.000 description 1
238000009826 distribution Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000001804 emulsifying effect Effects 0.000 description 1
150000002170 ethers Chemical class 0.000 description 1
235000010944 ethyl methyl cellulose Nutrition 0.000 description 1
239000000194 fatty acid Substances 0.000 description 1
229930195729 fatty acid Natural products 0.000 description 1
150000004665 fatty acids Chemical class 0.000 description 1
239000000835 fiber Substances 0.000 description 1
239000012065 filter cake Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
150000002334 glycols Chemical class 0.000 description 1
150000002431 hydrogen Chemical class 0.000 description 1
125000000468 ketone group Chemical group 0.000 description 1
239000000463 material Substances 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
229920003087 methylethyl cellulose Polymers 0.000 description 1
235000019426 modified starch Nutrition 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
150000002924 oxiranes Chemical class 0.000 description 1
239000003973 paint Substances 0.000 description 1
238000010422 painting Methods 0.000 description 1
230000000704 physical effect Effects 0.000 description 1
239000004033 plastic Substances 0.000 description 1
229920003023 plastic Polymers 0.000 description 1
238000006068 polycondensation reaction Methods 0.000 description 1
239000004848 polyfunctional curative Substances 0.000 description 1
229920002451 polyvinyl alcohol Polymers 0.000 description 1
235000019422 polyvinyl alcohol Nutrition 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
230000001376 precipitating effect Effects 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
239000002243 precursor Substances 0.000 description 1
238000003825 pressing Methods 0.000 description 1
QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
108090000623 proteins and genes Proteins 0.000 description 1
239000002994 raw material Substances 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
159000000000 sodium salts Chemical class 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000000126 substance Substances 0.000 description 1
PXQLVRUNWNTZOS-UHFFFAOYSA-N sulfanyl Chemical class [SH] PXQLVRUNWNTZOS-UHFFFAOYSA-N 0.000 description 1
238000010626 work up procedure Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/02—Polycondensates containing more than one epoxy group per molecule
- C08G59/04—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof
- C08G59/06—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols
- C08G59/063—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols with epihalohydrins

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Epoxy Resins (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)

CH103265A 1964-01-28 1965-01-25 Verfahren zur Herstellung von pulver- oder perlförmigen Kondensationsprodukten aus 2-wertigen phenolischen Verbindungen und Epihalogenhydrinen CH439759A (de)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
DED0043460		1964-01-28
DED0045023		1964-07-23
DED0045078		1964-07-30

Publications (1)

Publication Number	Publication Date
CH439759A true CH439759A (de)	1967-07-15

Family

ID=27209787

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CH103265A CH439759A (de)	1964-01-28	1965-01-25	Verfahren zur Herstellung von pulver- oder perlförmigen Kondensationsprodukten aus 2-wertigen phenolischen Verbindungen und Epihalogenhydrinen

Country Status (5)

Country	Link
BE (1)	BE658650A (fr)
CH (1)	CH439759A (fr)
FR (1)	FR1432615A (fr)
GB (1)	GB1088496A (fr)
NL (1)	NL6500994A (fr)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2914297C2 (de)	1979-04-09	1981-10-01	Basf Ag, 6700 Ludwigshafen	Verfahren zur Herstellung von Polyadditionsprodukten aus Ammoniak und Epoxidverbindungen und ihre Verwendung
US4260727A (en) *	1979-07-23	1981-04-07	Henkel Corporation	Epoxy-amine adducts for use in electrodeposition
MX2012002315A (es)	2009-08-24	2012-04-11	Dow Global Technologies Llc	Metodo para elaborar una resina epoxica particulada.
BR112012007770A2 (pt) *	2009-10-07	2019-09-24	Dow Global Technologies Llc	método para preparar uma resina epóxi sólida na forma de um particulado discreto e resina epóxi sólida

1965
- 1965-01-20 FR FR2649A patent/FR1432615A/fr not_active Expired
- 1965-01-21 BE BE658650A patent/BE658650A/fr unknown
- 1965-01-25 CH CH103265A patent/CH439759A/de unknown
- 1965-01-27 GB GB3710/65A patent/GB1088496A/en not_active Expired
- 1965-01-27 NL NL6500994A patent/NL6500994A/nl unknown

Also Published As

Publication number	Publication date
FR1432615A (fr)	1966-03-25
BE658650A (fr)	1965-07-22
NL6500994A (nl)	1965-07-29
GB1088496A (en)	1967-10-25

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DE69329152T2 (de)	2001-06-07	Herstellung von polysuccinimid und polyasparginsäure aus maleinanhydrid und ammoniak
AT157715B (de)	1940-01-10	Verfahren zur Herstellung von Aldehyd-Kondensationsprodukten.
CH668075A5 (de)	1988-11-30	Verfahren zur herstellung von natriumsalzen von lignosulfonsaeuren, die sich fuer die verwendung als farbstoff- und druckpastenadditive eignen.
DE3633421C1 (de)	1987-07-23	Hydroxyl- und Sulfonatgruppen aufweisende Polyoxyalkylenether und deren Verwendung zur Herstellung von dispergierbaren Polyurethanen
EP0069267A1 (fr)	1983-01-12	Procédé de préparation de cocondensats collants résistant aux intempéries
DE2347233C2 (de)	1982-12-02	Verfahren zur Herstellung von Epoxy- Novolakharzen
DE2105783A1 (de)	1972-09-07	Verfahren zur Herstellung von Aminotriazinderivaten
CH668773A5 (de)	1989-01-31	Verfahren zur herstellung von ammoniumsalzen von lignosulfonsaeuren, die fuer die verwendung als additive in farbstoffpraeparaten und waessrigen kohleaufschlaemmungen geeignet sind.
DE1138030B (de)	1962-10-18	Verfahren zur Herstellung von Bis-(ª‰-oxyaethyl)-terephthalat
DE102005022228A1 (de)	2006-11-23	Melamin-Formaldehyd Harzlösung und Verfahren zu deren Herstellung
DE1282653B (de)	1968-11-14	Herstellung von festen Glycidylaethern mehrwertiger Phenole
AT285175B (de)	1970-10-12	Verfahren zur Herstellung von pulver- oder perlförmigen Kondensationsprodukten aus 2-wertigen phenolischen Verbindungen mit Epihalogenhydrinen
DE2750542A1 (de)	1978-05-18	Verfahren zur herstellung von polymeren, die freie oder in salzform befindliche aminische gruppen und quaternaere ammoniumgruppen enthalten sowie die dabei erhaltenen produkte
DE1103582B (de)	1961-03-30	Verfahren zur Herstellung haertbarer Aminotriazin-Kondensations-produkte
CH390892A (de)	1965-04-30	Verfahren zur Herstellung von Dialdehydopolysaccharid-Acrylamid-Derivaten
EP0054755A1 (fr)	1982-06-30	Procédé de préparation d'une solution aqueuse stable au stockage à base d'une résine mélamine formaldéhyde
AT332128B (de)	1976-09-10	Verfahren zur emulgierung und hartung von epoxyharzen
DE1300670B (de)	1969-10-02	Verfahren zur Herstellung von wasserloeslicher und wasserunloeslicher Hydroxyalkylamylose
DE612626C (de)	1935-09-16	Verfahren zur Herstellung wasserunloeslicher Harze aus Harnstoff oder dessen Derivaten und Formaldehyd bzw. dessen Polymeren
DE1595206A1 (de)	1970-04-16	Verfahren zur Herstellung formaldehydarmer,veraetherter Aminotriazinharze
DE2516898A1 (de)	1975-10-23	Verfahren zur herstellung von durch waermeeinwirkung abbindenden phenol/formaldehyd-harzen
DE601539C (de)	1934-08-17	Verfahren zur Herstellung von harzartigen Kondensationsprodukten aus Phenolen, Harnstoff und Aldehyden
DE2604195C2 (de)	1984-03-08	Verfahren zur Herstellung von Melamin-Formaldehydharzen
CH193630A (de)	1937-10-31	Verfahren zur Herstellung eines harzartigen Aldehyd-Kondensationsproduktes.
AT160709B (de)	1941-12-10	Verfahren zur Herstellung von Kondensationsprodukten.