CH626064A5 - - Google Patents

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Info

Publication number: CH626064A5
Authority: CH; Switzerland
Prior art keywords: mixture; process step; mol; hydroxymethylphthalimide; amount
Prior art date: 1975-03-10

Application number

CH278676A

Other languages

German (de)

English (en)

Inventor

Shen-Fu Liang

Richard Alan Zeleny

Original Assignee

Stauffer Chemical Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-03-10

Filing date

1976-03-05

Publication date

1981-10-30

1976-03-05 Application filed by Stauffer Chemical Co filed Critical Stauffer Chemical Co

1981-10-30 Publication of CH626064A5 publication Critical patent/CH626064A5/de

Links

VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 88
238000000034 method Methods 0.000 claims description 83
MNSGOOCAMMSKGI-UHFFFAOYSA-N N-(hydroxymethyl)phthalimide Chemical compound C1=CC=C2C(=O)N(CO)C(=O)C2=C1 MNSGOOCAMMSKGI-UHFFFAOYSA-N 0.000 claims description 53
238000006243 chemical reaction Methods 0.000 claims description 49
UHOVQNZJYSORNB-UHFFFAOYSA-N monobenzene Natural products C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 40
239000000203 mixture Substances 0.000 claims description 35
JKGLRGGCGUQNEX-UHFFFAOYSA-N 2-(chloromethyl)isoindole-1,3-dione Chemical compound C1=CC=C2C(=O)N(CCl)C(=O)C2=C1 JKGLRGGCGUQNEX-UHFFFAOYSA-N 0.000 claims description 31
239000003960 organic solvent Substances 0.000 claims description 30
239000002904 solvent Substances 0.000 claims description 17
239000012074 organic phase Substances 0.000 claims description 16
239000011541 reaction mixture Substances 0.000 claims description 8
238000002360 preparation method Methods 0.000 claims description 7
-1 mercaptomethyl Chemical group 0.000 claims description 6
229910052708 sodium Inorganic materials 0.000 claims description 4
239000011734 sodium Substances 0.000 claims description 4
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 2
229910019142 PO4 Inorganic materials 0.000 claims 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 1
239000010452 phosphate Substances 0.000 claims 1
XKJCHHZQLQNZHY-UHFFFAOYSA-N phthalimide Chemical compound C1=CC=C2C(=O)NC(=O)C2=C1 XKJCHHZQLQNZHY-UHFFFAOYSA-N 0.000 claims 1
RYYWUUFWQRZTIU-UHFFFAOYSA-K thiophosphate Chemical compound [O-]P([O-])([O-])=S RYYWUUFWQRZTIU-UHFFFAOYSA-K 0.000 claims 1
150000002148 esters Chemical class 0.000 description 15
239000012071 phase Substances 0.000 description 12
239000002253 acid Substances 0.000 description 9
150000003839 salts Chemical class 0.000 description 8
238000004519 manufacturing process Methods 0.000 description 7
239000000047 product Substances 0.000 description 6
239000007795 chemical reaction product Substances 0.000 description 5
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
239000008346 aqueous phase Substances 0.000 description 4
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
238000000926 separation method Methods 0.000 description 3
239000000243 solution Substances 0.000 description 3
KOITVPOIFJTHPW-UHFFFAOYSA-N 2-(sulfanylmethyl)isoindole-1,3-dione Chemical compound C1=CC=C2C(=O)N(CS)C(=O)C2=C1 KOITVPOIFJTHPW-UHFFFAOYSA-N 0.000 description 2
238000005660 chlorination reaction Methods 0.000 description 2
238000001816 cooling Methods 0.000 description 2
239000000839 emulsion Substances 0.000 description 2
239000012065 filter cake Substances 0.000 description 2
239000011780 sodium chloride Substances 0.000 description 2
238000010626 work up procedure Methods 0.000 description 2
WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
101150054880 NASP gene Proteins 0.000 description 1
238000009825 accumulation Methods 0.000 description 1
239000003513 alkali Substances 0.000 description 1
238000013459 approach Methods 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
238000010923 batch production Methods 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
238000004140 cleaning Methods 0.000 description 1
239000000498 cooling water Substances 0.000 description 1
238000004821 distillation Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
239000000463 material Substances 0.000 description 1
239000012454 non-polar solvent Substances 0.000 description 1
238000005086 pumping Methods 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
238000005292 vacuum distillation Methods 0.000 description 1
238000005406 washing Methods 0.000 description 1
239000002699 waste material Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D209/00—Heterocyclic compounds containing five-membered rings, condensed with other rings, with one nitrogen atom as the only ring hetero atom
- C07D209/02—Heterocyclic compounds containing five-membered rings, condensed with other rings, with one nitrogen atom as the only ring hetero atom condensed with one carbocyclic ring
- C07D209/44—Iso-indoles; Hydrogenated iso-indoles
- C07D209/48—Iso-indoles; Hydrogenated iso-indoles with oxygen atoms in positions 1 and 3, e.g. phthalimide
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
- C07F9/5537—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom the heteroring containing the structure -C(=O)-N-C(=O)- (both carbon atoms belong to the heteroring)

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Biochemistry (AREA)
General Health & Medical Sciences (AREA)
Molecular Biology (AREA)
Indole Compounds (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

CH278676A 1975-03-10 1976-03-05 CH626064A5 (fr)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US05/557,002 US4013685A (en)	1975-03-10	1975-03-10	Process for the manufacture of n(mercaptomethyl) phthalimide s-(o,o-dimethyl phosphorodithioate

Publications (1)

Publication Number	Publication Date
CH626064A5 true CH626064A5 (fr)	1981-10-30

Family

ID=24223672

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CH278676A CH626064A5 (fr)	1975-03-10	1976-03-05

Country Status (27)

Country	Link
US (1)	US4013685A (fr)
JP (1)	JPS51108063A (fr)
AU (1)	AU1054676A (fr)
BE (1)	BE839213A (fr)
BG (2)	BG26524A3 (fr)
BR (1)	BR7600985A (fr)
CA (1)	CA1057293A (fr)
CH (1)	CH626064A5 (fr)
CS (1)	CS201537B2 (fr)
DD (1)	DD126602A5 (fr)
DE (1)	DE2607825A1 (fr)
DK (1)	DK141072B (fr)
ES (1)	ES445911A1 (fr)
FR (1)	FR2303800A1 (fr)
GB (1)	GB1487038A (fr)
HU (1)	HU174831B (fr)
IL (1)	IL48886A (fr)
IN (2)	IN144856B (fr)
IT (1)	IT1057937B (fr)
NL (1)	NL7601186A (fr)
NZ (1)	NZ179813A (fr)
PH (1)	PH12871A (fr)
PL (2)	PL104430B1 (fr)
RO (1)	RO76089A (fr)
SU (1)	SU652897A3 (fr)
TR (1)	TR18734A (fr)
ZA (1)	ZA76450B (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE3347913A1 (de) *	1983-03-25	1985-06-27	LuK Lamellen und Kupplungsbau GmbH, 7580 Bühl	Reibungskupplung

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2767194A (en) *	1955-03-18	1956-10-16	Stauffer Chemical Co	Compositions of matter

1975
- 1975-03-10 US US05/557,002 patent/US4013685A/en not_active Expired - Lifetime
1976
- 1976-01-21 IL IL48886A patent/IL48886A/xx unknown
- 1976-01-22 NZ NZ179813A patent/NZ179813A/xx unknown
- 1976-01-23 AU AU10546/76A patent/AU1054676A/en not_active Expired
- 1976-01-27 ZA ZA450A patent/ZA76450B/xx unknown
- 1976-01-27 GB GB3049/76A patent/GB1487038A/en not_active Expired
- 1976-02-03 JP JP51010081A patent/JPS51108063A/ja active Pending
- 1976-02-05 NL NL7601186A patent/NL7601186A/xx not_active Application Discontinuation
- 1976-02-06 IN IN213/CAL/76A patent/IN144856B/en unknown
- 1976-02-11 CA CA245,523A patent/CA1057293A/fr not_active Expired
- 1976-02-12 DK DK57876AA patent/DK141072B/da not_active IP Right Cessation
- 1976-02-17 BR BR7600985A patent/BR7600985A/pt unknown
- 1976-02-26 SU SU762325152A patent/SU652897A3/ru active
- 1976-02-26 DE DE19762607825 patent/DE2607825A1/de not_active Withdrawn
- 1976-03-03 PH PH18167A patent/PH12871A/en unknown
- 1976-03-04 BE BE7000791A patent/BE839213A/xx not_active IP Right Cessation
- 1976-03-05 CH CH278676A patent/CH626064A5/de not_active IP Right Cessation
- 1976-03-05 FR FR7606295A patent/FR2303800A1/fr active Granted
- 1976-03-08 IT IT48449/76A patent/IT1057937B/it active
- 1976-03-09 TR TR18734A patent/TR18734A/xx unknown
- 1976-03-09 HU HU76SA2898A patent/HU174831B/hu unknown
- 1976-03-09 ES ES445911A patent/ES445911A1/es not_active Expired
- 1976-03-10 DD DD191779A patent/DD126602A5/xx unknown
- 1976-03-10 CS CS761573A patent/CS201537B2/cs unknown
- 1976-03-10 PL PL1976200091A patent/PL104430B1/pl unknown
- 1976-03-10 BG BG032576A patent/BG26524A3/xx unknown
- 1976-03-10 PL PL1976187820A patent/PL98622B1/pl unknown
- 1976-03-10 BG BG033633A patent/BG26525A4/xx unknown
- 1976-03-30 RO RO7684982A patent/RO76089A/fr unknown
1977
- 1977-04-19 IN IN596/CAL/77A patent/IN145005B/en unknown

Also Published As

Publication number	Publication date
ZA76450B (en)	1977-01-26
TR18734A (tr)	1977-07-27
PH12871A (en)	1979-09-25
CS201537B2 (en)	1980-11-28
ES445911A1 (es)	1977-11-01
FR2303800A1 (fr)	1976-10-08
IN144856B (fr)	1978-07-15
GB1487038A (en)	1977-09-28
IL48886A (en)	1980-10-26
US4013685A (en)	1977-03-22
DK141072B (da)	1980-01-07
DE2607825A1 (de)	1976-09-23
DK57876A (fr)	1976-09-11
AU1054676A (en)	1977-07-28
IN145005B (fr)	1978-08-12
BR7600985A (pt)	1976-09-14
NZ179813A (en)	1978-04-03
DK141072C (fr)	1980-06-16
IL48886A0 (en)	1976-03-31
BG26525A4 (bg)	1979-04-12
NL7601186A (nl)	1976-09-14
PL104430B1 (pl)	1979-08-31
PL98622B1 (pl)	1978-05-31
BE839213A (nl)	1976-09-06
HU174831B (hu)	1980-03-28
RO76089A (fr)	1981-04-30
IT1057937B (it)	1982-03-30
FR2303800B1 (fr)	1982-01-29
BG26524A3 (bg)	1979-04-12
CA1057293A (fr)	1979-06-26
DD126602A5 (fr)	1977-08-03
SU652897A3 (ru)	1979-03-15
JPS51108063A (fr)	1976-09-25

Legal Events

Date	Code	Title	Description
1984-11-30	PL	Patent ceased
2024-10-31	PL	Patent ceased

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