CH626113A5 - Process for preparing concentrated water-soluble stock solutions of sulpho-containing 1:2 chromium complexes - Google Patents

Process for preparing concentrated water-soluble stock solutions of sulpho-containing 1:2 chromium complexes Download PDF

Info

Publication number: CH626113A5
Authority: CH; Switzerland
Prior art keywords: parts; chromium; sulpho; stock solutions; concentrated water
Prior art date: 1976-08-25

Application number

CH1040977A

Other languages

German (de)

English (en)

Inventor

Otto Dr Kaufmann

Original Assignee

Basf Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1976-08-25

Filing date

1977-08-25

Publication date

1981-10-30

1977-08-25 Application filed by Basf Ag filed Critical Basf Ag

1981-10-30 Publication of CH626113A5 publication Critical patent/CH626113A5/de

Links

239000011550 stock solution Substances 0.000 title description 7
150000001844 chromium Chemical class 0.000 title description 5
238000004519 manufacturing process Methods 0.000 title 1
-1 sulpho Chemical class 0.000 title 1
239000000975 dye Substances 0.000 description 14
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
239000011651 chromium Substances 0.000 description 10
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 9
229910052804 chromium Inorganic materials 0.000 description 9
239000001257 hydrogen Substances 0.000 description 9
229910052739 hydrogen Inorganic materials 0.000 description 9
239000000203 mixture Substances 0.000 description 9
239000000243 solution Substances 0.000 description 9
125000004435 hydrogen atom Chemical group [H]* 0.000 description 7
239000011877 solvent mixture Substances 0.000 description 7
JWAZRIHNYRIHIV-UHFFFAOYSA-N 2-naphthol Chemical compound C1=CC=CC2=CC(O)=CC=C21 JWAZRIHNYRIHIV-UHFFFAOYSA-N 0.000 description 6
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 6
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 6
239000000987 azo dye Substances 0.000 description 5
125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 5
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 4
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
240000007817 Olea europaea Species 0.000 description 4
239000000460 chlorine Substances 0.000 description 4
229910052801 chlorine Inorganic materials 0.000 description 4
150000002431 hydrogen Chemical class 0.000 description 4
238000000034 method Methods 0.000 description 4
238000002360 preparation method Methods 0.000 description 4
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
150000001768 cations Chemical class 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
OAYXUHPQHDHDDZ-UHFFFAOYSA-N 2-(2-butoxyethoxy)ethanol Chemical compound CCCCOCCOCCO OAYXUHPQHDHDDZ-UHFFFAOYSA-N 0.000 description 2
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
ZHNUHDYFZUAESO-UHFFFAOYSA-N Formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 description 2
AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 description 2
OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 2
125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 description 2
239000002253 acid Substances 0.000 description 2
125000000217 alkyl group Chemical group 0.000 description 2
235000011114 ammonium hydroxide Nutrition 0.000 description 2
125000004432 carbon atom Chemical group C* 0.000 description 2
238000001816 cooling Methods 0.000 description 2
230000008878 coupling Effects 0.000 description 2
238000010168 coupling process Methods 0.000 description 2
238000005859 coupling reaction Methods 0.000 description 2
239000000706 filtrate Substances 0.000 description 2
239000012535 impurity Substances 0.000 description 2
239000003960 organic solvent Substances 0.000 description 2
235000006408 oxalic acid Nutrition 0.000 description 2
125000001501 propionyl group Chemical group O=C([*])C([H])([H])C([H])([H])[H] 0.000 description 2
SMQUZDBALVYZAC-UHFFFAOYSA-N salicylaldehyde Chemical compound OC1=CC=CC=C1C=O SMQUZDBALVYZAC-UHFFFAOYSA-N 0.000 description 2
238000003756 stirring Methods 0.000 description 2
125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 2
125000000542 sulfonic acid group Chemical group 0.000 description 2
210000002268 wool Anatomy 0.000 description 2
ONMOULMPIIOVTQ-UHFFFAOYSA-N 98-47-5 Chemical compound OS(=O)(=O)C1=CC=CC([N+]([O-])=O)=C1 ONMOULMPIIOVTQ-UHFFFAOYSA-N 0.000 description 1
FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 1
SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
239000013078 crystal Substances 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
150000003948 formamides Chemical class 0.000 description 1
238000002955 isolation Methods 0.000 description 1
QVEIBLDXZNGPHR-UHFFFAOYSA-N naphthalene-1,4-dione;diazide Chemical class [N-]=[N+]=[N-].[N-]=[N+]=[N-].C1=CC=C2C(=O)C=CC(=O)C2=C1 QVEIBLDXZNGPHR-UHFFFAOYSA-N 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
235000011149 sulphuric acid Nutrition 0.000 description 1
235000002906 tartaric acid Nutrition 0.000 description 1
239000011975 tartaric acid Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B45/00—Complex metal compounds of azo dyes
- C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
- C09B45/14—Monoazo compounds
- C09B45/16—Monoazo compounds containing chromium
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0072—Preparations with anionic dyes or reactive dyes
- C09B67/0073—Preparations of acid or reactive dyes in liquid form

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Coloring (AREA)

CH1040977A 1976-08-25 1977-08-25 Process for preparing concentrated water-soluble stock solutions of sulpho-containing 1:2 chromium complexes CH626113A5 (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE19762638222 DE2638222C3 (de)	1976-08-25	1976-08-25	Verfahren zur Herstellung konzentrierter wasserlöslicher Stammlösungen von sulf ongruppenhaltigen 1 zu 2-Chromkomplexen

Publications (1)

Publication Number	Publication Date
CH626113A5 true CH626113A5 (en)	1981-10-30

Family

ID=5986322

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CH1040977A CH626113A5 (en)	1976-08-25	1977-08-25	Process for preparing concentrated water-soluble stock solutions of sulpho-containing 1:2 chromium complexes

Country Status (6)

Country	Link
JP (1)	JPS5326825A (it)
CH (1)	CH626113A5 (it)
DE (1)	DE2638222C3 (it)
FR (1)	FR2362900A2 (it)
GB (1)	GB1581469A (it)
IT (1)	IT1115775B (it)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4507125A (en) *	1982-11-02	1985-03-26	Ciba-Geigy Corporation	Use of 1:2 chrome complex dyes for dyeing leather and furs

1976
- 1976-08-25 DE DE19762638222 patent/DE2638222C3/de not_active Expired
1977
- 1977-08-01 IT IT5052377A patent/IT1115775B/it active
- 1977-08-10 GB GB3348977A patent/GB1581469A/en not_active Expired
- 1977-08-17 FR FR7725106A patent/FR2362900A2/fr not_active Withdrawn
- 1977-08-23 JP JP10022977A patent/JPS5326825A/ja active Pending
- 1977-08-25 CH CH1040977A patent/CH626113A5/de not_active IP Right Cessation

Also Published As

Publication number	Publication date
DE2638222C3 (de)	1980-08-21
DE2638222A1 (de)	1978-03-02
DE2638222B2 (de)	1979-12-06
JPS5326825A (en)	1978-03-13
GB1581469A (en)	1980-12-17
IT1115775B (it)	1986-02-03
FR2362900A2 (fr)	1978-03-24

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Legal Events

Date	Code	Title	Description
1987-04-30	PL	Patent ceased
2024-10-31	PL	Patent ceased