CH90705A - Process for the preparation of a monoazo dye. - Google Patents
Process for the preparation of a monoazo dye.Info
- Publication number
- CH90705A CH90705A CH90705DA CH90705A CH 90705 A CH90705 A CH 90705A CH 90705D A CH90705D A CH 90705DA CH 90705 A CH90705 A CH 90705A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- dye
- monoazo dye
- nitro
- good
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 3
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 title description 3
- 210000002268 wool Anatomy 0.000 claims description 3
- ZYECOAILUNWEAL-NUDFZHEQSA-N (4z)-4-[[2-methoxy-5-(phenylcarbamoyl)phenyl]hydrazinylidene]-n-(3-nitrophenyl)-3-oxonaphthalene-2-carboxamide Chemical compound COC1=CC=C(C(=O)NC=2C=CC=CC=2)C=C1N\N=C(C1=CC=CC=C1C=1)/C(=O)C=1C(=O)NC1=CC=CC([N+]([O-])=O)=C1 ZYECOAILUNWEAL-NUDFZHEQSA-N 0.000 claims description 2
- 239000003929 acidic solution Substances 0.000 claims 1
- 239000000975 dye Substances 0.000 description 5
- 239000002253 acid Substances 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 238000009963 fulling Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
Landscapes
- Coloring (AREA)
Description
Verfahren zur Darstellung eines Monoazofarbstoffes. Es wurde gefunden, dass man einen wert vollen Monoazofarbstoff erhält, wenn man die Diazoverbii <B>'</B> idung des 5-Nitro-2-amirio- benzol-l-earboiisäLiremethyl,itriilids -mit der 2- Methylaminonaphtaliii-7-stilfosäure in saurer Kupplung vereinigt.
Das neue Produkt färbt Wolle in saurem Bade in rotvioletten Tönen an. Es zeigt neben guter Walk- und Lichtechtheit ein gutes Egalisierungsvermögen.
<I>Beispiel:</I> <B>271</B> Gewichtsteile 5-Nitro-2-amiiiobenzol- 1-carbonsäuremethylanilid (Schmelzpunkt<B>183</B> bis. 184') werden diazotiert und bei Gegen wart von Natriumacetat mit<B>237</B> Gewichts teilen 2-Methylarninoiiaphtalin-7-stilfosä#ire vereinigt. Nach beendigter Kupplung wird der Farbstoff ausgesalzen und wie üblich aufgearbeitet.
Er färbt Wolle in rotvioletten. Tönen an, die sich durch gutes Egalisierungs- vermögen, Walk- und Lichteobtu'eif au s- zeichnen.
Process for the preparation of a monoazo dye. It has been found that a valuable monoazo dye is obtained if the diazoverbii <B> '</B> idung of 5-nitro-2-amirio-benzene-l-earboiisäLiremethyl, itriilids -with the 2- methylaminonaphtaliii-7- stilfosäure combined in acid coupling.
The new product dyes wool in an acid bath in red-violet tones. In addition to good fullness and lightfastness, it shows good leveling properties.
<I> Example: </I> <B> 271 </B> parts by weight of 5-nitro-2-amiobenzene-1-carboxylic acid methyl anilide (melting point 183 to 184 ') are diazotized and, if present, of sodium acetate with <B> 237 </B> parts by weight 2-Methylarninoiiaphtalin-7-stilfosä # ire combined. When the coupling is complete, the dye is salted out and worked up as usual.
He dyes wool in reddish-purple. Tones that are characterized by good equalization, fulling and light obtu'eif.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE90705X | 1916-07-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH90705A true CH90705A (en) | 1921-09-16 |
Family
ID=5643354
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH90705D CH90705A (en) | 1916-07-25 | 1917-06-26 | Process for the preparation of a monoazo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH90705A (en) |
-
1917
- 1917-06-26 CH CH90705D patent/CH90705A/en unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CH88562A (en) | Process for the preparation of an azo dye. | |
| AT88347B (en) | Process for the preparation of monoazo dyes. | |
| AT118399B (en) | Process for the preparation of azo dyes. | |
| CH185840A (en) | Process for the preparation of an azo dye. | |
| CH194955A (en) | Process for the preparation of a new monoazo dye. | |
| CH185842A (en) | Process for the preparation of an azo dye. | |
| CH167392A (en) | Process for the preparation of an azo dye. | |
| CH183593A (en) | Process for the preparation of an azo dye. | |
| CH170931A (en) | Process for the preparation of a monoazo dye. | |
| CH170932A (en) | Process for the preparation of a monoazo dye. | |
| CH302404A (en) | Process for the preparation of a trisazo dye. | |
| CH183592A (en) | Process for the preparation of an azo dye. | |
| CH167391A (en) | Process for the preparation of an azo dye. | |
| CH184768A (en) | Process for the preparation of an azo dye. | |
| CH164547A (en) | Process for the preparation of an azo dye. | |
| CH238791A (en) | Process for the preparation of a new monoazo dye. | |
| CH180962A (en) | Process for the preparation of an azo dye. | |
| CH210500A (en) | Process for the preparation of a monoazo dye. | |
| CH217236A (en) | Process for the preparation of a new disazo dye. | |
| CH189041A (en) | Process for the preparation of a monoazo dye. | |
| CH240128A (en) | Process for the preparation of a new monoazo dye. | |
| CH183596A (en) | Process for the preparation of an azo dye. | |
| CH146771A (en) | Process for the preparation of an azo dye. | |
| CH166089A (en) | Process for the preparation of an azo dye. | |
| CH230424A (en) | Process for the production of an acidic wool dye. |