CH98220A - Process for the preparation of an o-oxyazo dye. - Google Patents

Process for the preparation of an o-oxyazo dye.

Info

Publication number
CH98220A
CH98220A CH98220DA CH98220A CH 98220 A CH98220 A CH 98220A CH 98220D A CH98220D A CH 98220DA CH 98220 A CH98220 A CH 98220A
Authority
CH
Switzerland
Prior art keywords
preparation
dye
oxyazo
wool
bath
Prior art date
Application number
Other languages
German (de)
Inventor
Anilin-Fabrikation Actien Fuer
Original Assignee
Anilin Fabrikation Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anilin Fabrikation Ag filed Critical Anilin Fabrikation Ag
Publication of CH98220A publication Critical patent/CH98220A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/10Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
    • C09B29/103Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group of the naphthalene series
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B45/00Complex metal compounds of azo dyes
    • C09B45/02Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
    • C09B45/14Monoazo compounds
    • C09B45/16Monoazo compounds containing chromium

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

  Verfahren zur Darstellung eines     o-Oxyazofarbstoffes.       Es wurde gefunden, dass durch Kuppeln  von     3.4.5-Trichlor-2-cliazo-l-oxybenzol    mit       8-Chlor-l-oxynaphtalin-5-sulfosäure    ein Farb  stoff erhalten wird, der .auf chromgebeizter  Wolle oder durch     Nachchromieren    der     in     saurem Bade entstehenden Färbungen, oder  beim Färben von Wolle im     Einbadverfahren     in Gegenwart von     Chromaten    und dissoziie  renden     Ammoniumsalzen    gleichmässige,     walk-,     licht-     -und    reibechte blaue Nuancen liefert.

           Beispiet:     Die aus 21 Teilen     3.4.5-Trichlar-2-          amino-l-oxybenzol,    50 Teilen Salzsäure von  12   De und 6,9 Teilen     Natriumnitrit    bereitete       Diazoverbindung        lässt    man in eine durch Soda  alkalisch gehaltene Lösung von 25,9 Teilen       8-Chlor-l-oxyna,phtalin-5-sulfosäure    einlau  fen. Nach     beendeter    Kupplung salzt man    .den Farbstoff aus und arbeitet ihn in der  üblichen Weise auf.



  Process for the preparation of an o-oxyazo dye. It has been found that by coupling 3.4.5-trichloro-2-cliazo-l-oxybenzene with 8-chloro-l-oxynaphthalene-5-sulfonic acid, a dye is obtained that can be used on chrome-stained wool or by re-chrome-plating in acidic Bath dyeing, or when dyeing wool in the single bath process in the presence of chromates and dissociating ammonium salts, provides uniform blue nuances that are fast to kneading, light and rub fast.

           Example: The diazo compound prepared from 21 parts of 3.4.5-Trichlar-2-amino-1-oxybenzene, 50 parts of hydrochloric acid of 12 De and 6.9 parts of sodium nitrite is left in a solution of 25.9 parts of 8- Chlorine-l-oxyna, phthaline-5-sulphonic acid enter. After coupling has ended, the dye is salted out and worked up in the usual way.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Darstellung eines o-Oxy- azofarbstoffes, der auf chromgebeizter Wolle oder durch Nachchromieren der in saurem Bade entstehenden Färbungen, oder beim Fär ben von Wolle im Einbadverfahren in Gegen wart von Chromaten und dissoziierenden Ammoniumsalzen, gleichmässige, walk-, licht und reibechte blaue Nuancen liefert, dadurch gekennzeichnet, dass man 3.4. PATENT CLAIM: Process for the preparation of an o-oxy-azo dye, which is applied to chrome-stained wool or by re-chroming the dyeings produced in an acid bath, or when dyeing wool in a single bath in the presence of chromates and dissociating ammonium salts, uniform, milled, light and provides rub-fast blue nuances, characterized in that 3.4. 5-Trichlor-2- .dazo-l-oxybenzol mit 8-Chlor-l-oxynaphta- lin-5-sulfosäure kuppelt. Coupling 5-trichloro-2-dazo-1-oxybenzene with 8-chloro-1-oxynaphthalene-5-sulfonic acid.
CH98220D 1920-07-08 1921-08-30 Process for the preparation of an o-oxyazo dye. CH98220A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH89057T 1920-07-08
CH98220T 1921-08-30

Publications (1)

Publication Number Publication Date
CH98220A true CH98220A (en) 1923-03-01

Family

ID=25703937

Family Applications (1)

Application Number Title Priority Date Filing Date
CH98220D CH98220A (en) 1920-07-08 1921-08-30 Process for the preparation of an o-oxyazo dye.

Country Status (1)

Country Link
CH (1) CH98220A (en)

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