CH98220A - Process for the preparation of an o-oxyazo dye. - Google Patents
Process for the preparation of an o-oxyazo dye.Info
- Publication number
- CH98220A CH98220A CH98220DA CH98220A CH 98220 A CH98220 A CH 98220A CH 98220D A CH98220D A CH 98220DA CH 98220 A CH98220 A CH 98220A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- dye
- oxyazo
- wool
- bath
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title claims description 3
- 238000004043 dyeing Methods 0.000 claims description 4
- 210000002268 wool Anatomy 0.000 claims description 4
- 230000008878 coupling Effects 0.000 claims description 3
- 238000010168 coupling process Methods 0.000 claims description 3
- 238000005859 coupling reaction Methods 0.000 claims description 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 2
- 150000003863 ammonium salts Chemical class 0.000 claims description 2
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical class [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 239000000987 azo dye Substances 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000008049 diazo compounds Chemical class 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/10—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
- C09B29/103—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group of the naphthalene series
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B45/00—Complex metal compounds of azo dyes
- C09B45/02—Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
- C09B45/14—Monoazo compounds
- C09B45/16—Monoazo compounds containing chromium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Verfahren zur Darstellung eines o-Oxyazofarbstoffes. Es wurde gefunden, dass durch Kuppeln von 3.4.5-Trichlor-2-cliazo-l-oxybenzol mit 8-Chlor-l-oxynaphtalin-5-sulfosäure ein Farb stoff erhalten wird, der .auf chromgebeizter Wolle oder durch Nachchromieren der in saurem Bade entstehenden Färbungen, oder beim Färben von Wolle im Einbadverfahren in Gegenwart von Chromaten und dissoziie renden Ammoniumsalzen gleichmässige, walk-, licht- -und reibechte blaue Nuancen liefert.
Beispiet: Die aus 21 Teilen 3.4.5-Trichlar-2- amino-l-oxybenzol, 50 Teilen Salzsäure von 12 De und 6,9 Teilen Natriumnitrit bereitete Diazoverbindung lässt man in eine durch Soda alkalisch gehaltene Lösung von 25,9 Teilen 8-Chlor-l-oxyna,phtalin-5-sulfosäure einlau fen. Nach beendeter Kupplung salzt man .den Farbstoff aus und arbeitet ihn in der üblichen Weise auf.
Process for the preparation of an o-oxyazo dye. It has been found that by coupling 3.4.5-trichloro-2-cliazo-l-oxybenzene with 8-chloro-l-oxynaphthalene-5-sulfonic acid, a dye is obtained that can be used on chrome-stained wool or by re-chrome-plating in acidic Bath dyeing, or when dyeing wool in the single bath process in the presence of chromates and dissociating ammonium salts, provides uniform blue nuances that are fast to kneading, light and rub fast.
Example: The diazo compound prepared from 21 parts of 3.4.5-Trichlar-2-amino-1-oxybenzene, 50 parts of hydrochloric acid of 12 De and 6.9 parts of sodium nitrite is left in a solution of 25.9 parts of 8- Chlorine-l-oxyna, phthaline-5-sulphonic acid enter. After coupling has ended, the dye is salted out and worked up in the usual way.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH89057T | 1920-07-08 | ||
| CH98220T | 1921-08-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH98220A true CH98220A (en) | 1923-03-01 |
Family
ID=25703937
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH98220D CH98220A (en) | 1920-07-08 | 1921-08-30 | Process for the preparation of an o-oxyazo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH98220A (en) |
-
1921
- 1921-08-30 CH CH98220D patent/CH98220A/en unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CH98220A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH98227A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH98222A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH98221A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH98223A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH98023A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH98228A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH98225A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH98020A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH98224A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH184781A (en) | Process for the preparation of an azo dye. | |
| CH187345A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH90854A (en) | Process for the preparation of a mordant dye. | |
| CH104917A (en) | Process for the production of a chromium-containing dye. | |
| CH172587A (en) | Process for the preparation of a chromium-containing azo dye. | |
| CH105142A (en) | Process for the production of a chromium-containing dye. | |
| CH115469A (en) | Process for the production of a chromium-containing dye. | |
| CH196345A (en) | Process for the preparation of an azo dye. | |
| CH90853A (en) | Process for the preparation of a mordant dye. | |
| CH170914A (en) | Process for the preparation of an azo dye. | |
| CH115465A (en) | Process for the production of a new azo dye. | |
| CH164437A (en) | Process for the production of a chromium-containing dye which coloring in red shades. | |
| CH187334A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH187344A (en) | Process for the preparation of an o-oxyazo dye. | |
| CH105655A (en) | Process for the production of a new chromium-containing dye. |