CN100480171C - 过氧化氢水溶液及其制备方法 - Google Patents

过氧化氢水溶液及其制备方法 Download PDF

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Publication number
CN100480171C
CN100480171C CNB038233797A CN03823379A CN100480171C CN 100480171 C CN100480171 C CN 100480171C CN B038233797 A CNB038233797 A CN B038233797A CN 03823379 A CN03823379 A CN 03823379A CN 100480171 C CN100480171 C CN 100480171C
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CN
China
Prior art keywords
hydrogen peroxide
aqueous hydrogen
peroxide solution
solution
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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CNB038233797A
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English (en)
Chinese (zh)
Other versions
CN1684904A (zh
Inventor
克劳迪娅·布拉塞
于尔根·格伦尼贝格
托马斯·哈斯
吉多·施托赫尼奥
沃尔夫冈·韦尔
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Evonik Operations GmbH
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Degussa GmbH
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Application filed by Degussa GmbH filed Critical Degussa GmbH
Publication of CN1684904A publication Critical patent/CN1684904A/zh
Application granted granted Critical
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C01B15/022—Preparation from organic compounds
    • C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C01B15/013—Separation; Purification; Concentration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C01B15/037—Stabilisation by additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)
  • Saccharide Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Preventing Corrosion Or Incrustation Of Metals (AREA)
CNB038233797A 2002-09-30 2003-09-23 过氧化氢水溶液及其制备方法 Expired - Lifetime CN100480171C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP02021967.1 2002-09-30
EP20020021967 EP1403219A1 (de) 2002-09-30 2002-09-30 Neue wässrige Wasserstoffperoxid Lösungen

Publications (2)

Publication Number Publication Date
CN1684904A CN1684904A (zh) 2005-10-19
CN100480171C true CN100480171C (zh) 2009-04-22

Family

ID=31970344

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB038233797A Expired - Lifetime CN100480171C (zh) 2002-09-30 2003-09-23 过氧化氢水溶液及其制备方法

Country Status (15)

Country Link
EP (2) EP1403219A1 (de)
JP (1) JP4528625B2 (de)
KR (1) KR100990351B1 (de)
CN (1) CN100480171C (de)
AT (1) ATE419221T1 (de)
AU (1) AU2003299090A1 (de)
BR (1) BR0314941B1 (de)
CA (1) CA2500396C (de)
DE (1) DE60325616D1 (de)
ES (1) ES2320652T5 (de)
MY (1) MY140875A (de)
PL (1) PL204518B1 (de)
RU (1) RU2336225C2 (de)
WO (1) WO2004028962A1 (de)
ZA (1) ZA200502512B (de)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
UY30962A1 (es) * 2007-03-15 2009-09-30 Recuperación de peroxido de hidrogeno acuoso en la produccion de h2o2 por autooxidacion
CN101687639B (zh) 2007-04-05 2015-04-29 索尔维公司 水性过氧化氢溶液、它的制备方法及其用途
EP2103604A1 (de) 2008-03-17 2009-09-23 Evonik Degussa GmbH Verfahren zur Herstellung von Epichlorhydrin
EP2149569A1 (de) 2008-08-01 2010-02-03 Hexion Specialty Chemicals Research Belgium S.A. Verfahren zur Herstellung eines 1,2-Epoxid
EP2149570A1 (de) 2008-08-01 2010-02-03 Hexion Specialty Chemicals Research Belgium S.A. Verfahren zur Herstellung von Epichlorhydrin mit Wasserstoffperoxid und einem Mangankomplex
EP2501687B1 (de) 2009-11-19 2014-10-15 Dow Global Technologies LLC Epoxidation eines olefins
EP2343288A1 (de) 2009-11-27 2011-07-13 Momentive Specialty Chemicals Research Belgium S.A. Verfahren zur Herstellung von Propylenoxid
EP2357180A1 (de) 2010-02-02 2011-08-17 Momentive Specialty Chemicals Research Belgium S.A. Herstellung von Epoxyethylethern oder Glycidylethern
EP2354130A1 (de) 2010-02-02 2011-08-10 Momentive Specialty Chemicals Research Belgium Herstellung von Epoxydethylcarboxylat oder Glycidylcarboxylat
EP2354131A1 (de) 2010-02-02 2011-08-10 Momentive Specialty Chemicals Research Belgium Verfahren zur Herstellung von 1,2-Epoxid und Vorrichtung zur Durchführung besagten Verfahrens
RU2588575C2 (ru) * 2010-12-07 2016-07-10 Басф Се Способ получения пропиленоксида
PE20141489A1 (es) * 2011-10-11 2014-10-23 Solvay Proceso para producir peroxido de hidrogeno
EP2719692A1 (de) * 2012-10-09 2014-04-16 Momentive Specialty Chemicals Research Belgium S.A. Katalytischer Epoxidierungsprozess
KR102421905B1 (ko) * 2013-10-02 2022-07-18 솔베이(소시에떼아노님) 정제된 과산화수소 수용액의 제조 방법
US10087158B2 (en) 2015-02-17 2018-10-02 Evonik Degussa Gmbh Method for the epoxidation of an olefin with hydrogen peroxide
EP3059229A1 (de) 2015-02-17 2016-08-24 Evonik Degussa GmbH Verfahren zur Epoxidierung eines Olefins mit Wasserstoffperoxid
TWI707847B (zh) 2015-11-26 2020-10-21 德商贏創運營有限公司 丙烯之環氧化方法
WO2017089074A1 (en) 2015-11-26 2017-06-01 Evonik Degussa Gmbh Process for the epoxidation of an olefin
ES2804208T3 (es) * 2016-01-19 2021-02-04 Evonik Degussa Gmbh Procedimiento para la epoxidación de una olefina
ES2837144T3 (es) 2016-03-21 2021-06-29 Evonik Degussa Gmbh Procedimiento para la epoxidación de propeno
EP3246323A1 (de) 2016-05-17 2017-11-22 Evonik Degussa GmbH Integrierter prozess zur herststellung von propenoxid aus propan
CN106241746A (zh) * 2016-08-18 2016-12-21 黎明化工研究设计院有限责任公司 一种纯化工业过氧化氢溶液的方法
EP3406603A1 (de) 2017-05-22 2018-11-28 Evonik Degussa GmbH Verfahren zur epoxidierung von propen
CN108727226B (zh) * 2018-06-01 2021-02-09 黎明化工研究设计院有限责任公司 一种四丁基脲中二丁胺的去除方法
CN108862205B (zh) * 2018-08-29 2023-09-12 江苏德邦工程有限公司 一种双氧水制备装置
WO2021191134A1 (en) 2020-03-23 2021-09-30 Basf Se H2o2 without dibc for po production

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4999179A (en) * 1988-12-26 1991-03-12 Mitsubishi Gas Chemical Company, Inc. Method for purifying impure aqueous hydrogen peroxide solution
WO2000076989A2 (de) * 1999-06-11 2000-12-21 Basf Aktiengesellschaft Verfahren zur umsetzung organischer verbindungen mit wasserstoffperoxid
US6333018B2 (en) * 1998-01-16 2001-12-25 Ugo Piero Bianchi Process for the industrial production of high purity hydrogen peroxide

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE977130C (de) † 1954-04-28 1965-03-11 Pittsburgh Plate Glass Co Verfahren zur Herstellung von Wasserstoffperoxyd
BE756012A (fr) † 1969-09-10 1971-02-15 Degussa Procede de preparation de peroxyde d'hydrogene (a)
US3949063A (en) † 1971-11-18 1976-04-06 Oxysynthese Regeneration of a anthraquinone working solution by continuous multi-stage thin film distillation
FR2473488A1 (fr) † 1980-01-14 1981-07-17 Oxysynthese Procede cyclique de production de peroxyde d'hydrogene
IT1152299B (it) * 1982-07-28 1986-12-31 Anic Spa Procedimento per l'espossidazione di composti olefinici
JP2800043B2 (ja) * 1988-12-26 1998-09-21 三菱瓦斯化学株式会社 不純過酸化水素水溶液の精製法
GB8925376D0 (en) † 1989-11-09 1989-12-28 Interox Chemicals Ltd Stabilisation of concentrated hydrogen peroxide solutions
DE4013090A1 (de) † 1990-04-25 1991-10-31 Peroxid Chemie Gmbh Verfahren zur herstellung von alkyltetrahydroanthrahydrochinon und diese enthaltende arbeitsloesungen fuer die wasserstoffperoxid-herstellung nach dem anthrachinonverfahren
JP2629507B2 (ja) † 1991-01-14 1997-07-09 住友化学工業株式会社 過酸化水素水の精製方法
DE4107244A1 (de) † 1991-03-07 1992-09-10 Peroxid Chemie Gmbh Verfahren zur reinigung von wasserstoffperoxid fuer die mikroelektronik
US5646314A (en) * 1994-11-16 1997-07-08 Arco Chemical Technology, L.P. Process for titanium silicalite-catalyzed epoxidation
US5670028A (en) † 1994-11-22 1997-09-23 Ube Industries, Ltd. Process for preparing high purity hydrogen peroxide aqueous solution
DE19528219A1 (de) * 1995-08-01 1997-02-06 Degussa Verfahren zur Herstellung von Epoxiden aus Olefinen
JPH10291986A (ja) * 1997-04-18 1998-11-04 Mitsubishi Gas Chem Co Inc オレフィン系炭化水素及びそのハロゲン化物のエポキシ化方法
JP3978546B2 (ja) † 1997-11-07 2007-09-19 三菱瓦斯化学株式会社 高純度過酸化水素水溶液の製造方法
JPH11180704A (ja) † 1997-12-19 1999-07-06 Ube Ind Ltd 高純度過酸化水素水溶液の製造方法
JPH11292521A (ja) * 1998-04-08 1999-10-26 Mitsubishi Gas Chem Co Inc 精製過酸化水素水溶液の製造方法
JP2000302419A (ja) * 1999-04-20 2000-10-31 Mitsubishi Gas Chem Co Inc 精製過酸化水素水溶液の製造方法
IT1313572B1 (it) † 1999-07-27 2002-09-09 Enichem Spa Procedimento per la preparazione di epossidi.
DE19944839A1 (de) * 1999-09-18 2001-03-22 Degussa Verfahren zur Herstellung von Epoxiden aus Olefinen
DE19954055A1 (de) † 1999-11-10 2001-05-17 Basf Ag Vorrichtung und Verfahren zur Entfernung von Salzen aus Wasserstoffperoxid-Lösungen
EP1122249A1 (de) † 2000-02-02 2001-08-08 SOLVAY (Société Anonyme) Verfahren zur Herstellung von Oxyranen
DE10026363A1 (de) † 2000-05-27 2001-11-29 Merck Patent Gmbh Verfahren zur Aufreinigung von Wasserstoffperoxidlösungen
JP4030262B2 (ja) * 2000-06-21 2008-01-09 三徳化学工業株式会社 精製過酸化水素水の製造方法
EP1213262A1 (de) † 2000-12-02 2002-06-12 Degussa AG Verfahren zur Herstellung von höchstkonzentriertem Wasserstoffperoxid und hiermit erhältliches mindestens 99,9 gew.-%iges Wasserstoffperoxid

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4999179A (en) * 1988-12-26 1991-03-12 Mitsubishi Gas Chemical Company, Inc. Method for purifying impure aqueous hydrogen peroxide solution
US6333018B2 (en) * 1998-01-16 2001-12-25 Ugo Piero Bianchi Process for the industrial production of high purity hydrogen peroxide
WO2000076989A2 (de) * 1999-06-11 2000-12-21 Basf Aktiengesellschaft Verfahren zur umsetzung organischer verbindungen mit wasserstoffperoxid

Also Published As

Publication number Publication date
ZA200502512B (en) 2006-03-29
RU2005113688A (ru) 2006-02-27
KR20050057609A (ko) 2005-06-16
PL374703A1 (en) 2005-10-31
KR100990351B1 (ko) 2010-10-29
BR0314941B1 (pt) 2011-11-16
EP1546035B2 (de) 2021-04-21
DE60325616D1 (de) 2009-02-12
ATE419221T1 (de) 2009-01-15
ES2320652T5 (es) 2021-11-22
JP4528625B2 (ja) 2010-08-18
RU2336225C2 (ru) 2008-10-20
CA2500396A1 (en) 2004-04-08
EP1403219A1 (de) 2004-03-31
PL204518B1 (pl) 2010-01-29
EP1546035A1 (de) 2005-06-29
AU2003299090A1 (en) 2004-04-19
WO2004028962A1 (en) 2004-04-08
JP2006501278A (ja) 2006-01-12
CA2500396C (en) 2017-01-24
MY140875A (en) 2010-01-29
BR0314941A (pt) 2005-08-02
EP1546035B1 (de) 2008-12-31
CN1684904A (zh) 2005-10-19
ES2320652T3 (es) 2009-05-27

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SE01 Entry into force of request for substantive examination
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C56 Change in the name or address of the patentee

Owner name: EVONIK DEGUSSA CO., LTD.

Free format text: FORMER NAME: DECOUCHY STOCK COMPANY

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Patentee after: Evonik Degussa GmbH

Address before: Dusseldorf, Germany

Patentee before: Degussa AG

CP01 Change in the name or title of a patent holder

Address after: Essen, Germany

Patentee after: Evonik Operations Ltd.

Address before: Essen, Germany

Patentee before: EVONIK DEGUSSA GmbH

CP01 Change in the name or title of a patent holder
CX01 Expiry of patent term

Granted publication date: 20090422

CX01 Expiry of patent term