CN102665406B - 合成多环胍化合物的方法 - Google Patents
合成多环胍化合物的方法 Download PDFInfo
- Publication number
- CN102665406B CN102665406B CN201080058473.7A CN201080058473A CN102665406B CN 102665406 B CN102665406 B CN 102665406B CN 201080058473 A CN201080058473 A CN 201080058473A CN 102665406 B CN102665406 B CN 102665406B
- Authority
- CN
- China
- Prior art keywords
- guanidine
- certain embodiments
- ring
- bis
- aminopropyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 0 *CCCNCCN Chemical compound *CCCNCCN 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
- C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
- C07D487/04—Ortho-condensed systems
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US29008709P | 2009-12-24 | 2009-12-24 | |
| US61/290,087 | 2009-12-24 | ||
| US29904710P | 2010-01-28 | 2010-01-28 | |
| US61/299,047 | 2010-01-28 | ||
| US42249210P | 2010-12-13 | 2010-12-13 | |
| US61/422,492 | 2010-12-13 | ||
| PCT/US2010/060985 WO2011079041A1 (en) | 2009-12-24 | 2010-12-17 | Methods for the synthesis of polycyclic guanidine compounds |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102665406A CN102665406A (zh) | 2012-09-12 |
| CN102665406B true CN102665406B (zh) | 2016-03-09 |
Family
ID=44196108
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201080058473.7A Active CN102665406B (zh) | 2009-12-24 | 2010-12-17 | 合成多环胍化合物的方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US8642771B2 (2) |
| EP (1) | EP2515648B1 (2) |
| JP (1) | JP5766716B2 (2) |
| KR (1) | KR101885503B1 (2) |
| CN (1) | CN102665406B (2) |
| NO (1) | NO2515648T3 (2) |
| WO (1) | WO2011079041A1 (2) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8334380B2 (en) | 2008-05-09 | 2012-12-18 | Ppg Industries Ohio, Inc. | Method for producing bicyclic guanidines by use of a cyclic urea and a dehydrating agent |
| NO2515648T3 (2) | 2009-12-24 | 2018-01-13 | ||
| US8288504B2 (en) | 2010-03-10 | 2012-10-16 | Ppg Industries Ohio, Inc. | Method of making a cyclic guanidine from dicyandiamide and coating compositions containing same |
| US8148490B2 (en) | 2010-03-10 | 2012-04-03 | Ppg Industries Ohio, Inc. | Method of making a cyclic guanidine from a guanidinium salt and a weak acid and coating compositions containing the same |
| US8563560B2 (en) | 2011-02-25 | 2013-10-22 | Ppg Industries Ohio, Inc. | Preparation of bicyclic guanidine salts in an aqueous media |
| JP6110379B2 (ja) | 2011-07-18 | 2017-04-05 | ノボマー， インコーポレイテッド | 金属錯体 |
| WO2013055747A1 (en) * | 2011-10-10 | 2013-04-18 | Novomer, Inc. | Methods to produce alkylated polycyclic guanidine compounds |
| JP2015514848A (ja) | 2012-04-16 | 2015-05-21 | ノボマー， インコーポレイテッド | 接着剤組成物および方法 |
| US9108968B2 (en) | 2012-04-25 | 2015-08-18 | Ppg Industries Ohio, Inc. | Methods for producing 1,5,7-triazabicyclo[4.4.0]dec-5-ene by reaction of a disubstituted carbodiimide and dipropylene triamine |
| US20130289273A1 (en) * | 2012-04-25 | 2013-10-31 | Ppg Industries Ohio, Inc. | Methods for producing 1,5,7-triazabicyclo[4.4.0]dec-5-ene by reaction of a disubstituted carbodiimide and dipropylene triamine |
| WO2014031811A1 (en) | 2012-08-24 | 2014-02-27 | Novomer, Inc. | Metal complexes |
| JP6169193B2 (ja) * | 2013-01-30 | 2017-07-26 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | ２，６−ビス（アミノメチル）ピペリジン誘導体 |
| US9068089B2 (en) | 2013-03-15 | 2015-06-30 | Ppg Industries Ohio, Inc. | Phenolic admix for electrodepositable coating composition containing a cyclic guanidine |
| CN103172639B (zh) * | 2013-03-18 | 2015-08-12 | 惠州市莱佛士制药技术有限公司 | 一种基于盐酸胍的六元二环胍的制备方法 |
| US9688874B2 (en) | 2013-10-25 | 2017-06-27 | Ppg Industries Ohio, Inc. | Method of making a bicyclic guanidine-cured acrylic coating |
| CN103539798A (zh) * | 2013-11-12 | 2014-01-29 | 南京大学 | 一种双环胍（1,5,7-三氮杂双环[5.5.0]癸-5-烯）的合成方法 |
| CN103755598A (zh) * | 2014-01-23 | 2014-04-30 | 上海旭新化工科技有限公司 | 胍丁胺硫酸盐的合成方法 |
| CN104844608B (zh) * | 2015-04-13 | 2017-09-19 | 南京大学 | 相转移催化法合成双环胍tbd的工艺方法 |
| CN110121548A (zh) * | 2017-01-03 | 2019-08-13 | 陈煌兴 | 支化聚合双胍化合物及其用途 |
| CN107325102B (zh) * | 2017-08-11 | 2019-11-12 | 南京大学 | 自催化双亲混合溶剂中合成1,5,7-三氮杂双环[4.4.0]癸-5-烯的工艺方法 |
| FI129024B (en) | 2017-11-08 | 2021-05-14 | Helsingin Yliopisto | Process for the preparation of bicyclic guanidine and its derivatives |
| WO2019126221A1 (en) | 2017-12-22 | 2019-06-27 | Saudi Aramco Technologies Company | Catalysts for polycarbonate production |
| EP3774807B1 (de) | 2018-09-06 | 2021-09-01 | Wacker Chemie AG | Verfahren zur herstellung bicyclischer guanidine |
| CN114585626B (zh) * | 2019-10-22 | 2024-06-25 | 巴斯夫欧洲公司 | 生产环状胍衍生物的方法 |
| CN112094273A (zh) * | 2020-08-07 | 2020-12-18 | 天津全和诚科技有限责任公司 | 一种的双环胍的合成方法 |
| CN112961343B (zh) * | 2021-02-19 | 2023-08-29 | 上海凯赛生物技术股份有限公司 | 一种戊二胺磷酸胍盐齐聚物、其制备方法及由其制得的抗菌聚合物 |
| CN121752569A (zh) | 2023-08-25 | 2026-03-27 | 赢创运营有限公司 | 制造双环胍的方法 |
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| US2473111A (en) * | 1949-06-14 | Process for production of z-amino | ||
| US3873266A (en) * | 1971-03-19 | 1975-03-25 | Sandoz Ag | Solutions of polyalkylene polyamine-cyanamide condensation products |
| JPS585904B2 (ja) | 1977-04-05 | 1983-02-02 | 三井東圧化学株式会社 | グアニジン及びその塩類の製造方法 |
| GB2070006B (en) | 1980-02-22 | 1984-05-02 | Sandoz Ltd | Amine condencates useful in textile treatment |
| FR2509724B1 (fr) * | 1981-07-15 | 1985-10-25 | Centre Nat Rech Scient | Nouvelles guanidines a fort encombrement sterique et procedes pour leur preparation |
| GB8509531D0 (en) * | 1985-04-13 | 1985-05-15 | Bp Chem Int Ltd | Preparation of guanidines |
| US5101041A (en) * | 1989-04-26 | 1992-03-31 | The Curators Of The University Of Missouri | Triamines and their derivatives as bifunctional chelating agents |
| US5637739A (en) | 1990-03-21 | 1997-06-10 | Research Corporation Technologies, Inc. | Chiral catalysts and catalytic epoxidation catalyzed thereby |
| JPH09505591A (ja) * | 1993-11-23 | 1997-06-03 | ケンブリッジ・ニューロサイエンス・インコーポレーテッド | 治療用置換グアニジン類 |
| US5659011A (en) * | 1994-09-23 | 1997-08-19 | Waldmann; John J. | Agents having high nitrogen content and high cationic charge based on dicyanimide dicyandiamide or guanidine and inorganic ammonium salts |
| US5665890A (en) | 1995-03-14 | 1997-09-09 | President And Fellows Of Harvard College | Stereoselective ring opening reactions |
| AU3813997A (en) | 1996-07-26 | 1998-02-20 | Princeton University | Catalytic oxygenation of hydrocarbons by metalloporphyrin and metallosalen complexes |
| TW420693B (en) | 1997-04-25 | 2001-02-01 | Mitsui Chemicals Inc | Olefin polymerization catalysts, transition metal compounds, and <alpha>-olefin/conjugated diene copolymers |
| US6130340A (en) | 1998-01-13 | 2000-10-10 | President And Fellows Of Harvard College | Asymmetric cycloaddition reactions |
| US6521561B1 (en) | 1998-05-01 | 2003-02-18 | President And Fellows Of Harvard College | Main-group metal based asymmetric catalysts and applications thereof |
| KR100342659B1 (en) | 2000-12-15 | 2002-07-04 | Rstech Co Ltd | Chiral polymer salene catalyst and process for preparing chiral compounds from racemic epoxide using the same |
| JP3968076B2 (ja) | 2001-06-27 | 2007-08-29 | アールエス テック コーポレイション | 新しいキラルサレン化合物、キラルサレン触媒及びこれを利用したラセミックエポキシ化合物からキラル化合物を製造する方法 |
| US6639087B2 (en) | 2001-08-22 | 2003-10-28 | Rhodia Pharma Solutions Inc. | Kinetic resolution method |
| DE10235316A1 (de) | 2002-08-01 | 2004-02-12 | Basf Ag | Katalysator und Verfahren zur Carbonylierung von Oxiranen |
| EP1663993B1 (de) | 2003-09-05 | 2008-03-12 | Actelion Pharmaceuticals Ltd. | Guanidinderivate |
| KR100724550B1 (ko) | 2004-12-16 | 2007-06-04 | 주식회사 엘지화학 | 이중 금속 아연 착화합물과 이를 촉매로 사용한폴리카보네이트의 제조 방법 |
| WO2006099162A2 (en) | 2005-03-14 | 2006-09-21 | Georgia Tech Research Corporation | Polymeric salen compounds and methods thereof |
| US8232267B2 (en) | 2006-10-06 | 2012-07-31 | The Trustees Of Princeton University | Porphyrin catalysts and methods of use thereof |
| GB0708016D0 (en) | 2007-04-25 | 2007-06-06 | Univ Newcastle | Synthesis of cyclic carbonates |
| EP2573126B1 (en) | 2007-05-04 | 2014-09-24 | SK Innovation Co. Ltd. | A process for producing polycarbonates and a coordination complex used therefor |
| WO2008150033A1 (ja) | 2007-06-08 | 2008-12-11 | The University Of Tokyo | エポキシドと二酸化炭素との立体選択的交互共重合 |
| EP2096132A1 (en) | 2008-02-26 | 2009-09-02 | Total Petrochemicals Research Feluy | Monomers issued from renewable resources and process for polymerising them |
| US20110015409A1 (en) | 2008-03-07 | 2011-01-20 | University Of Newcastle Upon Tyne | Synthesis of cyclic carbonates |
| US8039618B2 (en) | 2008-05-09 | 2011-10-18 | Ppg Industries Ohio, Inc. | Method for producing bicyclic guanidines by use of a cyclic urea |
| US8334380B2 (en) | 2008-05-09 | 2012-12-18 | Ppg Industries Ohio, Inc. | Method for producing bicyclic guanidines by use of a cyclic urea and a dehydrating agent |
| CA2727959A1 (en) | 2008-07-30 | 2010-02-04 | Sk Energy, Co., Ltd. | Novel coordination complexes and process of producing polycarbonate by copolymerization of carbon dioxide and epoxide using the same as catalyst |
| CA2639870A1 (en) | 2008-09-29 | 2010-03-29 | Nova Chemicals Corporation | Trimerization |
| NO2515648T3 (2) | 2009-12-24 | 2018-01-13 | ||
| KR101503745B1 (ko) | 2010-02-25 | 2015-03-19 | 에스케이이노베이션 주식회사 | 나이트레이트 음이온의 이산화탄소/에폭사이드 공중합 촉매 시스템 |
| US8148490B2 (en) | 2010-03-10 | 2012-04-03 | Ppg Industries Ohio, Inc. | Method of making a cyclic guanidine from a guanidinium salt and a weak acid and coating compositions containing the same |
| US8288504B2 (en) | 2010-03-10 | 2012-10-16 | Ppg Industries Ohio, Inc. | Method of making a cyclic guanidine from dicyandiamide and coating compositions containing same |
| US8563560B2 (en) | 2011-02-25 | 2013-10-22 | Ppg Industries Ohio, Inc. | Preparation of bicyclic guanidine salts in an aqueous media |
| GB201115565D0 (en) | 2011-09-08 | 2011-10-26 | Imp Innovations Ltd | Method of synthesising polycarbonates in the presence of a bimetallic catalyst and a chain transfer agent |
-
2010
- 2010-12-17 NO NO10840015A patent/NO2515648T3/no unknown
- 2010-12-17 CN CN201080058473.7A patent/CN102665406B/zh active Active
- 2010-12-17 US US13/515,634 patent/US8642771B2/en active Active
- 2010-12-17 JP JP2012546076A patent/JP5766716B2/ja active Active
- 2010-12-17 WO PCT/US2010/060985 patent/WO2011079041A1/en not_active Ceased
- 2010-12-17 KR KR1020127019400A patent/KR101885503B1/ko active Active
- 2010-12-17 EP EP10840015.1A patent/EP2515648B1/en active Active
-
2014
- 2014-01-06 US US14/148,455 patent/US9738647B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN102665406A (zh) | 2012-09-12 |
| JP5766716B2 (ja) | 2015-08-19 |
| US20120259112A1 (en) | 2012-10-11 |
| KR20120124419A (ko) | 2012-11-13 |
| EP2515648B1 (en) | 2017-08-16 |
| US20140194622A1 (en) | 2014-07-10 |
| US9738647B2 (en) | 2017-08-22 |
| WO2011079041A1 (en) | 2011-06-30 |
| NO2515648T3 (2) | 2018-01-13 |
| EP2515648A1 (en) | 2012-10-31 |
| KR101885503B1 (ko) | 2018-08-07 |
| US8642771B2 (en) | 2014-02-04 |
| JP2013515728A (ja) | 2013-05-09 |
| EP2515648A4 (en) | 2014-08-27 |
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Legal Events
| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171229 Address after: Saudi Aramco Patentee after: Saudi Aram technology company Address before: American New York Patentee before: Novomer Inc. |