CN102952425A - Water-based printing ink cleaning agent and preparation method thereof - Google Patents
Water-based printing ink cleaning agent and preparation method thereof Download PDFInfo
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- CN102952425A CN102952425A CN2012104672297A CN201210467229A CN102952425A CN 102952425 A CN102952425 A CN 102952425A CN 2012104672297 A CN2012104672297 A CN 2012104672297A CN 201210467229 A CN201210467229 A CN 201210467229A CN 102952425 A CN102952425 A CN 102952425A
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000012459 cleaning agent Substances 0.000 title abstract description 7
- 238000005260 corrosion Methods 0.000 claims abstract description 12
- 230000007797 corrosion Effects 0.000 claims abstract description 12
- 229910052751 metal Inorganic materials 0.000 claims abstract description 11
- 239000002184 metal Substances 0.000 claims abstract description 11
- 239000003112 inhibitor Substances 0.000 claims abstract description 9
- 239000003599 detergent Substances 0.000 claims description 32
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 239000003795 chemical substances by application Substances 0.000 claims description 12
- 239000013543 active substance Substances 0.000 claims description 10
- 239000012466 permeate Substances 0.000 claims description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 8
- 239000004202 carbamide Substances 0.000 claims description 8
- RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 claims description 7
- RGHNJXZEOKUKBD-SQOUGZDYSA-N Gluconic acid Natural products OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 claims description 7
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 7
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 claims description 7
- 239000012964 benzotriazole Substances 0.000 claims description 7
- 239000000174 gluconic acid Substances 0.000 claims description 7
- 235000012208 gluconic acid Nutrition 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 7
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 7
- 229960004418 trolamine Drugs 0.000 claims description 7
- 235000019353 potassium silicate Nutrition 0.000 claims description 6
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 6
- 235000010234 sodium benzoate Nutrition 0.000 claims description 6
- 239000004299 sodium benzoate Substances 0.000 claims description 6
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 6
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 4
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 4
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 4
- 235000017550 sodium carbonate Nutrition 0.000 claims description 4
- 229910019142 PO4 Inorganic materials 0.000 claims description 3
- 229920002125 Sokalan® Polymers 0.000 claims description 3
- 238000005352 clarification Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 239000010452 phosphate Substances 0.000 claims description 3
- 239000004584 polyacrylic acid Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 4
- 239000004094 surface-active agent Substances 0.000 abstract description 2
- 239000006184 cosolvent Substances 0.000 abstract 1
- 230000007547 defect Effects 0.000 abstract 1
- 238000011086 high cleaning Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 8
- 239000000203 mixture Substances 0.000 description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 239000003960 organic solvent Substances 0.000 description 4
- ONJQDTZCDSESIW-UHFFFAOYSA-N polidocanol Chemical compound CCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO ONJQDTZCDSESIW-UHFFFAOYSA-N 0.000 description 4
- 230000007613 environmental effect Effects 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 239000004411 aluminium Substances 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- 229910000975 Carbon steel Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000010962 carbon steel Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- BEGBSFPALGFMJI-UHFFFAOYSA-N ethene;sodium Chemical group [Na].C=C BEGBSFPALGFMJI-UHFFFAOYSA-N 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000003502 gasoline Substances 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000003350 kerosene Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- -1 phosphate ester salt Chemical class 0.000 description 1
- 239000011814 protection agent Substances 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
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- Detergent Compositions (AREA)
Abstract
本发明为克服现有产品清洗效果不理想以及性能不稳定的缺陷，提供一种清洗效率高、体系稳定性好、无腐蚀作用、使用安全的水基印刷油墨清洗剂及其制备方法。本发明的水基印刷油墨清洗剂由以下质量百分比的组份配制而成：表面活性剂6%~15%；碱性无机物0.5~5%；助溶剂1~5%；渗透剂1%~5%；金属防蚀剂0.3%~3%；余量为水。
In order to overcome the defects of unsatisfactory cleaning effect and unstable performance of existing products, the invention provides a water-based printing ink cleaning agent with high cleaning efficiency, good system stability, no corrosion, and safe use and a preparation method thereof. The water-based printing ink cleaning agent of the present invention is prepared from the following components in mass percentage: surfactant 6%~15%; alkaline inorganic substance 0.5%~5%; cosolvent 1~5%; penetrant 1%~ 5%; metal corrosion inhibitor 0.3%~3%; the balance is water.
Description
Technical field:
The present invention relates to a kind of detergent for ink for printing-ink on cleaning printing press tool, press plate, ink roller and the blanket.In particular, be a kind of detergent for water-based print ink and preparation method thereof.
Background technology:
In printing process, it is the important leverage of producing the high quality printing product that residual ink dirt on the printing equipment is effectively cleaned.The fast development of producing along with China printed matter is also continuing to increase the demand of the detergent for ink of cleaning of graphic arts equipment.
In the detergent for ink of selling on the domestic market, traditional clean-out system is made host with organic solvents such as gasoline, kerosene, and organic solvent content is very high, at machine room's high volatility, the severe contamination printing environment, and the harm worker is healthy, production cost is higher simultaneously.Half aq. type printing ink washing agent has reduced the content of organic solvent, but not yet fundamentally solves the environmental problem that the volatile gases discharging causes; Simultaneously, the easy breakdown of emulsion of this class clean-out system, unstable properties.The aq. type printing ink washing agent replaces organic solvent with tensio-active agent, produces and the equal non-volatility gas purging of use procedure environmental protection; Do not fire fully, use safety; Water content is large, and production cost is low.
In present stage, domestic commercially available detergent for water-based print ink effect is all unsatisfactory, and the water-base ink cleaning agent that effect is good mainly relies on external import, and expensive.In order to reduce enterprise's production cost, from the angle of protection of the environment, save energy, independent research production cleaning performance detergent for water-based print ink good, low production cost seems very necessary, and potential market is wide.
At present, the detergent for water-based print ink of domestic development is many to be formed by surfactant compound, or with highly basic black dirt is removed, but still there is a lot of drawbacks in the product that this several method is produced, undesirable such as effect, have a toxic ingredient, unstable properties, to shortcomings such as equipment corrosions.Provide a kind of water-base ink cleaning agent take ester and organic acid as main component such as the CN02102265.8 patent, the common existence of ester class and acids can cause its unstable properties in this clean-out system, and there are etching problem in carbon steel, Al-alloy metal printing equipment; CN200710177421.1 and CN200810122550.5 patent provide a kind of water-base ink cleaning agent; its effective constituent all is tensio-active agent; although performance is gentle; corrosion rate to equipment is low; but cleaning performance is undesirable, and the CN201010100923.6 patent application provides a kind of water-base ink cleaning agent, and this cleans composite and various solubility promoter, permeate agent and the metal protection agent and the water that adopt phosphate ester salt and consists of; its cleaning performance is good, but larger to the corrodibility of aluminium.
Goal of the invention:
Main purpose of the present invention is, overcomes the defective of the undesirable and unstable properties of currently available products cleaning performance, provide that a kind of cleaning efficiency is high, system stability is good, without corrosive nature, use the detergent for water-based print ink of safety.
Another object of the present invention provides the preparation method of above-mentioned detergent for water-based print ink.
A kind of detergent for water-based print ink, it is formulated by the component of following mass percent:
Tensio-active agent 6% ~ 15%
Alkalescence inorganics 0.5 ~ 5%
Solubility promoter 1 ~ 5%
Permeate agent 1% ~ 5%
Corrosion inhibitor for metal 0.3% ~ 3%
Water surplus.
Tensio-active agent in the component is selected one or both any mixing of fatty alcohol-polyoxyethylene ether (such as AEO-9) or fatty alcohol-ether phosphate kalium salt (such as MOA-3PK).
Alkaline inorganics yellow soda ash in the component is selected one or more any mixing in water glass, sodium hydroxide or the disodium ethylene diamine tetraacetate.
Solubility promoter in the component is selected one or more any mixing in gluconic acid, polyacrylic acid, the urea.
Permeate agent in the component is selected one or more any mixing in fatty alcohol-polyoxyethylene ether or the trolamine.
Corrosion inhibitor for metal in the component is selected one or more any mixing in Sodium Benzoate, vulkacit H or the benzotriazole.
The preparation method of above-mentioned detergent for water-based print ink, take by weighing each component in above ratio, at normal temperatures, first tensio-active agent, alkaline inorganics, solubility promoter are added to the water, fully stir, each component is dissolved fully after, add again permeate agent, corrosion inhibitor for metal etc., be stirred to transparent clarification, the uniform liquid that obtains is detergent for water-based print ink.
The present invention has following beneficial effect compared to existing technology:
The scientific formulation of detergent for water-based print ink of the present invention is reasonable, and raw material sources are extensive, and production cost is lower; Compare with domestic similar detergent for water-based print ink, cleansing power, product stability and aspect the corrodibility of hardware, very large change has been arranged; Have no irritating odor, safe and reliable, be a kind of printing ink washing agent of environmental protection.
Preparation method's production technique of the present invention and equipment are simple, are fit to mass industrialized production.
Description of drawings:
Fig. 1 is the aluminium flake outside drawing of (not inking) before cleaning.
Fig. 2 is the aluminium flake outside drawing of (being coated with curing ink) before cleaning.
Fig. 3 is the aluminium flake outside drawing of Fig. 2 after product of the present invention cleans.
Fig. 4 is that product of the present invention prepares the stoste view.
Fig. 5 is for preparing the view after stoste is placed month to product of the present invention.
Among the figure, the product that adopts the embodiment of the invention 1 to make among Fig. 3 cleans.Cleaning way adopts cloth to dip detergent solution press plate is cleaned.
Can be drawn by Fig. 1, Fig. 2, Fig. 3 contrast, product of the present invention is strong to the printing ink cleansing power, and cleaning performance is good, simultaneously to aluminium also without corrosive nature.
Can be drawn by Fig. 4, Fig. 5, detergent for water-based print ink stable system of the present invention can long storage time.
Embodiment:
Raw material used in the present invention is the commercial goods, below in conjunction with specific examples, further sets forth the present invention.
Embodiment 1
Detergent for water-based print ink in this example is to be mixed by the composition in the following table.
Table 1
| Component | Per-cent |
| AEO-9 | 8% |
| Sodium hydroxide | 1.5% |
| Urea | 2% |
| Trolamine | 1% |
| Benzotriazole | 1.5% |
| Water | 86% |
Take by weighing each component in upper table ratio, under normal temperature condition, first tensio-active agent, alkaline inorganics, solubility promoter are added to the water, fully stir until completely dissolved, add again permeate agent, corrosion inhibitor for metal, be stirred to transparent clarification, the uniform liquid that obtains is detergent for water-based print ink of the present invention.
Embodiment 2
Detergent for water-based print ink in this example is to be mixed by the composition in the following table.
Table 2
| Component | Per-cent |
| AEO-9 | 10% |
| Water glass | 2% |
| Urea | 2% |
| Gluconic acid | 0.5% |
| Trolamine | 1% |
| Sodium Benzoate | 1% |
| Vulkacit H | 0.5% |
| Water | 83% |
The preparation method is identical with example 1.
Embodiment 3
Detergent for water-based print ink in this example is to be mixed by the composition in the following table.
Table 3
| Component | Per-cent |
| MOA-3PK | 6% |
| AEO-9 | 6% |
| Sodium ethylene diamine tetracetate | 2% |
| Yellow soda ash | 1% |
| Urea | 2% |
| Fatty alcohol-polyoxyethylene ether | 1% |
| Sodium Benzoate | 1% |
| Benzotriazole | 0.5% |
| Water | 80.5% |
The preparation method is identical with example 1.
Embodiment 4
Detergent for water-based print ink in this example is to be mixed by the composition in the following table.
Table 4
| Component | Per-cent |
| MOA-3PK | 6% |
| Water glass | 5% |
| Urea | 2% |
| Gluconic acid | 3% |
| Trolamine | 5% |
| Benzotriazole | 3% |
| Water | 76% |
The preparation method is identical with example 1.
Embodiment 5
Detergent for water-based print ink in this example is to be mixed by the composition in the following table.
Table 5
| Component | Per-cent |
| MOA-3PK | 13% |
| Water glass | 1% |
| Sodium hydroxide | 1% |
| Disodium ethylene diamine tetraacetate | 2% |
| Gluconic acid | 1% |
| Urea | 2% |
| Gluconic acid | 3% |
| Trolamine | 5% |
| Sodium Benzoate | 2% |
| Benzotriazole | 3% |
| Water | 67% |
The preparation method is identical with example 1.
Claims (8)
1. detergent for water-based print ink, it is characterized in that: it is formulated by the component of following mass percent:
Tensio-active agent 6% ~ 15%
Alkalescence inorganics 0.5 ~ 5%
Solubility promoter 1 ~ 5%
Permeate agent 1% ~ 5%
Corrosion inhibitor for metal 0.3% ~ 3%
Water surplus.
2. the technical recipe of detergent for water-based print ink according to claim 1 is characterized in that: the tensio-active agent in the component select fatty alcohol-polyoxyethylene ether or one or both mixing.
3. the technical recipe of detergent for water-based print ink according to claim 1, it is characterized in that: the alkaline inorganics yellow soda ash in the component is selected one or more in water glass, sodium hydroxide or the disodium ethylene diamine tetraacetate.
4. the technical recipe of detergent for water-based print ink according to claim 1, it is characterized in that: the solubility promoter in the component is selected one or more in gluconic acid, polyacrylic acid, the urea.
5. the technical recipe of detergent for water-based print ink according to claim 1, it is characterized in that: the permeate agent in the component is selected one or more in fatty alcohol-polyoxyethylene ether or the trolamine.
6. according to claim 1, the technical recipe of 2,3,4 or 5 described detergent for water-based print ink, it is characterized in that: the corrosion inhibitor for metal in the component is selected one or more in Sodium Benzoate, vulkacit H or the benzotriazole.
7. the preparation method of the described detergent for water-based print ink of claim 1, it is characterized in that: take by weighing each component in above ratio, at normal temperatures, first tensio-active agent, alkaline inorganics, solubility promoter are added to the water, fully stir, each component is dissolved fully after, add again permeate agent, corrosion inhibitor for metal etc., be stirred to transparent clarification, the uniform liquid that obtains is detergent for water-based print ink.
8. the preparation method of detergent for water-based print ink according to claim 7 is characterized in that: described tensio-active agent is selected one or both the mixing in fatty alcohol-polyoxyethylene ether or the fatty alcohol-ether phosphate kalium salt; Described alkaline inorganics yellow soda ash is selected one or more in water glass, sodium hydroxide or the disodium ethylene diamine tetraacetate; Described solubility promoter is selected one or more in gluconic acid, polyacrylic acid, the urea; Described permeate agent is selected one or more in fatty alcohol-polyoxyethylene ether or the trolamine; Described corrosion inhibitor for metal is selected one or more in Sodium Benzoate, vulkacit H or the benzotriazole.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2012104672297A CN102952425A (en) | 2012-11-19 | 2012-11-19 | Water-based printing ink cleaning agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104672297A CN102952425A (en) | 2012-11-19 | 2012-11-19 | Water-based printing ink cleaning agent and preparation method thereof |
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| CN103214898A (en) * | 2013-04-26 | 2013-07-24 | 南京信息工程大学 | Water-based printing ink cleaning agent and preparation method thereof |
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Application publication date: 20130306 |