CN102995403B - The method solidifying high-performance chitosan on fabric - Google Patents
The method solidifying high-performance chitosan on fabric Download PDFInfo
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- CN102995403B CN102995403B CN201210525242.3A CN201210525242A CN102995403B CN 102995403 B CN102995403 B CN 102995403B CN 201210525242 A CN201210525242 A CN 201210525242A CN 102995403 B CN102995403 B CN 102995403B
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- fabric
- chitosan
- pseudobulbus bletillae
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- bletillae polysaccharose
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- 229920001661 Chitosan Polymers 0.000 title claims abstract description 60
- 239000004744 fabric Substances 0.000 title claims abstract description 41
- 238000000034 method Methods 0.000 title claims abstract description 19
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 230000000844 anti-bacterial effect Effects 0.000 claims abstract description 15
- 238000003756 stirring Methods 0.000 claims abstract description 10
- 238000007711 solidification Methods 0.000 claims abstract description 6
- 230000008023 solidification Effects 0.000 claims abstract description 6
- -1 polyhexamethylene guanidine Polymers 0.000 claims description 5
- 238000002386 leaching Methods 0.000 claims 1
- 239000002068 microbial inoculum Substances 0.000 claims 1
- 230000000845 anti-microbial effect Effects 0.000 abstract description 2
- 229920002101 Chitin Polymers 0.000 description 10
- 239000000835 fiber Substances 0.000 description 9
- 230000036541 health Effects 0.000 description 7
- 238000005406 washing Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 150000004676 glycans Chemical class 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 229920001282 polysaccharide Polymers 0.000 description 3
- 239000005017 polysaccharide Substances 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- ZRALSGWEFCBTJO-UHFFFAOYSA-N Guanidine Chemical compound NC(N)=N ZRALSGWEFCBTJO-UHFFFAOYSA-N 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000003053 immunization Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 241000371997 Eriocheir sinensis Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- CHJJGSNFBQVOTG-UHFFFAOYSA-N N-methyl-guanidine Natural products CNC(N)=N CHJJGSNFBQVOTG-UHFFFAOYSA-N 0.000 description 1
- 241000238040 Panulirus Species 0.000 description 1
- 241000927735 Penaeus Species 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 230000001413 cellular effect Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 230000006196 deacetylation Effects 0.000 description 1
- 238000003381 deacetylation reaction Methods 0.000 description 1
- 239000002781 deodorant agent Substances 0.000 description 1
- SWSQBOPZIKWTGO-UHFFFAOYSA-N dimethylaminoamidine Natural products CN(C)C(N)=N SWSQBOPZIKWTGO-UHFFFAOYSA-N 0.000 description 1
- 238000003618 dip coating Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000036449 good health Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000002649 immunization Methods 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 210000002751 lymph Anatomy 0.000 description 1
- 239000006247 magnetic powder Substances 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000000392 somatic effect Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of method solidifying high-performance chitosan on fabric, under room temperature, water, granular water soluble chitosan and antimicrobial granular agent are mixed, and stir, make high-performance chitosan finishing agent, the concentration of chitosan is 1～3%, and the concentration of antibacterial is 1～2%；Being put into by fabric in high-performance chitosan finishing agent and arrange, high-performance chitosan finishing agent is 2: 1 with the weight ratio of fabric, is dehydrated, dries after arrangement；Under room temperature, water and granular water soluble Pseudobulbus Bletillae polysaccharose are mixed and stirred for uniformly, make Pseudobulbus Bletillae polysaccharose solution, the concentration of Pseudobulbus Bletillae polysaccharose solution is 0.5～1.5%, the fabric arranged, dry is put in Pseudobulbus Bletillae polysaccharose solution and solidifies, Pseudobulbus Bletillae polysaccharose solution is 4: 1 with the weight ratio of fabric, is dehydrated, dries after solidification.The method solidifying high-performance chitosan on fabric, technique is simple, flexible, and low cost is effectively improved the antibacterial durability of fabric and washability.
Description
Technical field
The invention belongs to fabric-handling techniques field, be specifically related to one high-performance chitosan finish fabric, and make
High-performance chitosan is solidificated in the method on fabric, makes fabric have health care.
Background technology
Along with the development and progress of society, and improving constantly of people's living standard is increased the weight of day by day with environmental pollution,
The consciousness of own health is gradually strengthened by people, and up to the present, the theory of health care has been not only stop
Stressing pollution-free food, balanced in nutrition and eat the aspects such as health product, people are to passing the consciousness of health the most increasingly
Strongly, therefore, occurring in that the product such as " magnetic force fiber sock ", " Taka Magnetotherapeutic pants " in recent years, these products are adopted
Be physical technique, magnetic force fiber sock is that magnetic powder etc. combines polypropylene fiber and processes, and price is higher, it is difficult to shape
Seriation on a large scale.
Chitin is the animality high molecular cellulose that application gene engineering is extracted from Eriocheir sinensis, Crusta Penaeus seu Panulirus, shell
Polysaccharide is again chitosan, chitosan, deacetylation chitin and chitin etc..1996.12.21 it is " healthy
Report " once reported " chitosan-very important " vital principle " ", report chitosan be sugar,
After protein, fat, vitamin and mineral, the human body the obligato 6th that scientists is recognized
Vital principle, has the effect of enhancing body cellular immunization, and scientist also demonstrates that, chitosan can be dissolved in stomach
Acid, may be present in the blood of people, lymph, each internal organs and skeleton, have human body affinity, bactericidal properties and
Row cholesterol, chloride ion, heavy metal performance, and block cancerous cell, the somatic function of activation equipment.
Biological activity that chitosan is had and safety, increasingly obtain the accreditation of people, and its application is the most increasingly
Extensively.According to " China Textile News ", chitin fiber is natural possesses five functional: nontoxic, mildew-resistant, anti-
Bacterium, fire-retardant, antistatic, in textile garment field, chitin fiber moisture absorbing and sweat releasing, antistatic, bacteria mildew-proof etc.
Functional so that it is to be particularly suitable for making bedding, underwear, socks, towel etc. and directly contact the product of skin.20
At the initial stage nineties in century, Japan utilizes the characteristic of chitin fiber at first, makes and in the antibacterial deodourizing class of cotton blending
Clothing and panty hose, favored by consumers.1999～2000, Donghua University developed chitin series and has mixed
Yarn and fabric also make various health care underwear, panty hose and articles for babies.
Chitin fiber directly contacts skin and has good health care, antibacterial action, but chitin fiber is harder,
Its comfort level is poor, and additionally chitin fiber spinnability is poor, and expensive, and the method for there is no meets popular needs.Cause
This, many producers, by directly fabric being padded Final finishing with degradation of chitosan liquid, obtain the fabric that keeps healthy, but
The pull-out capacity being degradation of chitosan liquid is low, poor durability, and additionally manufacturing process flow is complicated, adds manufacturing cost.
Summary of the invention
For the above-mentioned technical problem overcoming prior art to exist, it is an object of the invention to, it is provided that Yi Zhong
The method solidifying high-performance chitosan on fabric, technique is simple, low cost, improves the antibacterial durability of fabric and washable
Property.
The method solidifying high-performance chitosan on fabric that the present invention provides, comprises the following steps:
One, allotment high-performance chitosan finishing agent: at normal temperatures, by water, granular water soluble chitosan and granule
Shape antibacterial mixes, and stirs, and makes high-performance chitosan finishing agent；Wherein, antibacterial is poly-six methylenes
Base guanidine, the concentration of chitosan is 1～3%, and the concentration of antibacterial is 1～2%；
Two, high-performance chitosan arranges: the high-performance chitosan finishing agent deployed by step one soaks, arranges and knit
Thing, high-performance chitosan finishing agent is 2: 1 with the weight ratio of fabric, fabric is first put into high-performance chitosan and arranges
Agent is stirred 20 minutes, then soaks 30 minutes, be dehydrated afterwards, dry；
Three, allotment Pseudobulbus Bletillae polysaccharose solution: at normal temperatures, mixes water and granular water soluble Pseudobulbus Bletillae polysaccharose, and stirs
Mixing uniformly, make Pseudobulbus Bletillae polysaccharose solution, the concentration of Pseudobulbus Bletillae polysaccharose is 0.5～1.5%；
Four, Pseudobulbus Bletillae polysaccharose solidification: fabric step 2 put in order puts into the Pseudobulbus Bletillae polysaccharose solution that step 3 is deployed
Soaking, solidify, Pseudobulbus Bletillae polysaccharose solution is 4: 1 with the weight ratio of fabric, fabric is first put into Pseudobulbus Bletillae polysaccharose solution and stirs
Mix 10 minutes, then soak 30 minutes, be dehydrated afterwards, dry.
The method solidifying high-performance chitosan on fabric that the present invention provides, it has the beneficial effects that, uses granule
Shape water-soluble chitosan and the high-performance chitosan finishing agent of antimicrobial granular agent mixed preparing, arrange fabric,
Enhance the functional of chitosan, on fabric after film forming, improve the quality of fabric, give fabric and have antibacterial
Antiinflammatory, ultraviolet radiation preventing, reduction content of formaldehyde, suppression skin pruritus, suppression inflammation, skin-friendly be good,
Deodorant and the effect of absorption abnormal flavour, up to more than 96% in antibacterial bacteriostatic rate；Fabric solidifies high-performance shell gather
The method of sugar, technique is simple, maneuverability, low cost, through the fabric peace that high-performance chitosan finishing agent arranged
Atoxic, immunizing health；After Pseudobulbus Bletillae polysaccharose is solution cured, biological polyoses pull-out capacity is strong, is effectively increased fabric
Antibacterial durability and washability.
Detailed description of the invention
Below in conjunction with two embodiments, the method solidifying high-performance chitosan on fabric providing the present invention is carried out
Detailed description.
Embodiment one
The present embodiment solidifies the method for high-performance chitosan on fabric, arranges finished product towel, including following
Step:
One, allotment high-performance chitosan finishing agent: at normal temperatures, by water, granular water soluble chitosan and granule
Shape polyhexamethylene guanidine is put into industrial washing machine and is mixed, and the concentration of chitosan is 2%, polyhexamethylene guanidine
Concentration is 1%, and positive and negative rotation is stirred 30 minutes, makes high-performance chitosan finishing agent；
Two, high-performance chitosan arranges: towel is put into the deployed high-performance chitosan finishing agent of step one soak,
Arranging, high-performance chitosan finishing agent is 2: 1 with the weight ratio of towel, first towel is put into high-performance chitosan whole
In reason agent, positive and negative rotation is stirred 20 minutes, then soaks 30 minutes, is dehydrated afterwards, dries；
Three, allotment Pseudobulbus Bletillae polysaccharose solution: at normal temperatures, water and granular water soluble Pseudobulbus Bletillae polysaccharose are put into industrial
Mixing in washing machine, the concentration of Pseudobulbus Bletillae polysaccharose is 0.5%, and positive and negative rotation is stirred 20 minutes, makes Pseudobulbus Bletillae polysaccharose molten
Liquid；
Four, Pseudobulbus Bletillae polysaccharose solidification: the towel that step 2 is dried is put in the Pseudobulbus Bletillae polysaccharose solution that step 3 is deployed
Soaking, solidify, Pseudobulbus Bletillae polysaccharose solution is 4: 1 with the weight ratio of towel, first towel is being put into Pseudobulbus Bletillae polysaccharose solution just
Reverse turn stirs 10 minutes, then soaks 30 minutes, is dehydrated afterwards, dries.
Embodiment two
One, allotment high-performance chitosan finishing agent: at normal temperatures, by water-soluble to 100 kg of water, 1500 grams of graininess
Property chitosan and 1000 grams of graininess polyhexamethylene guanidines are put into industrial washing machine simultaneously and are mixed, and rotating
Dynamic stirring 30 minutes, makes high-performance chitosan finishing agent；
Two, high-performance chitosan arranges: 50 kilograms of towels are put into the deployed high-performance chitosan of step one and arranges
Agent, positive and negative rotation is stirred 20 minutes, then is soaked 30 minutes, is dehydrated afterwards, dries；
Three, allotment Pseudobulbus Bletillae polysaccharose solution: at normal temperatures, by 200 kg of water and 1500 grams of granular water soluble Pseudobulbus Bletillae (Rhizoma Bletillae)s
Polysaccharide is put in industrial washing machine and is mixed, and positive and negative rotation is stirred 20 minutes, makes Pseudobulbus Bletillae polysaccharose solution；
Four, Pseudobulbus Bletillae polysaccharose solidification: 50 kilograms of towels that step 2 is dried are put into the Pseudobulbus Bletillae polysaccharose that step 3 is deployed
In solution, positive and negative rotation is stirred 10 minutes, then soaks 30 minutes, is dehydrated afterwards, dries.
Practical proof: the towel will crossed through high-performance chitosan finishing agent dip-coating and Pseudobulbus Bletillae polysaccharose cured, uses
Unboiled water soaks sealing, 25-30 DEG C, humidity more than 80% environment in, carry out mildew test, after 8 days break seal,
Free from extraneous odour, still has the features such as good antibacterial anti-inflammatory, moldproof, anti-odour.
The method solidifying high-performance chitosan on fabric of the present invention, employing natural polysaccharide, environment-friendly degradable, entirely
Workflow environment is friendly, and technology is clean, even if the lean solution pH value of discharge also can reach 6-7, due in lean solution
Containing chitosan solvent, so the effect of flocculation sludge can also be played.
Claims (1)
1. the method solidifying high-performance chitosan on fabric, it is characterised in that it comprises the following steps:
One, allotment high-performance chitosan finishing agent: at normal temperatures, water, granular water soluble chitosan and graininess are resisted
Microbial inoculum mixes, and stirs, and makes high-performance chitosan finishing agent；Wherein, antibacterial is polyhexamethylene guanidine,
The concentration of chitosan is 1.5～3%, and the concentration of antibacterial is 1～2%；
Two, high-performance chitosan arranges: the high-performance chitosan finishing agent deployed by step one soaks, finish fabric,
High-performance chitosan finishing agent is 2: 1 with the weight ratio of fabric, is first put in high-performance chitosan finishing agent by fabric
Stir 20 minutes, then soak 30 minutes, be dehydrated afterwards, dry；
Three, allotment Pseudobulbus Bletillae polysaccharose solution: at normal temperatures, mixes water and granular water soluble Pseudobulbus Bletillae polysaccharose, and stirs all
Even, make Pseudobulbus Bletillae polysaccharose solution, the concentration of Pseudobulbus Bletillae polysaccharose is 0.5～1.5%；
Four, Pseudobulbus Bletillae polysaccharose solidification: fabric step 2 put in order puts into the Pseudobulbus Bletillae polysaccharose solution leaching that step 3 is deployed
Bubble, solidification, Pseudobulbus Bletillae polysaccharose solution is 4: 1 with the weight ratio of fabric, and fabric is first put into Pseudobulbus Bletillae polysaccharose solution stirring
10 minutes, then soak 30 minutes, it is dehydrated afterwards, dries.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210525242.3A CN102995403B (en) | 2012-11-17 | 2012-11-17 | The method solidifying high-performance chitosan on fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210525242.3A CN102995403B (en) | 2012-11-17 | 2012-11-17 | The method solidifying high-performance chitosan on fabric |
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| Publication Number | Publication Date |
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| CN102995403A CN102995403A (en) | 2013-03-27 |
| CN102995403B true CN102995403B (en) | 2016-10-12 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103938445A (en) * | 2014-02-25 | 2014-07-23 | 江志清 | Method for processing and finishing ecologic, oxygen permeable and antibiotic mouth mask by using chitosan oligosaccharide |
| CN105803776A (en) * | 2016-05-20 | 2016-07-27 | 青岛德喜哆瑭生物科技有限公司 | Isatis root polysaccharide modified fibers and preparation method thereof |
| CN119775570B (en) * | 2024-12-10 | 2025-12-12 | 苏州大学 | Multifunctional finishing liquid, preparation method thereof and application thereof in silk products |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101028535A (en) * | 2006-02-27 | 2007-09-05 | 权力敏 | Chitose coating with medical biological material |
| KR20090121506A (en) * | 2008-05-22 | 2009-11-26 | 아이텍스플래닝 주식회사 | Antimicrobial Processing Method of Cellulose Fabric or Cotton Fabric |
| CN101781849A (en) * | 2010-01-25 | 2010-07-21 | 江志清 | Method for curing chitosan on fabrics |
| CN102296465A (en) * | 2010-12-30 | 2011-12-28 | 上海水星家用纺织品股份有限公司 | Cassia seed composite antibacterial finishing agent, preparation method, method for processing fiber and application |
-
2012
- 2012-11-17 CN CN201210525242.3A patent/CN102995403B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101028535A (en) * | 2006-02-27 | 2007-09-05 | 权力敏 | Chitose coating with medical biological material |
| KR20090121506A (en) * | 2008-05-22 | 2009-11-26 | 아이텍스플래닝 주식회사 | Antimicrobial Processing Method of Cellulose Fabric or Cotton Fabric |
| CN101781849A (en) * | 2010-01-25 | 2010-07-21 | 江志清 | Method for curing chitosan on fabrics |
| CN102296465A (en) * | 2010-12-30 | 2011-12-28 | 上海水星家用纺织品股份有限公司 | Cassia seed composite antibacterial finishing agent, preparation method, method for processing fiber and application |
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Effective date of registration: 20180817 Address after: 266200 No. 568 Taishan Road, Jimo District, Qingdao, Shandong. Patentee after: Hang Ni Zhi (Qingdao) Technology Co., Ltd. Address before: 266200 81 shopping mall street, Jimo, Shandong Patentee before: Jiang Zhiqing |
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Effective date of registration: 20190428 Address after: 266200 No. 568 Taishan Road, Jimo District, Qingdao, Shandong. Patentee after: Qingdao Hongni Clothes Manufacture Co., Ltd. Address before: 266200 No. 568 Taishan Road, Jimo District, Qingdao, Shandong. Patentee before: Hang Ni Zhi (Qingdao) Technology Co., Ltd. |