CN104233473A - Seed crystal melting height measurement device for universal ingot furnace and measurement method therefor - Google Patents

Seed crystal melting height measurement device for universal ingot furnace and measurement method therefor Download PDF

Info

Publication number
CN104233473A
CN104233473A CN201410517436.8A CN201410517436A CN104233473A CN 104233473 A CN104233473 A CN 104233473A CN 201410517436 A CN201410517436 A CN 201410517436A CN 104233473 A CN104233473 A CN 104233473A
Authority
CN
China
Prior art keywords
height
crystal bar
long
seed crystal
ingot furnace
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201410517436.8A
Other languages
Chinese (zh)
Other versions
CN104233473B (en
Inventor
李书森
冯媛
兰洵
刘兴翀
林洪峰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tianwei New Energy Holdings Co Ltd
Original Assignee
Tianwei New Energy Holdings Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tianwei New Energy Holdings Co Ltd filed Critical Tianwei New Energy Holdings Co Ltd
Priority to CN201410517436.8A priority Critical patent/CN104233473B/en
Publication of CN104233473A publication Critical patent/CN104233473A/en
Application granted granted Critical
Publication of CN104233473B publication Critical patent/CN104233473B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

The invention relates to a seed crystal melting height measurement device for a universal ingot furnace and a measurement method therefor. The measurement method comprises the following specific steps: arranging a measurement device with good leakproofness at a cooling argon buckling portion at the top of an ingot furnace, fixing a long quartz crystal bar with a customized length on the measurement device, during the measuring process of the seed crystal height, manually adjusting the height of the long quartz crystal bar, and calculating the melting length of the seed crystal through the declining height of the long quartz crystal bar. The measurement device and the measurement method disclosed by the invention overcome the technical problem that in the prior art, the efficient ingot casting technology cannot be applied to the ingot furnace without a probe hole to measure the seed crystal melting height; the long quartz crystal bar with the customized length avoids the potential safety hazards caused by over high long quartz crystal bar and waste of the quartz raw material.

Description

For measuring apparatus and the measuring method of general ingot furnace seed crystal fusing height
Technical field
The present invention relates to the brilliant measuring apparatus field of photovoltaic art ingot casting furnace superintendent, particularly, relate to the measuring apparatus for general ingot furnace seed crystal fusing height and measuring method.
Background technology
Polysilicon is current topmost photovoltaic material, and polysilicon mostly takes directional solidification processes to prepare, casting polycrystalline silicon has the advantages such as easy and simple to handle, single feeds intake greatly, production cost is low compared with pulling of crystals, but there is a large amount of crystal boundaries and defect in polysilicon in castingprocesses, crystal boundary and defect can introduce deep energy level in silicon forbidden band, the deathnium of easy formation photogenerated minority carriers, and then the photoelectric transformation efficiency reducing polycrystalline silicon battery plate.Therefore, casting polycrystalline silicon number of grain boundaries how is reduced and defect concentration improves the research focus of polycrystal silicon cell photoelectric transformation efficiency at present.
At present, cast in the industry the method that high quality polysilicon generally adopts seed crystal seeding, one adopts monocrystalline silico briquette as seed crystal, and monocrystal seeding can reduce number of grain boundaries and defect concentration, effectively improves the photoelectric transformation efficiency of silicon chip quality and polycrystal silicon cell; But monocrystalline adds the production cost of silicon chip as seed crystal, further battery needs to adopt alkali making herbs into wool, increases production difficulty; Another kind adopts silicon chip fragment in production process as seed crystal, do not increase any production cost, just can reach the object of cost efficiency compared with conventional foundry ingot.
No matter be adopt monocrystalline or fragment as seed crystal, all relate to the requirement to seed crystal fusing extent control, only guaranteed seed portion fusing just can grow high-quality silicon ingot, measure seed crystal fusing fusing degree and become the principal element determining Ingot quality, measure with the open long crystal bar of quartz when measuring seed crystal fusing height, adopt the long crystal bar test of quartz that is high-purity, high temperature resistant, even thickness in molten silicon, measure the height that furnace chamber remains quartzy long crystal bar outward, indirect calculation goes out the fusing height of polysilicon.The current producer of ingot furnace is in the industry many, as U.S. GT, Germany PVA, domestic Zhejiang crystalline substance is contained, capital fortune is logical etc., GT, the ingot furnaces such as brilliant victory are built-in with the exploration hole of quartzy long crystal bar, and PVA polycrystalline silicon ingot or purifying furnace needs custom probe aperture apparatus, and different ingot furnace furnace chamber height differs, existing is measure on the ingot furnace being configured with exploration hole to the measurement of seed crystal fusing height in ingot furnace, long for quartz crystal bar is inserted and secured in corresponding exploration hole, the fusing height of seed crystal in ingot furnace is judged by the falling head calculating quartzy long crystal bar, the ingot furnace not configuring exploration hole then cannot carry out the measurement of seed crystal fusing height, existing measuring method cannot promote efficient ingot casting technology on this kind of ingot furnace, therefore, existing measuring method is not suitable for the measurement of seed crystal fusing height in general ingot furnace.
Summary of the invention
Technical problem to be solved by this invention is to provide the measuring apparatus and the measuring method that melt height for general ingot furnace seed crystal, overcomes existing measuring method and cannot apply the technical problem that efficient ingot casting technology measures seed crystal fusing height on the ingot furnace not configuring exploration hole.
The present invention's adopted technical scheme that solves the problem is: for the measuring apparatus of general ingot furnace seed crystal fusing height, comprise exploration hole interface pedestal, stationary installation, exploration hole interface pedestal offers fixed orifices, the outer cylinder of stationary installation one end is set to helicitic texture, the other end is connected with exploration hole interface pedestal, exploration hole interface pedestal and stationary installation inside are provided with through hole, stationary installation is also provided with the nut coordinated with sealing-ring, metal gasket, pass through nut, long for quartz crystal bar is fixed in through hole by the cooperation of metal gasket and helicitic texture, described exploration hole interface pedestal is arranged on ingot furnace top open part.Long for quartz crystal bar is inserted in through hole, sealing-ring is placed under metal gasket, again nut sleeve be located at helicitic texture and slowly tighten, metal gasket press seal circle is made to fix quartzy long crystal bar, realize the sealing of quartzy long crystal bar and measuring apparatus, ingot furnace top open part is the cooling argon gas export of ingot furnace, the circular flange of measuring apparatus screw or exploration hole interface pedestal is fixed on ingot furnace top open part, realize the sealing between measuring apparatus and ingot furnace, so, melting measuring process highly at whole seed crystal is seal in intact environment at one; During measurement, unscrew nut, adjust the height of quartzy long crystal bar, manual detection when contacting seed crystal, measures and records the height of quartzy long crystal bar, the fusing of seed crystal thereupon, the height of the long crystal bar of manual setting quartz gradually, until whole seed crystal melting process terminates, measure and record the height of quartzy long crystal bar, the difference of altitude of quartzy long crystal bar is the height of seed crystal fusing; Afterwards, determine that quartzy long crystal bar puts in order the position at place, guarantee deformation to occur bottom quartzy long crystal bar during ingot casting, the cooling argon gas in furnace chamber shields to the long crystal bar of quartz; By arranging a measuring apparatus at the cooling argon gas export of ingot furnace top of chamber, even if make also can apply efficient ingot casting technology to measure seed crystal fusing height at the ingot furnace not arranging exploration hole, instant invention overcomes prior art and cannot apply the technical problem that efficient ingot casting technology measures seed crystal fusing height on the ingot furnace not configuring exploration hole.
Further, the length of the long crystal bar of quartz is that the height of the long crystal bar of the quartz customized is the furnace chamber height of described ingot furnace, exploration hole interface height, hand-held height sum deduct seed crystal height, quartz crucible height, graphite bottom plate heights sum according to specific table customization height.The actual height of the furnace chamber of ingot furnace when furnace chamber height is practical application, exploration hole interface height is the height of the measuring apparatus of actual measurement, hand-held height is the height of the long crystal bar of quartz being exposed at measuring apparatus outside, seed crystal height is the elemental height of seed crystal, and quartz crucible height, graphite bottom plate heights are respectively the quartz crucible height, the graphite bottom plate heights that use ingot furnace to coordinate with reality, the long crystal bar standard size of quartz measuring in the industry seed crystal fusing height is at present that diameter is about 9mm, length is about 1825mm, and different brands ingot furnace furnace chamber height is different, 1825mm length is for long some ingot furnace, the long crystal bar of quartz puts in order the outer excessive height of rear furnace chamber, certain potential safety hazard is there is in this to ingot casting, and bring unnecessary difficulty to elevation carrection, quartzy long crystal bar is long in addition wastes material, add production cost, the different ingot furnace key distinction is that furnace roof is to DS radiating block height and furnace roof, exploration hole height is different with graphite bottom plate heights, the long boule length of industry universal is improper to some ingot furnaces, therefore the long crystal bar proposed for different ingot furnace customization different lengths is necessary, therefore, the present invention is first according to ingot furnace used in actual seed crystal melting process, exploration hole interface arrangement, quartz crucible, the height of graphite base plate and hand-held height calculate the height of the long crystal bar of required quartz, in addition, the long crystal bar ride out of quartz is no more than 1000mm, be convenient to the measurement that quartzy long crystal bar puts in order position, customize the long crystal bar of quartz of corresponding height again, the too high potential safety hazard caused of quartzy long crystal bar is avoided by the height customizing quartzy long crystal bar, and the waste of silica starting material.
Further, described hand-held height is 150 ~ 400mm.Quartz long crystal bar reserve certain hand-held height, be convenient to manual setting quartz long crystal bar height, suitable hand-held height convenient operation, make measure time operate safer, measure more accurate.
Further, exploration hole interface pedestal bottom offer with rubber packing with the use of groove.The groove of exploration hole interface pedestal bottom and rubber packing with the use of, increase the cushion effect of the through hole contact position of quartzy long crystal bar and gaging hole interface pedestal, avoid quartzy long crystal bar impaired in artificial adjustment process.
Further, appropriate vacuum grease smeared by rubber packing.To make between rubber packing and groove fixing more stable, better tightness, prevents gas leakage.
Further, appropriate vacuum grease smeared by sealing-ring.The stopping property that vacuum grease can strengthen quartzy long crystal bar and exploration hole interface arrangement further smeared by sealing-ring, prevents gas leakage.
For the measuring method of the measuring apparatus of general ingot furnace seed crystal fusing height, comprise the following steps:
First, long for the quartz of customized lengths crystal bar is inserted in through hole, lentamente long for quartz crystal bar is moved down, until quartzy long crystal bar touches the seed crystal in ingot furnace, sealing-ring is placed under metal gasket, again nut sleeve be located at helicitic texture and slowly tighten, making metal gasket press seal circle fix quartzy long crystal bar, record the elemental height of quartzy long crystal bar;
Secondly, ingot furnace is heated, makes the seed crystal melted by heat in stove, in measuring process, unscrew the height of the long crystal bar of nut manual regulation quartz, quartzy long crystal bar is contacted with seed crystal all the time in measuring process, and records the falling head of quartzy long crystal bar;
Then, calculated the fusing height of seed crystal by the height of the decline of the long crystal bar of quartz, when the height of seed crystal fusing meets the requirements, measuring process terminates, and stops heating, records the height of quartzy long crystal bar;
Finally, carried by long for quartz crystal bar to the quartzy long crystal bar of argon shield cooling, long for quartz crystal bar is fixed on argon shield district by fastening nut.
To sum up, the invention has the beneficial effects as follows:
1, the present invention is by arranging a measuring apparatus at the cooling argon gas export of ingot furnace top of chamber, even if make also can apply efficient ingot casting technology to measure seed crystal fusing height on the ingot furnace not arranging exploration hole, overcome prior art and cannot apply the technical problem that efficient ingot casting technology measures seed crystal fusing height on the ingot furnace not configuring exploration hole.
2, the present invention avoids the too high potential safety hazard caused of quartzy long crystal bar by the height customizing quartzy long crystal bar.
3, the present invention avoids the waste of the too high silica starting material caused of quartzy long crystal bar by the height customizing quartzy long crystal bar.
4, the present invention is by smearing vacuum grease to sealing-ring, improves the stopping property of quartzy long crystal bar and exploration hole interface arrangement.
Accompanying drawing explanation
Fig. 1 is nut;
Fig. 2 is metal gasket;
Fig. 3 is measuring apparatus schematic diagram;
Fig. 4 is measuring apparatus upward view;
Fig. 5 is metal closures.
Mark and corresponding component title in accompanying drawing:
1-nut; 2-metal gasket; 3-stationary installation; 4-exploration hole interface pedestal; 5-fixed orifices; 6-groove; 7-through hole; 8-metal closures, 31-helicitic texture.
Embodiment
Below in conjunction with embodiment and accompanying drawing, to the detailed description further of the present invention's do, but embodiments of the present invention are not limited thereto; Those skilled in the art also can make many distortion and improvement on basis of the present invention, the change of material, the change of size dimension, and the configuration aspects done on basis of the present invention is changed accordingly and all should be considered as protection scope of the present invention.
Embodiment:
As shown in Fig. 1 to 5, the present invention relates to the measuring apparatus for general ingot furnace seed crystal fusing height, comprise exploration hole interface pedestal 4, stationary installation 3, exploration hole interface pedestal 4 offers fixed orifices 5, the outer cylinder of stationary installation 3 one end is set to helicitic texture 31, the other end is connected with exploration hole interface pedestal 4, exploration hole interface pedestal 4 and stationary installation 3 inside are provided with through hole 7, stationary installation 3 is also provided with the nut 1 coordinated with sealing-ring, metal gasket 2, by nut 1, long for quartz crystal bar is fixed in through hole 7 by the cooperation of metal gasket 2 and helicitic texture 31, appropriate vacuum grease smeared by sealing-ring, exploration hole interface pedestal 4 is arranged on ingot furnace top open part, the long crystal bar of quartz is the quartz pushrod according to specific table customization height, the height of the long crystal bar of the quartz customized is the furnace chamber height of ingot furnace, exploration hole interface height, hand-held height sum deducts seed crystal height, quartz crucible height, graphite bottom plate heights sum, hand-held height is 150-400mm, exploration hole interface pedestal 4 bottom offer with rubber packing with the use of groove 6, appropriate vacuum grease smeared by rubber packing, when need not detect fusing for a long time under casting ingot process, long for quartz crystal bar can be replaced with metal closures 8 and be used for sealing.
As shown in Figures 1 to 3, the invention still further relates to the measuring method of the measuring apparatus for general ingot furnace seed crystal fusing height, comprise the following steps:
First, long for the quartz of customized lengths crystal bar is inserted in through hole 7, lentamente long for quartz crystal bar is moved down, until quartzy long crystal bar touches the seed crystal in ingot furnace, metal gasket places sealing-ring 2 times, again nut 1 be set in helicitic texture 31 and slowly tighten, making metal gasket 2 press seal circle fix quartzy long crystal bar, record the elemental height of quartzy long crystal bar;
Secondly, ingot furnace is heated, makes the seed crystal melted by heat in stove, in measuring process, unscrew the height of the long crystal bar of nut 1 manual regulation quartz, quartzy long crystal bar is contacted with seed crystal all the time in measuring process, and records the falling head of quartzy long crystal bar;
Then, calculated the fusing height of seed crystal by the height of the decline of the long crystal bar of quartz, when the height of seed crystal fusing meets the requirements, measuring process terminates, and stops heating, records the height of quartzy long crystal bar;
Finally, carried by long for quartz crystal bar to the quartzy long crystal bar of argon shield cooling, long for quartz crystal bar is fixed on argon shield district by fastening nut 1.
The measuring method of seed crystal fusing height extends on the PVA ingot furnace that can not directly measure or the ingot furnace not having device exploration hole by the present invention, and the present invention is that this type of ingot furnace is provided with general measuring apparatus.
As mentioned above, the present invention can be realized preferably.

Claims (7)

1. for the measuring apparatus of general ingot furnace seed crystal fusing height, comprise exploration hole interface pedestal (4), stationary installation (3), exploration hole interface pedestal (4) offers fixed orifices (5), the outer cylinder of stationary installation (3) one end is set to helicitic texture (31), the other end is connected with exploration hole interface pedestal (4), exploration hole interface pedestal (4) and stationary installation (3) inside are provided with through hole (7), it is characterized in that, described stationary installation (3) is also provided with the nut (1) coordinated with sealing-ring, metal gasket (2), by nut (1), long for quartz crystal bar is fixed in through hole (7) by the cooperation of metal gasket (2) and helicitic texture (31), described exploration hole interface pedestal (4) is arranged on ingot furnace top open part.
2. the measuring apparatus for general ingot furnace seed crystal fusing height according to claim 1, it is characterized in that, the length of the long crystal bar of described quartz is that the height of the long crystal bar of the quartz customized is the furnace chamber height of described ingot furnace, exploration hole interface height, hand-held height sum deduct seed crystal height, quartz crucible height, graphite bottom plate heights sum according to specific table customization height.
3. the measuring apparatus for general ingot furnace seed crystal fusing height according to claim 2, it is characterized in that, described hand-held height is 150 ~ 400mm.
4. the measuring apparatus for general ingot furnace seed crystal fusing height according to claim 1, is characterized in that, exploration hole interface pedestal (4) bottom offer with rubber packing with the use of groove (6).
5. the measuring apparatus for general ingot furnace seed crystal fusing height according to claim 4, it is characterized in that, appropriate vacuum grease smeared by described rubber packing.
6., according to the arbitrary described measuring apparatus for general ingot furnace seed crystal fusing height of claim 1 to 5, it is characterized in that, appropriate vacuum grease smeared by described sealing-ring.
7., for the measuring method of the measuring apparatus of general ingot furnace seed crystal fusing height, it is characterized in that, comprise the following steps:
First, long for the quartz of customized lengths crystal bar is inserted in through hole (7), lentamente long for quartz crystal bar is moved down, until quartzy long crystal bar touches the seed crystal in ingot furnace, metal gasket places sealing-ring under (2), again nut (1) be set in helicitic texture (31) and slowly tighten, making metal gasket (2) press seal circle fix quartzy long crystal bar, record the elemental height of quartzy long crystal bar;
Secondly, ingot furnace is heated, makes the seed crystal melted by heat in stove, in measuring process, unscrew the height of the long crystal bar of nut (1) manual regulation quartz, quartzy long crystal bar is contacted with seed crystal all the time in measuring process, and records the falling head of quartzy long crystal bar;
Then, calculated the fusing height of seed crystal by the height of the decline of the long crystal bar of quartz, when the height of seed crystal fusing meets the requirements, measuring process terminates, and stops heating, records the height of quartzy long crystal bar;
Finally, carried by long for quartz crystal bar to the quartzy long crystal bar of argon shield cooling, long for quartz crystal bar is fixed on argon shield district by fastening nut (1).
CN201410517436.8A 2014-09-30 2014-09-30 Measurement apparatus and measuring method for general ingot furnace seed crystal fusing height Expired - Fee Related CN104233473B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410517436.8A CN104233473B (en) 2014-09-30 2014-09-30 Measurement apparatus and measuring method for general ingot furnace seed crystal fusing height

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410517436.8A CN104233473B (en) 2014-09-30 2014-09-30 Measurement apparatus and measuring method for general ingot furnace seed crystal fusing height

Publications (2)

Publication Number Publication Date
CN104233473A true CN104233473A (en) 2014-12-24
CN104233473B CN104233473B (en) 2016-08-24

Family

ID=52222339

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410517436.8A Expired - Fee Related CN104233473B (en) 2014-09-30 2014-09-30 Measurement apparatus and measuring method for general ingot furnace seed crystal fusing height

Country Status (1)

Country Link
CN (1) CN104233473B (en)

Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06234592A (en) * 1985-01-14 1994-08-23 Komatsu Electron Metals Co Ltd Production of semiconductor silicon single crystal
CN202099411U (en) * 2011-04-06 2012-01-04 镇江荣德新能源科技有限公司 Automatic measuring device for crystal growth speed of multi-crystal furnace
CN102692199A (en) * 2012-06-11 2012-09-26 苏州禹石自动化工程技术有限公司 Unfused silicon ingot height measuring system
CN202482491U (en) * 2012-02-03 2012-10-10 昆山中辰矽晶有限公司 Height analysis apparatus
CN202755099U (en) * 2012-09-06 2013-02-27 镇江荣德新能源科技有限公司 Solid liquid interface determination device for silicon ingot furnace
CN203144556U (en) * 2013-02-21 2013-08-21 无锡开日能源科技股份有限公司 Device for measuring height of crystal
CN103409797A (en) * 2013-08-27 2013-11-27 天威新能源控股有限公司 Device for measuring long crystal bar of ingot furnace
CN203382851U (en) * 2013-08-01 2014-01-08 安徽大晟新能源设备科技有限公司 Testing device for melting thickness of seed crystals of pseudo-single crystal ingot furnace
CN203384363U (en) * 2013-07-25 2014-01-08 天津市亚安科技股份有限公司 Nut sealing structure
CN103668449A (en) * 2012-09-06 2014-03-26 镇江荣德新能源科技有限公司 Solid-liquid interface determination device for silicon ingot furnace
CN203728966U (en) * 2014-03-07 2014-07-23 江苏华盛天龙光电设备股份有限公司 Crystal measurement device of polycrystal furnace
TW201432102A (en) * 2013-02-08 2014-08-16 Sino American Silicon Prod Inc Ingot measurement rod
CN204058658U (en) * 2014-09-30 2014-12-31 天威新能源控股有限公司 A kind of measuring apparatus for general ingot furnace seed crystal fusing height

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06234592A (en) * 1985-01-14 1994-08-23 Komatsu Electron Metals Co Ltd Production of semiconductor silicon single crystal
CN202099411U (en) * 2011-04-06 2012-01-04 镇江荣德新能源科技有限公司 Automatic measuring device for crystal growth speed of multi-crystal furnace
CN202482491U (en) * 2012-02-03 2012-10-10 昆山中辰矽晶有限公司 Height analysis apparatus
CN102692199A (en) * 2012-06-11 2012-09-26 苏州禹石自动化工程技术有限公司 Unfused silicon ingot height measuring system
CN103668449A (en) * 2012-09-06 2014-03-26 镇江荣德新能源科技有限公司 Solid-liquid interface determination device for silicon ingot furnace
CN202755099U (en) * 2012-09-06 2013-02-27 镇江荣德新能源科技有限公司 Solid liquid interface determination device for silicon ingot furnace
TW201432102A (en) * 2013-02-08 2014-08-16 Sino American Silicon Prod Inc Ingot measurement rod
CN203144556U (en) * 2013-02-21 2013-08-21 无锡开日能源科技股份有限公司 Device for measuring height of crystal
CN203384363U (en) * 2013-07-25 2014-01-08 天津市亚安科技股份有限公司 Nut sealing structure
CN203382851U (en) * 2013-08-01 2014-01-08 安徽大晟新能源设备科技有限公司 Testing device for melting thickness of seed crystals of pseudo-single crystal ingot furnace
CN103409797A (en) * 2013-08-27 2013-11-27 天威新能源控股有限公司 Device for measuring long crystal bar of ingot furnace
CN203728966U (en) * 2014-03-07 2014-07-23 江苏华盛天龙光电设备股份有限公司 Crystal measurement device of polycrystal furnace
CN204058658U (en) * 2014-09-30 2014-12-31 天威新能源控股有限公司 A kind of measuring apparatus for general ingot furnace seed crystal fusing height

Also Published As

Publication number Publication date
CN104233473B (en) 2016-08-24

Similar Documents

Publication Publication Date Title
CN101148777B (en) Method and device for growing gallium-mixing silicon monocrystal by czochralski method
CN202139324U (en) Graphite thermal field system of upward-exhausting thermal field type czochralski silicon mono-crystal furnace
CN103103604A (en) Manufacturing method of large-size C-oriented sapphire crystals
CN102936747A (en) Method for casting ingot of pseudo-single crystal through large-sized crucible
CN201058893Y (en) Device for growing gallium-doped silicon single crystal by Czochralski method
CN102181925A (en) Growth process and device for growing IC-level silicon single crystal with low Fe content by czochralski method
CN106435714A (en) Polycrystalline silicon solution liquid level distance positioning method
CN208976814U (en) Aluminium alloy smelting, heat preservation, casting all-in-one oven
CN204058658U (en) A kind of measuring apparatus for general ingot furnace seed crystal fusing height
CN206052206U (en) A kind of sapphire single-crystal furnace
CN104233473B (en) Measurement apparatus and measuring method for general ingot furnace seed crystal fusing height
CN208419812U (en) Length-measuring appliance is used in a kind of production of silicon single crystal rod
CN101774583A (en) Crucible device for polycrystalline silicon growth process
CN103397378A (en) Preparation method of polycrystalline silicon ingot
CN100552096C (en) A kind of improved BaY that is applicable to 2F 8The temperature gradient method of single crystal growth and device thereof
CN203923449U (en) A kind of low-energy consumption single-crystal stove
CN207877928U (en) A kind of crystal height measuring device of polycrystalline silicon ingot or purifying furnace
CN205175504U (en) Measurement device for seed crystal height in liquid silicon of high temperature in polycrystalline silicon ingot furnace
CN214060708U (en) Czochralski single crystal thermal field
CN205893456U (en) Single crystal growing furnace silicon solution liquid surface position detecting device and adjustment system
CN203639604U (en) Flexible shaft lifting type single crystal furnace
CN207811928U (en) The single crystal growing furnace of heat shielding component is set
CN209276672U (en) A kind of vertical pulling heavy Sb-admixed silicon monocrystal antimony source purifying plant
CN109097822A (en) A kind of carbon content method reduced in monocrystalline crystal bar
CN207793470U (en) The single crystal growing furnace of applicating energy-saving type thermal field

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160824

Termination date: 20170930

CF01 Termination of patent right due to non-payment of annual fee