CN106687569A - 制备硫化的碱土金属十二烷基酚盐的方法 - Google Patents

制备硫化的碱土金属十二烷基酚盐的方法 Download PDF

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Publication number
CN106687569A
CN106687569A CN201580029206.XA CN201580029206A CN106687569A CN 106687569 A CN106687569 A CN 106687569A CN 201580029206 A CN201580029206 A CN 201580029206A CN 106687569 A CN106687569 A CN 106687569A
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CN
China
Prior art keywords
reaction
amount
earth metal
oil
alkyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201580029206.XA
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English (en)
Chinese (zh)
Inventor
M·G·法赫米
R·L·帕森斯
L·K·柯南特
D·J·贝克尔
J·T·施特劳赫
R·J·卢卡谢夫斯基
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Lubrizol Corp
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Lubrizol Corp
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Filing date
Publication date
Application filed by Lubrizol Corp filed Critical Lubrizol Corp
Publication of CN106687569A publication Critical patent/CN106687569A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M135/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing sulfur, selenium or tellurium
    • C10M135/02—Sulfurised compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M159/00—Lubricating compositions characterised by the additive being of unknown or incompletely defined constitution
    • C10M159/12—Reaction products
    • C10M159/20—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products
    • C10M159/22—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products containing phenol radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
    • C07G99/00—Subject matter not provided for in other groups of this subclass
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/08—Thiols; Sulfides; Polysulfides; Mercaptals
    • C10M2219/082—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms
    • C10M2219/087—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Derivatives thereof, e.g. sulfurised phenols
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/08—Thiols; Sulfides; Polysulfides; Mercaptals
    • C10M2219/082—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms
    • C10M2219/087—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Derivatives thereof, e.g. sulfurised phenols
    • C10M2219/089—Overbased salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/04—Groups 2 or 12
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/04—Detergent property or dispersant property
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/25—Internal-combustion engines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2070/00—Specific manufacturing methods for lubricant compositions

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Lubricants (AREA)
CN201580029206.XA 2014-04-04 2015-03-23 制备硫化的碱土金属十二烷基酚盐的方法 Pending CN106687569A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201461975256P 2014-04-04 2014-04-04
US61/975,256 2014-04-04
PCT/US2015/021949 WO2015153160A1 (en) 2014-04-04 2015-03-23 Method for preparing a sulfurized alkaline earth metal dodecylphenate

Publications (1)

Publication Number Publication Date
CN106687569A true CN106687569A (zh) 2017-05-17

Family

ID=52875774

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201580029206.XA Pending CN106687569A (zh) 2014-04-04 2015-03-23 制备硫化的碱土金属十二烷基酚盐的方法

Country Status (6)

Country Link
US (1) US20170015925A1 (de)
EP (1) EP3126476A1 (de)
CN (1) CN106687569A (de)
CA (1) CA2944879A1 (de)
SG (1) SG11201608327TA (de)
WO (1) WO2015153160A1 (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3199612A1 (de) 2016-01-26 2017-08-02 Infineum International Limited Metallreinigungsmittel
US9688939B1 (en) 2016-01-26 2017-06-27 Infineum International Limited Metal detergents
EP3205708A1 (de) 2016-02-15 2017-08-16 Infineum International Limited Metallreinigungsmittel

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3474035A (en) * 1967-03-20 1969-10-21 Texaco Inc Lubricating oil containing overbased sulfurized calcium alkylphenolate
WO2013119623A1 (en) * 2012-02-08 2013-08-15 The Lubrizol Corporation Method of preparing a sulfurized alkaline earth metal dodecylphenate

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US2501731A (en) 1946-10-14 1950-03-28 Union Oil Co Modified lubricating oil
US2680096A (en) 1951-02-12 1954-06-01 California Research Corp Process for preparing sulfurized polyvalent metal phenates
US2616911A (en) 1951-03-16 1952-11-04 Lubrizol Corp Organic alkaline earth metal complexes formed by use of sulfonic promoters
US2616925A (en) 1951-03-16 1952-11-04 Lubrizol Corp Organic alkaline earth metal complexes formed by use of thiophosphoric promoters
US2616905A (en) 1952-03-13 1952-11-04 Lubrizol Corp Organic alkaline earth metal complexes and methods of making same
US2777874A (en) 1952-11-03 1957-01-15 Lubrizol Corp Metal complexes and methods of making same
US3036971A (en) 1958-12-24 1962-05-29 Socony Mobil Oil Co Inc Lubricating oils containing carbonated basic sulfurized calcium phenates
DE1248643B (de) 1959-03-30 1967-08-31 The Lubrizol Corporation, Cleveland, Ohio (V. St. A.) Verfahren zur Herstellung von öllöslichen aeylierten Aminen
US3488284A (en) 1959-12-10 1970-01-06 Lubrizol Corp Organic metal compositions and methods of preparing same
US3282835A (en) 1963-02-12 1966-11-01 Lubrizol Corp Carbonated bright stock sulfonates and lubricants containing them
US3381022A (en) 1963-04-23 1968-04-30 Lubrizol Corp Polymerized olefin substituted succinic acid esters
US3320162A (en) 1964-05-22 1967-05-16 Phillips Petroleum Co Increasing the base number of calcium petroleum sulfonate
US3318809A (en) 1965-07-13 1967-05-09 Bray Oil Co Counter current carbonation process
GB1105217A (en) 1965-10-05 1968-03-06 Lubrizol Corp Process for preparing basic metal phenates
US3365396A (en) 1965-12-28 1968-01-23 Texaco Inc Overbased calcium sulfonate
US3384585A (en) 1966-08-29 1968-05-21 Phillips Petroleum Co Overbasing lube oil additives
US3464970A (en) 1967-03-13 1969-09-02 Maruzen Oil Co Ltd Process for preparing over-based sulfurized calcium phenates
US3634515A (en) 1968-11-08 1972-01-11 Standard Oil Co Alkylene polyamide formaldehyde
US3629109A (en) 1968-12-19 1971-12-21 Lubrizol Corp Basic magnesium salts processes and lubricants and fuels containing the same
US4234435A (en) 1979-02-23 1980-11-18 The Lubrizol Corporation Novel carboxylic acid acylating agents, derivatives thereof, concentrate and lubricant compositions containing the same, and processes for their preparation
US4285822A (en) 1979-06-28 1981-08-25 Chevron Research Company Process for preparing a sulfurized molybdenum-containing composition and lubricating oil containing the composition
US4594378A (en) 1985-03-25 1986-06-10 The Lubrizol Corporation Polymeric compositions, oil compositions containing said polymeric compositions, transmission fluids and hydraulic fluids
GB8531626D0 (en) 1985-12-23 1986-02-05 Shell Int Research Grease composition
US5024773A (en) 1986-10-21 1991-06-18 Chevron Research Company Methods for preparing, group II metal overbased sulfurized alkylphenols
DE69327515T2 (de) 1992-12-07 2000-06-21 Ethyl Petroleum Additives, Inc. Verfahren zur Herstellung von überbasischen Phenolaten
US6310011B1 (en) 1994-10-17 2001-10-30 The Lubrizol Corporation Overbased metal salts useful as additives for fuels and lubricants
CA2277469C (en) 1997-11-13 2005-07-05 Lubrizol Adibis Holdings (Uk) Limited Salicyclic calixarenes and their use as lubricant additives
EP1254100A1 (de) 2000-02-07 2002-11-06 Bp Oil International Limited Calixarene und ihre verwendung als schmierstoffadditive
US6310009B1 (en) 2000-04-03 2001-10-30 The Lubrizol Corporation Lubricating oil compositions containing saligenin derivatives
US6569818B2 (en) 2000-06-02 2003-05-27 Chevron Oronite Company, Llc Lubricating oil composition
ATE292667T1 (de) 2001-11-05 2005-04-15 Lubrizol Corp Schmiermittelzusammensetzung mit verbesserter brennstoffersparnis
US7651987B2 (en) 2004-10-12 2010-01-26 The Lubrizol Corporation Tartaric acid derivatives as fuel economy improvers and antiwear agents in crankcase oils and preparation thereof
EP4098724A1 (de) 2005-03-28 2022-12-07 The Lubrizol Corporation Titanzusammensetzungen und komplexe als additive in schmiermitteln
CN101679900A (zh) 2007-05-24 2010-03-24 卢布里佐尔公司 包含基于羟基多羧酸衍生物和钼化合物的无灰抗磨剂的润滑组合物
US7838474B2 (en) * 2007-10-31 2010-11-23 Chevron Oronite Company Llc Lubricating oil compositions comprising a biodiesel fuel and a detergent
EP2367917A1 (de) 2008-12-09 2011-09-28 The Lubrizol Corporation Schmiermittelzusammensetzung, enthaltend eine von einer hydroxycarbonsäure abgeleitete verbindung

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3474035A (en) * 1967-03-20 1969-10-21 Texaco Inc Lubricating oil containing overbased sulfurized calcium alkylphenolate
WO2013119623A1 (en) * 2012-02-08 2013-08-15 The Lubrizol Corporation Method of preparing a sulfurized alkaline earth metal dodecylphenate

Also Published As

Publication number Publication date
SG11201608327TA (en) 2016-11-29
US20170015925A1 (en) 2017-01-19
EP3126476A1 (de) 2017-02-08
CA2944879A1 (en) 2015-10-08
WO2015153160A1 (en) 2015-10-08

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EE01 Entry into force of recordation of patent licensing contract
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Application publication date: 20170517

Assignee: Lubrizol additive (Zhuhai) Co., Ltd.

Assignor: Lubrizol Corp.

Contract record no.: 2018990000081

Denomination of invention: Method for preparing a sulfurized alkaline earth metal dodecylphenate

License type: Common License

Record date: 20180410

EC01 Cancellation of recordation of patent licensing contract

Assignee: Lubrizol additive (Zhuhai) Co., Ltd.

Assignor: Lubrizol Corp.

Contract record no.: 2018990000081

Date of cancellation: 20190322

EC01 Cancellation of recordation of patent licensing contract
EE01 Entry into force of recordation of patent licensing contract
EE01 Entry into force of recordation of patent licensing contract

Application publication date: 20170517

Assignee: Lubrizol additive (Zhuhai) Co., Ltd.

Assignor: Lubrizol Corp.

Contract record no.: 2019990000109

Denomination of invention: Method for preparing a sulfurized alkaline earth metal dodecylphenate

License type: Common License

Record date: 20190403

WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170517

EC01 Cancellation of recordation of patent licensing contract
EC01 Cancellation of recordation of patent licensing contract

Assignee: Lubrizol additive (Zhuhai) Co., Ltd.

Assignor: THE LUBRIZOL Corp.

Contract record no.: 2019990000109

Date of cancellation: 20200309