CN106977111A - A kind of production method of environment-friendly type colored glazed glass - Google Patents
A kind of production method of environment-friendly type colored glazed glass Download PDFInfo
- Publication number
- CN106977111A CN106977111A CN201710363270.2A CN201710363270A CN106977111A CN 106977111 A CN106977111 A CN 106977111A CN 201710363270 A CN201710363270 A CN 201710363270A CN 106977111 A CN106977111 A CN 106977111A
- Authority
- CN
- China
- Prior art keywords
- glass
- parts
- glass substrate
- low temperature
- glaze
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000011521 glass Substances 0.000 title claims abstract description 95
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- 239000000758 substrate Substances 0.000 claims abstract description 37
- 238000001035 drying Methods 0.000 claims abstract description 21
- 239000011248 coating agent Substances 0.000 claims abstract description 14
- 238000000576 coating method Methods 0.000 claims abstract description 14
- 238000001816 cooling Methods 0.000 claims abstract description 7
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 229910017083 AlN Inorganic materials 0.000 claims description 6
- PIGFYZPCRLYGLF-UHFFFAOYSA-N Aluminum nitride Chemical compound [Al]#N PIGFYZPCRLYGLF-UHFFFAOYSA-N 0.000 claims description 6
- 239000001856 Ethyl cellulose Substances 0.000 claims description 6
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 claims description 6
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 6
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 claims description 6
- MCMNRKCIXSYSNV-UHFFFAOYSA-N ZrO2 Inorganic materials O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 6
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 6
- 239000004327 boric acid Substances 0.000 claims description 6
- 239000000919 ceramic Substances 0.000 claims description 6
- 229910000423 chromium oxide Inorganic materials 0.000 claims description 6
- 229920001249 ethyl cellulose Polymers 0.000 claims description 6
- 235000019325 ethyl cellulose Nutrition 0.000 claims description 6
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims description 6
- 239000011863 silicon-based powder Substances 0.000 claims description 6
- 239000004925 Acrylic resin Substances 0.000 claims description 3
- 229920000178 Acrylic resin Polymers 0.000 claims description 3
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 238000002360 preparation method Methods 0.000 abstract description 3
- 230000007774 longterm Effects 0.000 abstract 1
- 239000002253 acid Substances 0.000 description 4
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 3
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/02—Surface treatment of glass, not in the form of fibres or filaments, by coating with glass
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/30—Aspects of methods for coating glass not covered above
- C03C2218/365—Coating different sides of a glass substrate
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Laminated Bodies (AREA)
Abstract
The invention discloses a kind of production method of environment-friendly type colored glazed glass, comprise the following steps：A, by glass substrate surface deionized water rinsing, low temperature drying in low temperature baking oven is put into afterwards；B, one side one layer of glass glaze of coating in glass substrate, are coated with being put into after one layer of glass glaze in low temperature baking oven after drying at room temperature and dry；C, another side one layer of glass glaze of coating in glass substrate；D, glass substrate is finally integrally put into the high temperature oven high temperature preheated one-section time；E, glass substrate is finally integrally heated to fast cooling after softening point annealed finished product, preparation method of the present invention is simple, and obtained colored glazed glass is indeformable, colour-fast, good environmental protection, and long-term use is not in glass glaze obscission.
Description
Technical field
The present invention relates to colored glazed glass preparing technical field, specially a kind of production method of environment-friendly type colored glazed glass.
Background technology
Colored glazed glass is that inorganic glaze is printed onto into glass surface, then drying, tempering or thermalization working process, by glaze
Material is forever sintered in glass surface and obtains a kind of wear-resisting, acid and alkali-resistance decorative glasses product.This product has very high
Feature and dicoration.It has many different colors and decorative pattern, such as strip, netted and electric shape pattern.Can also basis
The difference of client needs otherwise designed decorative pattern.Colored glazed glass advocates out a kind of Urban Landscape as one kind decoration and advertisement screen
New look, existing colored glazed glass complex manufacturing technology, glass is easily deformed, and glass glaze poor adhesive force, easily fade
Or come off.
The content of the invention
It is an object of the invention to provide a kind of production method of environment-friendly type colored glazed glass, to solve in above-mentioned background technology
The problem of proposition.
To achieve the above object, the present invention provides following technical scheme：A kind of production method of environment-friendly type colored glazed glass, bag
Include following steps：
A, by glass substrate surface deionized water rinsing, low temperature drying in low temperature baking oven is put into afterwards；
B, one side one layer of glass glaze of coating in glass substrate, low temperature is put into after one layer of glass glaze is coated with after drying at room temperature
Dried in baking oven；
C, another side one layer of glass glaze of coating in glass substrate；
D, glass substrate is finally integrally put into the high temperature oven high temperature preheated one-section time；
E, glass substrate is finally integrally heated to fast cooling after softening point annealed finished product.
It is preferred that, the glass glaze in the step B and step C is completely the same, and its component includes boric acid 5- by weight
12 parts, 5-10 parts of ceramic powder, 3-8 parts of zirconium dioxide, 5-15 parts of silicon powder, 4-12 parts of titania powder, 5-10 parts of stalactite,
5-10 parts of chromium oxide, 10-20 parts of acrylic resin, 3-8 parts of ethyl cellulose, 4-15 parts of aluminium nitride.
It is preferred that, low temperature oven temperature is 40 DEG C -50 DEG C in the step A, and drying time is 5min-10min.
It is preferred that, the step D high temperatures oven temperature is 180 DEG C -220 DEG C, and preheating time is 10min-20min.
Compared with prior art, the beneficial effects of the invention are as follows：Preparation method of the present invention is simple, and obtained colored glazed glass is not
Deformation, colour-fast, good environmental protection；Wherein, using glass substrate to be integrally put into the high temperature oven high temperature preheated one-section time；
Temperature is 180 DEG C -220 DEG C, and preheating time is 10min-20min.Ensure that colored glazed glass is used for a long time is not in glass
Glaze obscission.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model that the present invention is protected
Enclose.
Embodiment one：
A kind of production method of environment-friendly type colored glazed glass, comprises the following steps：
A, by glass substrate surface deionized water rinsing, low temperature drying in low temperature baking oven is put into afterwards；Low temperature oven temperature is
40 DEG C, drying time is 5min；
B, one side one layer of glass glaze of coating in glass substrate, low temperature is put into after one layer of glass glaze is coated with after drying at room temperature
Dried in baking oven；
C, another side one layer of glass glaze of coating in glass substrate；
D, glass substrate is finally integrally put into the high temperature oven high temperature preheated one-section time；High temperature oven temperature is 180 DEG C, in advance
The hot time is 10min；
E, glass substrate is finally integrally heated to fast cooling after softening point annealed finished product.
In the present embodiment, the glass glaze in step B and step C is completely the same, and its component includes boric acid 5 by weight
Part, 5 parts of ceramic powder, 3 parts of zirconium dioxide, 5 parts of silicon powder, 4 parts of titania powder, 5- parts of stalactite, 5 parts of chromium oxide, propylene
10 parts of acid resin, 3 parts of ethyl cellulose, 4 parts of aluminium nitride.
Embodiment two：
A kind of production method of environment-friendly type colored glazed glass, comprises the following steps：
A, by glass substrate surface deionized water rinsing, low temperature drying in low temperature baking oven is put into afterwards；Low temperature oven temperature is
50 DEG C, drying time is 10min；
B, one side one layer of glass glaze of coating in glass substrate, low temperature is put into after one layer of glass glaze is coated with after drying at room temperature
Dried in baking oven；
C, another side one layer of glass glaze of coating in glass substrate；
D, glass substrate is finally integrally put into the high temperature oven high temperature preheated one-section time；High temperature oven temperature is 220 DEG C, in advance
The hot time is 20min；
E, glass substrate is finally integrally heated to fast cooling after softening point annealed finished product.
In the present embodiment, the glass glaze in step B and step C is completely the same, and its component includes boric acid 12 by weight
Part, 10 parts of ceramic powder, 8 parts of zirconium dioxide, 15 parts of silicon powder, 12 parts of titania powder, 10 parts of stalactite, 10 parts of chromium oxide,
20 parts of acrylic resin, 8 parts of ethyl cellulose, 15 parts of aluminium nitride.
Embodiment three：
A kind of production method of environment-friendly type colored glazed glass, comprises the following steps：
A, by glass substrate surface deionized water rinsing, low temperature drying in low temperature baking oven is put into afterwards；Low temperature oven temperature is
42 DEG C, drying time is 8min；
B, one side one layer of glass glaze of coating in glass substrate, low temperature is put into after one layer of glass glaze is coated with after drying at room temperature
Dried in baking oven；
C, another side one layer of glass glaze of coating in glass substrate；
D, glass substrate is finally integrally put into the high temperature oven high temperature preheated one-section time；High temperature oven temperature is 210 DEG C, in advance
The hot time is 14min；
E, glass substrate is finally integrally heated to fast cooling after softening point annealed finished product.
In the present embodiment, the glass glaze in step B and step C is completely the same, and its component includes boric acid 10 by weight
Part, 6 parts of ceramic powder, 4 parts of zirconium dioxide, 6 parts of silicon powder, 11 parts of titania powder, 8 parts of stalactite, 7 parts of chromium oxide, propylene
18 parts of acid resin, 4 parts of ethyl cellulose, 13 parts of aluminium nitride.
Example IV：
A kind of production method of environment-friendly type colored glazed glass, comprises the following steps：
A, by glass substrate surface deionized water rinsing, low temperature drying in low temperature baking oven is put into afterwards；Low temperature oven temperature is
45 DEG C, drying time is 8min；
B, one side one layer of glass glaze of coating in glass substrate, low temperature is put into after one layer of glass glaze is coated with after drying at room temperature
Dried in baking oven；
C, another side one layer of glass glaze of coating in glass substrate；
D, glass substrate is finally integrally put into the high temperature oven high temperature preheated one-section time；High temperature oven temperature is 200 DEG C, in advance
The hot time is 15min；
E, glass substrate is finally integrally heated to fast cooling after softening point annealed finished product.
In the present embodiment, the glass glaze in step B and step C is completely the same, and its component includes boric acid 9 by weight
Part, 8 parts of ceramic powder, 5 parts of zirconium dioxide, 10 parts of silicon powder, 8 parts of titania powder, 8 parts of stalactite, 8 parts of chromium oxide, propylene
15 parts of acid resin, 6 parts of ethyl cellulose, 10 parts of aluminium nitride.
Preparation method of the present invention is simple, and obtained colored glazed glass is indeformable, colour-fast, good environmental protection；Wherein, using general
Glass substrate is integrally put into the high temperature oven high temperature preheated one-section time；Temperature is 180 DEG C -220 DEG C, and preheating time is 10min-
20min.Ensure that colored glazed glass is used for a long time is not in glass glaze obscission.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (4)
1. a kind of production method of environment-friendly type colored glazed glass, it is characterised in that：Comprise the following steps：
A, by glass substrate surface deionized water rinsing, low temperature drying in low temperature baking oven is put into afterwards；
B, one side one layer of glass glaze of coating in glass substrate, low temperature is put into after one layer of glass glaze is coated with after drying at room temperature
Dried in baking oven；
C, another side one layer of glass glaze of coating in glass substrate；
D, glass substrate is finally integrally put into the high temperature oven high temperature preheated one-section time；
E, glass substrate is finally integrally heated to fast cooling after softening point annealed finished product.
2. a kind of production method of environment-friendly type colored glazed glass according to claim 1, it is characterised in that：The step B and
Glass glaze in step C is completely the same, and its component includes 5-12 parts of boric acid, 5-10 parts of ceramic powder, zirconium dioxide by weight
3-8 parts, 5-15 parts of silicon powder, 4-12 parts of titania powder, 5-10 parts of stalactite, 5-10 parts of chromium oxide, acrylic resin 10-
20 parts, 3-8 parts of ethyl cellulose, 4-15 parts of aluminium nitride.
3. a kind of production method of environment-friendly type colored glazed glass according to claim 1, it is characterised in that：In the step A
Low temperature oven temperature is 40 DEG C -50 DEG C, and drying time is 5min-10min.
4. a kind of production method of environment-friendly type colored glazed glass according to claim 1, it is characterised in that：In the step D
High temperature oven temperature is 180 DEG C -220 DEG C, and preheating time is 10min-20min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710363270.2A CN106977111A (en) | 2017-05-22 | 2017-05-22 | A kind of production method of environment-friendly type colored glazed glass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710363270.2A CN106977111A (en) | 2017-05-22 | 2017-05-22 | A kind of production method of environment-friendly type colored glazed glass |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106977111A true CN106977111A (en) | 2017-07-25 |
Family
ID=59342467
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710363270.2A Pending CN106977111A (en) | 2017-05-22 | 2017-05-22 | A kind of production method of environment-friendly type colored glazed glass |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106977111A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108640530A (en) * | 2018-08-01 | 2018-10-12 | 维达力实业(深圳)有限公司 | Cover sheet and its preparation method and application |
| CN110304835A (en) * | 2018-12-25 | 2019-10-08 | 深圳丽朴显像量子高科技有限公司 | A kind of glass display screen and its preparation process |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101704633A (en) * | 2009-05-14 | 2010-05-12 | 郑州恒昊玻璃技术有限公司 | Colored glazed glass and production method thereof |
| CN104513022A (en) * | 2013-09-26 | 2015-04-15 | 青岛市首胜实业有限公司 | Production method of enameled glass |
| CN105036557A (en) * | 2015-07-29 | 2015-11-11 | 无锡隆傲电子有限公司 | Ceramic glass glaze slurry and ceramic capacitor manufactured by using same |
-
2017
- 2017-05-22 CN CN201710363270.2A patent/CN106977111A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101704633A (en) * | 2009-05-14 | 2010-05-12 | 郑州恒昊玻璃技术有限公司 | Colored glazed glass and production method thereof |
| CN104513022A (en) * | 2013-09-26 | 2015-04-15 | 青岛市首胜实业有限公司 | Production method of enameled glass |
| CN105036557A (en) * | 2015-07-29 | 2015-11-11 | 无锡隆傲电子有限公司 | Ceramic glass glaze slurry and ceramic capacitor manufactured by using same |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108640530A (en) * | 2018-08-01 | 2018-10-12 | 维达力实业(深圳)有限公司 | Cover sheet and its preparation method and application |
| CN108640530B (en) * | 2018-08-01 | 2021-03-26 | 维达力实业(深圳)有限公司 | Protective cover plate and preparation method and application thereof |
| CN110304835A (en) * | 2018-12-25 | 2019-10-08 | 深圳丽朴显像量子高科技有限公司 | A kind of glass display screen and its preparation process |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170725 |
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