CN108486872A - A kind of inorganic agent preventing pure cotton textile pilling - Google Patents
A kind of inorganic agent preventing pure cotton textile pilling Download PDFInfo
- Publication number
- CN108486872A CN108486872A CN201810297430.2A CN201810297430A CN108486872A CN 108486872 A CN108486872 A CN 108486872A CN 201810297430 A CN201810297430 A CN 201810297430A CN 108486872 A CN108486872 A CN 108486872A
- Authority
- CN
- China
- Prior art keywords
- parts
- inorganic agent
- pure cotton
- cotton textile
- pilling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920000742 Cotton Polymers 0.000 title claims abstract description 72
- 239000004753 textile Substances 0.000 title claims abstract description 46
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 62
- 239000000843 powder Substances 0.000 claims abstract description 60
- 235000014676 Phragmites communis Nutrition 0.000 claims abstract description 39
- 239000010902 straw Substances 0.000 claims abstract description 39
- 239000004744 fabric Substances 0.000 claims abstract description 35
- 229920002689 polyvinyl acetate Polymers 0.000 claims abstract description 28
- 239000007788 liquid Substances 0.000 claims abstract description 26
- 239000011118 polyvinyl acetate Substances 0.000 claims abstract description 24
- 239000003381 stabilizer Substances 0.000 claims abstract description 19
- LHJQIRIGXXHNLA-UHFFFAOYSA-N calcium peroxide Chemical compound [Ca+2].[O-][O-] LHJQIRIGXXHNLA-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 13
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 13
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000008117 stearic acid Substances 0.000 claims abstract description 13
- -1 fatty acid sucrose ester Chemical class 0.000 claims abstract description 12
- 239000000341 volatile oil Substances 0.000 claims abstract description 12
- 239000004343 Calcium peroxide Substances 0.000 claims abstract description 9
- 241000723346 Cinnamomum camphora Species 0.000 claims abstract description 9
- 244000060011 Cocos nucifera Species 0.000 claims abstract description 9
- 235000013162 Cocos nucifera Nutrition 0.000 claims abstract description 9
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims abstract description 9
- 229930195725 Mannitol Natural products 0.000 claims abstract description 9
- 235000019402 calcium peroxide Nutrition 0.000 claims abstract description 9
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 9
- 239000000194 fatty acid Substances 0.000 claims abstract description 9
- 229930195729 fatty acid Natural products 0.000 claims abstract description 9
- 239000000835 fiber Substances 0.000 claims abstract description 9
- 239000000594 mannitol Substances 0.000 claims abstract description 9
- 235000010355 mannitol Nutrition 0.000 claims abstract description 9
- 229920000609 methyl cellulose Polymers 0.000 claims abstract description 9
- 239000001923 methylcellulose Substances 0.000 claims abstract description 9
- 229920000747 poly(lactic acid) Polymers 0.000 claims abstract description 9
- 239000004626 polylactic acid Substances 0.000 claims abstract description 9
- 239000002689 soil Substances 0.000 claims abstract description 9
- 239000002023 wood Substances 0.000 claims abstract description 9
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims abstract description 8
- 229930006000 Sucrose Natural products 0.000 claims abstract description 8
- 229960000846 camphor Drugs 0.000 claims abstract description 8
- 229930008380 camphor Natural products 0.000 claims abstract description 8
- 239000005720 sucrose Substances 0.000 claims abstract description 8
- ODLHGICHYURWBS-LKONHMLTSA-N trappsol cyclo Chemical compound CC(O)COC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](COCC(C)O)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](COCC(C)O)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](COCC(C)O)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](COCC(C)O)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)COCC(O)C)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1COCC(C)O ODLHGICHYURWBS-LKONHMLTSA-N 0.000 claims abstract description 7
- 238000009941 weaving Methods 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 24
- 238000006243 chemical reaction Methods 0.000 claims description 20
- 238000002360 preparation method Methods 0.000 claims description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 16
- 238000002156 mixing Methods 0.000 claims description 13
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 12
- 229910052757 nitrogen Inorganic materials 0.000 claims description 12
- 239000006228 supernatant Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 11
- 238000010790 dilution Methods 0.000 claims description 9
- 239000012895 dilution Substances 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 9
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 8
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 8
- 244000166124 Eucalyptus globulus Species 0.000 claims description 8
- 241000628997 Flos Species 0.000 claims description 8
- 240000000950 Hippophae rhamnoides Species 0.000 claims description 8
- 235000003145 Hippophae rhamnoides Nutrition 0.000 claims description 8
- 244000246386 Mentha pulegium Species 0.000 claims description 8
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 8
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 8
- 240000003152 Rhus chinensis Species 0.000 claims description 8
- 235000014220 Rhus chinensis Nutrition 0.000 claims description 8
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 8
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 8
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 8
- 238000007599 discharging Methods 0.000 claims description 8
- 235000019441 ethanol Nutrition 0.000 claims description 8
- 235000001050 hortel pimenta Nutrition 0.000 claims description 8
- 238000009413 insulation Methods 0.000 claims description 8
- 238000001556 precipitation Methods 0.000 claims description 8
- 239000000047 product Substances 0.000 claims description 8
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 claims description 8
- 239000000661 sodium alginate Substances 0.000 claims description 8
- 235000010413 sodium alginate Nutrition 0.000 claims description 8
- 229940005550 sodium alginate Drugs 0.000 claims description 8
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 7
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 7
- 238000004321 preservation Methods 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 4
- 239000001293 FEMA 3089 Substances 0.000 claims description 4
- 239000003814 drug Substances 0.000 claims description 4
- 238000004945 emulsification Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 239000004615 ingredient Substances 0.000 claims description 4
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 238000007670 refining Methods 0.000 claims description 4
- 238000010992 reflux Methods 0.000 claims description 4
- 229960004889 salicylic acid Drugs 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 4
- 239000000243 solution Substances 0.000 claims description 4
- BIFQHCGLXZWNLN-UHFFFAOYSA-N 2,2,6-trifluoro-4-methyl-4-propyl-1,3,5,2,4,6-trioxatrisilinane Chemical compound CCC[Si]1(C)O[SiH](F)O[Si](F)(F)O1 BIFQHCGLXZWNLN-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 229920001467 poly(styrenesulfonates) Polymers 0.000 claims description 3
- 239000002244 precipitate Substances 0.000 claims description 3
- 150000001412 amines Chemical class 0.000 claims description 2
- 239000000706 filtrate Substances 0.000 claims description 2
- 230000003993 interaction Effects 0.000 claims description 2
- 125000001844 prenyl group Chemical group [H]C([*])([H])C([H])=C(C([H])([H])[H])C([H])([H])[H] 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims 1
- 240000008821 Menyanthes trifoliata Species 0.000 claims 1
- 235000004443 Ricinus communis Nutrition 0.000 claims 1
- 210000004556 brain Anatomy 0.000 claims 1
- 238000005660 chlorination reaction Methods 0.000 claims 1
- 238000005374 membrane filtration Methods 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 238000000108 ultra-filtration Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 4
- 231100000252 nontoxic Toxicity 0.000 abstract description 4
- 230000003000 nontoxic effect Effects 0.000 abstract description 4
- 235000001674 Agaricus brunnescens Nutrition 0.000 abstract description 3
- 241000233866 Fungi Species 0.000 abstract description 3
- 239000000428 dust Substances 0.000 abstract description 3
- PNZOFKOTVXSWKQ-UHFFFAOYSA-N OCCC[Si]1(O[SiH2]O[SiH2]O1)C Chemical compound OCCC[Si]1(O[SiH2]O[SiH2]O1)C PNZOFKOTVXSWKQ-UHFFFAOYSA-N 0.000 description 4
- 238000002604 ultrasonography Methods 0.000 description 4
- 238000001914 filtration Methods 0.000 description 3
- 239000008236 heating water Substances 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- 229920000858 Cyclodextrin Polymers 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 229940059939 kayexalate Drugs 0.000 description 2
- CRVGTESFCCXCTH-UHFFFAOYSA-N methyl diethanolamine Chemical compound OCCN(C)CCO CRVGTESFCCXCTH-UHFFFAOYSA-N 0.000 description 2
- PZNOBXVHZYGUEX-UHFFFAOYSA-N n-prop-2-enylprop-2-en-1-amine;hydrochloride Chemical compound Cl.C=CCNCC=C PZNOBXVHZYGUEX-UHFFFAOYSA-N 0.000 description 2
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 2
- 230000037303 wrinkles Effects 0.000 description 2
- 206010067484 Adverse reaction Diseases 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 206010020112 Hirsutism Diseases 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 240000000111 Saccharum officinarum Species 0.000 description 1
- 235000007201 Saccharum officinarum Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000006838 adverse reaction Effects 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000009881 electrostatic interaction Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 210000004209 hair Anatomy 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920006389 polyphenyl polymer Polymers 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- BWYYYTVSBPRQCN-UHFFFAOYSA-M sodium;ethenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C=C BWYYYTVSBPRQCN-UHFFFAOYSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000007447 staining method Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/74—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon or graphite; with carbides; with graphitic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
- D06M15/09—Cellulose ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/507—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/35—Abrasion, pilling or fibrillation resistance
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of inorganic agent preventing pure cotton textile pilling, it is related to correlative technology field of weaving；The present invention prevents the inorganic agent component of pure cotton textile pilling from including；Camphor, stearic acid, volatile oil, Aloe Vera Gel, concavo-convex rod soil, ash wood, calper calcium peroxide, coconut fatty acid sucrose ester, Chu's bark powder, wingceltis bark powder, reed straw powder, stabilizer, hydroxypropyl beta cyclodextrin, polylactic acid, mannitol, modified polyvinyl acetate, herb liquid, methylcellulose；The present invention prevents the inorganic agent of pure cotton textile pilling, easy to use, safe and non-toxic, and has very high practicability, can cure wollen fabrics surface fiber and cotton yarn；Chu's bark powder, wingceltis bark powder, reed straw powder and herb liquid are added in inorganic agent, increases the adsorptivity of inorganic agent, effectively adsorbs dust, mushroom, inhibits fungus grown；Also it can soften wollen fabrics, keep wollen fabrics more soft, pro-skin, and pilling effect will not occur for worn for long periods.
Description
Technical field：
The present invention relates to weaving correlative technology fields, and in particular to a kind of inorganic agent preventing pure cotton textile pilling.
Background technology：
Pure cotton fabric be using cotton as raw material, by loom, by rise and fall in length and breadth through weft yarn be interweaved made of textile.
Pure cotton fabric fabric variety is various, and pattern is different.
Pure cotton fabric is made by purified cotton yarns, and fabric variety is various, and pattern is different.It can be divided into primary colors cotton by staining method
Cloth, dyed cotton fabric, chintz, yarn-dyed cotton fabric；Plain, twill, forging line cloth can also be divided by fabric structure.
Not by bleaching, dyeing and printing process processing, the cotton of the color and luster with natural cotton fiber is known as grey cotton fabric.It
Grew sheet, coarse cloth, fine cloth can be divided into according to the thickness of yarn count, they the characteristics of be：Body is thick and solid, cloth cover is smooth, durable, contracting
Water rate is larger.It can be used as sheeting, base auxiliary material or skyteens.
Cotton is the general name of all kinds of wollen fabrics.It is mostly used to manufacture fashionable dress, easy dress, underwear and shirt.Its strong point
It is easily warming, soft personal, hygroscopicity, gas permeability are favourable.Compared with chemical fibre, warmth retention property is good, hygroscopicity is strong, flexibility
There is no the adverse reactions such as electrostatic interaction for good and cotton fiber.But because cotton, flaxen fiber elasticity is weak, wrinkle resistance is poor, clothes
It simply wrinkles in wearing and scrubbing process, is not well-pressed, many inconveniences are brought in usual clothing is arranged to consumer.
Pure-cotton fabric also can pilling because pure-cotton fabric is also point several grades, best pure cotton is refined in cotton
Longest fiber be fabricated, after being handled by fluffing, good pure-cotton fabric surface has the suede of one layer of soft comfortable
Hair.The phenomenon that fabric of any surface hairiness, by friction, the wool fibre on surface can all intertwine, formation pilling.Pure cotton
Textile is no exception, in long-term wearing or in use, pilling effect occurs because often rubbing against.
Invention content：
The present invention is directed to above-mentioned pure cotton fabric pilling problem, provides a kind of inorganic agent preventing pure cotton textile pilling, this
Pure cotton textile pilling effect can be effectively relieved in invention inorganic agent, and can soften wollen fabrics, make wollen fabrics more
Pilling effect will not occur for softness, pro-skin, and worn for long periods, and inorganic agent can also play the role of restraining and sterilizing bacteria, present invention processing
Agent is easy to use, quick, safe and non-toxic.
It is realized using following technical scheme using the technical problems to be solved by the invention：
A kind of inorganic agent preventing pure cotton textile pilling, the inorganic agent include following mass fraction component：Camphor 11-
18 parts, 6-15 parts of stearic acid, 15-20 parts of volatile oil, 5-10 parts of Aloe Vera Gel, 10-20 parts of concavo-convex rod soil, 10-20 parts of ash wood,
5-8 parts of calper calcium peroxide, 1-9 parts of coconut fatty acid sucrose ester, 25-40 parts of Chu's bark powder, 23-35 parts of wingceltis bark powder, reed straw
5-12 parts of powder, 0.5-3 parts of stabilizer, 6-11 parts of hydroxypropylβ-cyclodextrin, 5-14 parts of polylactic acid, 20-30 parts of mannitol, modified vinegar
Sour polyethylene 6-13 parts, 20-30 parts of herb liquid, 3-15 parts of methylcellulose.
The wherein described herb liquid Chinese medicine includes：12-28 parts of Chinese gall, 13-32 parts of dark plum, 13-25 parts of sea-buckthorn, eucalyptus leaves
15-36 parts, 14-32 parts of bush, 9-28 parts of granatum, 8-37 parts of peppermint, 11-29 parts of flos caryophylli.
The wherein described stabilizer is made from the following raw materials in parts by weight：3-5 parts of acrylic acid, carboxymethyl cellulose 0.6-1.0
Part, 0.3-0.5 parts of trifluoro propyl methyl cyclotrisiloxane, 1.5-3 parts of sodium alginate, 0.2-2 parts of lauric monoglyceride, water
12-21 parts；The preparation method of stabilizer is that carboxymethyl cellulose is first added to the water stirring until being completely dissolved, and is then added third
Olefin(e) acid, sodium alginate and trifluoro propyl methyl cyclotrisiloxane 800-1000r/min stir 0.5-1h, are eventually adding remaining raw material
70-80 DEG C of reaction 2-4h, up to stabilizer after cooling.
The wherein described modified polyvinyl acetate preparation method is：The modified polyvinyl acetate be modified by polyvinyl acetate and
At method of modifying is：3-5 parts of turpentine oil, 0.5-1 parts of poly dimethyl allyls are added into 15-20 parts of polyvinyl acetates
Ammonium chloride, after being sufficiently mixed under microwave frequency 2450MHz, power 700W microwave treatment 5-30min, add 1-2 parts of hydrogenations
Castor oil, 0.5-1 part kayexalate and 0.5-1 parts of N methyldiethanol amines, continue microwave treatment after mixing
5min is transferred to sealing and standing 3h in 0-5 DEG C of environment after microwave treatment immediately, is then heated to 125-130 DEG C of heat preservation mixing
6-8 parts of 0-5 DEG C of cold water are added into gained mixture, 1h is stood after being sufficiently mixed, is then heated to reflux state by 10-30min
Heat preservation mixing 5-30min, after by mixture as rotation volatilize distilling machinery in, disperse extra volatile ingredient, rear natural cooling
It to room temperature, is finally sent into spray dryer, dry gained particle is modified polyvinyl acetate.
Chu's bark powder, wingceltis bark powder, the preparation method of reed straw powder are：
(1) it chooses without rotten, the high-quality Chu's bark of quality, wingceltis bark, reed straw, first by Chu's bark, wingceltis bark, reed straw
Stalk, which is positioned in 2-10% aqueous slkalis, impregnates 6-24h；
(2) Chu's bark after immersion, wingceltis bark, reed straw taking-up are placed in drying frame and drained away the water, after by Chu's bark, wingceltis
Bark, reed straw allow in dryer, 30-45 DEG C of baking 5-12h, until Chu's bark, wingceltis bark, reed straw moisture are 20%
Within；
(3) by Chu's bark, wingceltis bark, reed straw input pulverizer after, comminuted powder is within 200 mesh；
(4) Chu's bark, wingceltis bark, reed straw powder and essential oil input retort are sealed after, then retort is placed in water
In bath, under heating water bath to thermostatted water after 80-100 DEG C soften 1-3h to get Chu's bark powder, wingceltis bark powder used in the present invention,
Reed straw powder.
A kind of above-mentioned preparation method for the inorganic agent for preventing pure cotton textile pilling of the present invention, includes the following steps：
(1) good Chinese gall, dark plum, sea-buckthorn, eucalyptus leaves, bush, granatum, peppermint, flos caryophylli is selected to be added to 10
10-30min is boiled in big fire heating in times water, after switch to small fire and endure 12-24h slowly, postcooling to room temperature is stored at room temperature and precipitated
Night, after abandon precipitation supernatant 2000-3000rpm/min taken to centrifuge, abandon precipitation and take supernatant, it is 0.5-100 μm that rear supernatant, which carries out aperture,
Supermicro filtration membrane filters, and filtrate is taken to obtain herb liquid；
(2) 45-50% for taking above-mentioned herb liquid weight, with concavo-convex rod soil, ash wood, calper calcium peroxide, coconut fatty acid sugarcane
Sugar ester is added in the stearic acid of 7-8 times of mixture weight, 30-50 minutes ultrasonic, is sent into reaction kettle, is passed through nitrogen, is increased
Temperature is 60-97 DEG C, insulation reaction 35-40 hours, and product is filtered, washed 3-4 times with ethyl alcohol, is placed in 40-50 DEG C by discharging
It is dried to constant weight in baking oven, obtains material I；
(3) camphor, stearic acid, volatile oil, Aloe Vera Gel, Chu's bark powder, wingceltis bark powder, reed straw powder are mixed, is added
Enter into the salicylic acid of 3-5 times of mixture weight, it is 30-60 minutes ultrasonic, it is sent into reaction kettle, is passed through nitrogen, increasing temperature is
68-70 DEG C, product is filtered, is washed 3-4 times with ethyl alcohol, is placed in 70-80 DEG C of baking oven by insulation reaction 3.5-4 hours, discharging
Drying obtains material II to constant weight；
(4) stabilizer, hydroxypropylβ-cyclodextrin, mannitol are taken, is added in the polylactic acid of its weight 17-20%, stirring is mixed
It closes 20-30 minutes, the acetic acid solution of a concentration of 0.3-0.6mol/L is added dropwise, adjusting pH is 6.5-7.0, is passed through nitrogen, is heated to
25-35 DEG C of holding 30-60min, discharge to obtain material III；
(5) above-mentioned material I, material II, material III are mixed, is preheated 40-60 minutes at 27-35 DEG C, insulated and stirred 30-
It 40 minutes, is filtered to remove big impurity material and obtains inorganic agent basis bottom material；
(6) above-mentioned inorganic agent basis bottom material is mixed with remaining herb liquid, modified polyvinyl acetate, methylcellulose, is stirred
It mixes uniformly, homogeneous, emulsification preheats 25-35 DEG C, and heat refining 2-5h is up to inorganic agent.
The present invention prevents the inorganic agent application method of pure cotton textile pilling from being：
(1) the pure cotton textile prepared is first prewetted and is heated to 50-60 DEG C, humidity is maintained at 45-65%, and keeps the temperature
30-60min；
(2) inorganic agent by above-mentioned preparation is diluted with water, dilution ratio 2-5:10, and the dilution inorganic agent after dilution is added
Heat is to 60-80 DEG C；
(3) temperature control can be immersed in 50-60 DEG C of pure cotton textile in 60-80 DEG C of dilution inorganic agent after, or
Dilution inorganic agent is sprayed into rapidly pure cotton textile surrounded surface, keeps temperature, pure cotton textile and inorganic agent interaction 60-
120min, after by pure cotton textile taking-up room temperature be cooled to 25-30 DEG C；
(4) at room temperature, pure cotton textile is positioned on weaving friction machine, unfolds flat pure cotton textile surface and makes
Pure cotton textile further cures fabric fiber and cotton yarn.
The present invention prevents the inorganic agent advantages and beneficial effects of pure cotton textile pilling from being：
1, for the present invention for pure cotton textile there are problem, invention prevents the inorganic agent of pure cotton textile pilling, user
Just, safe and non-toxic, and there is very high practicability, wollen fabrics surface fiber and cotton yarn can be cured.
2, Chu's bark powder, wingceltis bark powder, reed is added in the inorganic agent for preventing pure cotton textile pilling prepared by the present invention
Straw powder and herb liquid can dramatically increase the adsorptivity of inorganic agent, effectively adsorb dust, mushroom, can inhibit fungus grown.
3, the inorganic agent for preventing pure cotton textile pilling prepared by the present invention can soften wollen fabrics, make wollen fabrics more
Pilling effect will not occur for softness, pro-skin, and worn for long periods.
Specific implementation mode：
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1：
A kind of children's towel eliminates the unusual smell inorganic agent；
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of inorganic agent preventing pure cotton textile pilling, the inorganic agent include following mass fraction component：Camphor 11
Part, 9 parts of stearic acid, 15 parts of volatile oil, 7 parts of Aloe Vera Gel, 13 parts of concavo-convex rod soil, 14 parts of ash wood, 5 parts of calper calcium peroxide, coconut
4 parts of fatty acid sucrose ester, 25 parts of Chu's bark powder, 23 parts of wingceltis bark powder, 5 parts of reed straw powder, 1.5 parts of stabilizer, hydroxypropyl beta-
8 parts of cyclodextrin, 12 parts of polylactic acid, 20 parts of mannitol, modified 6 parts of polyvinyl acetate, 20 parts of herb liquid, 13 parts of methylcellulose.
The wherein described herb liquid Chinese medicine includes：12 parts of Chinese gall, 15 parts of dark plum, 13 parts of sea-buckthorn, 17 parts of eucalyptus leaves, bush 14
Part, 9 parts of granatum, 21 parts of peppermint, 19 parts of flos caryophylli.
The wherein described stabilizer is made from the following raw materials in parts by weight：3 parts of acrylic acid, 0.6 part of carboxymethyl cellulose, trifluoro
0.3 part of hydroxypropyl methyl cyclotrisiloxane, 1.5 parts of sodium alginate, 1.2 parts of lauric monoglyceride, 12 parts of water；The preparation of stabilizer
Method is that carboxymethyl cellulose is first added to the water stirring until being completely dissolved, and acrylic acid, sodium alginate and trifluoro is then added
Hydroxypropyl methyl cyclotrisiloxane 1000r/min stirs 0.5h, is eventually adding 80 DEG C of reaction 3h of remaining raw material, stablizes to obtain the final product after cooling
Agent.
The wherein described modified polyvinyl acetate preparation method is：The modified polyvinyl acetate be modified by polyvinyl acetate and
At method of modifying is：3 parts of turpentine oil, 0.5 part of polydimethyl diallyl ammonium chloride are added into 15 parts of polyvinyl acetates,
After being sufficiently mixed under microwave frequency 2450MHz, power 700W microwave treatment 15min, add 2 parts of rilanit specials, 0.5 part
Kayexalate and 0.5 part of N methyldiethanol amine continue microwave treatment 5min, after microwave treatment after mixing
It is transferred to sealing and standing 3h in 0-5 DEG C of environment immediately, is then heated to 125 DEG C of heat preservation mixing 10min, is added into gained mixture
6 parts of 0-5 DEG C of cold water, stand 1h after being sufficiently mixed, be then heated to reflux state heat preservation mixing 10min, after by mixture as
In rotation volatilization distilling machinery, extra volatile ingredient is dispersed, rear cooled to room temperature is finally sent into spray dryer, is done
Dry gained particle is modified polyvinyl acetate.
Chu's bark powder, wingceltis bark powder, the preparation method of reed straw powder are：
(1) it chooses without rotten, the high-quality Chu's bark of quality, wingceltis bark, reed straw, first by Chu's bark, wingceltis bark, reed straw
Stalk, which is positioned in 5% aqueous slkali, impregnates 12h；
(2) Chu's bark after immersion, wingceltis bark, reed straw taking-up are placed in drying frame and drained away the water, after by Chu's bark, wingceltis
Bark, reed straw allow in dryer, 45 DEG C of baking 5h, until Chu's bark, wingceltis bark, reed straw moisture are within 20%；
(3) by Chu's bark, wingceltis bark, reed straw input pulverizer after, comminuted powder is within 200 mesh；
(4) Chu's bark, wingceltis bark, reed straw powder and essential oil input retort are sealed after, then retort is placed in water
Soften 2h in bath, under heating water bath to thermostatted water after 100 DEG C to get Chu's bark powder, wingceltis bark powder, reed straw used in the present invention
Stalk powder.
A kind of above-mentioned preparation method for the inorganic agent for preventing pure cotton textile pilling of the present invention, includes the following steps：
(1) good Chinese gall, dark plum, sea-buckthorn, eucalyptus leaves, bush, granatum, peppermint, flos caryophylli is selected to be added to 10
15min is boiled in big fire heating in times water, after switch to small fire and endure 12h slowly, postcooling to room temperature is stored at room temperature precipitates overnight, after abandon
Precipitation takes supernatant 2000rpm/min to centrifuge, and abandons precipitation and takes supernatant, it is that 0.5 μm of supermicro filtration membrane filters that rear supernatant, which carries out aperture, takes filter
Liquid obtains herb liquid；
(2) the 45% of above-mentioned herb liquid weight is taken, with concavo-convex rod soil, ash wood, calper calcium peroxide, coconut fatty acid sucrose
Ester is added in the stearic acid of 7 times of mixture weight, and ultrasound 30 minutes is sent into reaction kettle, and nitrogen is passed through, and is increased temperature and is
65 DEG C, product is filtered, is washed 3 times with ethyl alcohol by insulation reaction 35 hours, discharging, is placed in 40 DEG C of baking oven and is dried to constant weight,
Obtain material I；
(3) camphor, stearic acid, volatile oil, Aloe Vera Gel, Chu's bark powder, wingceltis bark powder, reed straw powder are mixed, is added
Entering into the salicylic acid of 3 times of mixture weight, ultrasound 30 minutes is sent into reaction kettle, and nitrogen is passed through, and it is 65 DEG C to increase temperature,
Insulation reaction 3.5 hours, discharging, product is filtered, is washed 3 times with ethyl alcohol, is placed in 70 DEG C of baking oven and is dried to constant weight, obtains object
Material II；
(4) stabilizer, hydroxypropylβ-cyclodextrin, mannitol are taken, is added in the polylactic acid of its weight 17%, is stirred 20
Minute, the acetic acid solution of a concentration of 0.3mol/L is added dropwise, it is 6.5 to adjust pH, is passed through nitrogen, is heated to 30 DEG C of holding 30min, goes out
Expect to obtain material III；
(5) above-mentioned material I, material II, material III are mixed, is preheated 40 minutes at 30 DEG C, insulated and stirred 30 minutes, mistake
It filters out big impurity material and obtains inorganic agent basis bottom material；
(6) above-mentioned inorganic agent basis bottom material is mixed with remaining herb liquid, modified polyvinyl acetate, methylcellulose, is stirred
It mixes uniformly, homogeneous, emulsification preheats 35 DEG C, and heat refining 2.5h is up to inorganic agent.
Embodiment 2：
A kind of children's towel eliminates the unusual smell inorganic agent；
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of inorganic agent preventing pure cotton textile pilling, the inorganic agent include following mass fraction component：Camphor 11
Part, 6 parts of stearic acid, 15 parts of volatile oil, 7 parts of Aloe Vera Gel, 14 parts of concavo-convex rod soil, 10 parts of ash wood, 6 parts of calper calcium peroxide, coconut
6 parts of fatty acid sucrose ester, 25 parts of Chu's bark powder, 23 parts of wingceltis bark powder, 5 parts of reed straw powder, 0.5 part of stabilizer, hydroxypropyl beta-
6 parts of cyclodextrin, 9 parts of polylactic acid, 20 parts of mannitol, modified 11 parts of polyvinyl acetate, 20 parts of herb liquid, 13 parts of methylcellulose.
The wherein described herb liquid Chinese medicine includes：12 parts of Chinese gall, 13 parts of dark plum, 15 parts of sea-buckthorn, 15 parts of eucalyptus leaves, bush 14
Part, 9 parts of granatum, 17 parts of peppermint, 11 parts of flos caryophylli.
The wherein described stabilizer is made from the following raw materials in parts by weight：3 parts of acrylic acid, 0.8 part of carboxymethyl cellulose, trifluoro
0.5 part of hydroxypropyl methyl cyclotrisiloxane, 1.5 parts of sodium alginate, 0.9 part of lauric monoglyceride, 14 parts of water；The preparation of stabilizer
Method is that carboxymethyl cellulose is first added to the water stirring until being completely dissolved, and acrylic acid, sodium alginate and trifluoro is then added
Hydroxypropyl methyl cyclotrisiloxane 1000r/min stirs 0.5h, is eventually adding 80 DEG C of reaction 4h of remaining raw material, stablizes to obtain the final product after cooling
Agent.
The wherein described modified polyvinyl acetate preparation method is：The modified polyvinyl acetate be modified by polyvinyl acetate and
At method of modifying is：5 parts of turpentine oil, 1 part of polydimethyl diallyl ammonium chloride are added into 15 parts of polyvinyl acetates, fills
Point mixing after under microwave frequency 2450MHz, power 700W microwave treatment 30min, add 2 parts of rilanit specials, 1 part of polyphenyl
Vinyl sulfonic acid sodium and 0.5 part of N methyldiethanol amine continue microwave treatment 5min after mixing, after microwave treatment immediately
It is transferred to sealing and standing 3h in 0-5 DEG C of environment, 125 DEG C of heat preservation mixing 30min is then heated to, 8 parts is added into gained mixture
0-5 DEG C of cold water, stands 1h after being sufficiently mixed, be then heated to reflux state heat preservation mixing 20min, after by mixture as rotation
It volatilizees in distilling machinery, disperses extra volatile ingredient, rear cooled to room temperature is finally sent into spray dryer, dry institute
It is modified polyvinyl acetate to obtain particle.
Chu's bark powder, wingceltis bark powder, the preparation method of reed straw powder are：
(1) it chooses without rotten, the high-quality Chu's bark of quality, wingceltis bark, reed straw, first by Chu's bark, wingceltis bark, reed straw
Stalk, which is positioned in 5% aqueous slkali, impregnates 14h；
(2) Chu's bark after immersion, wingceltis bark, reed straw taking-up are placed in drying frame and drained away the water, after by Chu's bark, wingceltis
Bark, reed straw allow in dryer, 45 DEG C of baking 9h, until Chu's bark, wingceltis bark, reed straw moisture are within 20%；
(3) by Chu's bark, wingceltis bark, reed straw input pulverizer after, comminuted powder is within 200 mesh；
(4) Chu's bark, wingceltis bark, reed straw powder and essential oil input retort are sealed after, then retort is placed in water
Soften 2h in bath, under heating water bath to thermostatted water after 100 DEG C to get Chu's bark powder, wingceltis bark powder, reed straw used in the present invention
Stalk powder.
A kind of above-mentioned preparation method for the inorganic agent for preventing pure cotton textile pilling of the present invention, includes the following steps：
(1) good Chinese gall, dark plum, sea-buckthorn, eucalyptus leaves, bush, granatum, peppermint, flos caryophylli is selected to be added to 10
15min is boiled in big fire heating in times water, after switch to small fire and endure 12h slowly, postcooling to room temperature is stored at room temperature precipitates overnight, after abandon
Precipitation takes supernatant 2000rpm/min to centrifuge, and abandons precipitation and takes supernatant, it is that 0.5 μm of supermicro filtration membrane filters that rear supernatant, which carries out aperture, takes filter
Liquid obtains herb liquid；
(2) the 45% of above-mentioned herb liquid weight is taken, with concavo-convex rod soil, ash wood, calper calcium peroxide, coconut fatty acid sucrose
Ester is added in the stearic acid of 7 times of mixture weight, and ultrasound 30 minutes is sent into reaction kettle, and nitrogen is passed through, and is increased temperature and is
60 DEG C, product is filtered, is washed 3 times with ethyl alcohol by insulation reaction 35 hours, discharging, is placed in 40 DEG C of baking oven and is dried to constant weight,
Obtain material I；
(3) camphor, stearic acid, volatile oil, Aloe Vera Gel, Chu's bark powder, wingceltis bark powder, reed straw powder are mixed, is added
Entering into the salicylic acid of 3 times of mixture weight, ultrasound 30 minutes is sent into reaction kettle, and nitrogen is passed through, and it is 68 DEG C to increase temperature,
Insulation reaction 3.5 hours, discharging, product is filtered, is washed 3 times with ethyl alcohol, is placed in 70 DEG C of baking oven and is dried to constant weight, obtains object
Material II；
(4) stabilizer, hydroxypropylβ-cyclodextrin, mannitol are taken, is added in the polylactic acid of its weight 17-20%, stirring is mixed
It closes 20 minutes, the acetic acid solution of a concentration of 0.4mol/L is added dropwise, it is 6.5 to adjust pH, is passed through nitrogen, is heated to 35 DEG C of holdings
30min, discharge to obtain material III；
(5) above-mentioned material I, material II, material III are mixed, is preheated 40 minutes at 30 DEG C, 30-40 points of insulated and stirred
Clock is filtered to remove big impurity material and obtains inorganic agent basis bottom material；
(6) above-mentioned inorganic agent basis bottom material is mixed with remaining herb liquid, modified polyvinyl acetate, methylcellulose, is stirred
It mixes uniformly, homogeneous, emulsification preheats 30 DEG C, and heat refining 2h is up to inorganic agent.
To carrying out experiment investigation in embodiment provided by the invention respectively, embodiment 1 and embodiment 2 prevent pure cotton textile
The inorganic agent detection project of pilling is investigated, and it is pair that anti-pilling inorganic agent processing of the present invention, which is not used, with common pure cotton textile
According to the results are shown in Table 1；
Table 1 investigates result
Pilling situation investigates experiment：The pure cotton fabric of same quality carries out identical dynamics (20-50N), phase in rubbing machine
It rubs with the time, observes pure cotton fabric pilling situation.
By the above results show that：
The present invention prevents the inorganic agent of pure cotton textile pilling, easy to use, safe and non-toxic, and has very high practicality
Property, wollen fabrics surface fiber and cotton yarn can be cured；Be added in inorganic agent Chu bark powder, wingceltis bark powder, reed straw powder and
Herb liquid can dramatically increase the adsorptivity of inorganic agent, effectively adsorb dust, mushroom, can inhibit fungus grown；Inorganic agent can soften
Wollen fabrics keep wollen fabrics more soft, pro-skin, and pilling effect will not occur for worn for long periods.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (3)
1. a kind of inorganic agent preventing pure cotton textile pilling, it is characterised in that：Inorganic agent includes following mass fraction component：Camphor tree
11-18 parts of brain, 6-15 parts of stearic acid, 15-20 parts of volatile oil, 5-10 parts of Aloe Vera Gel, 10-20 parts of concavo-convex rod soil, ash wood 10-
20 parts, 5-8 parts of calper calcium peroxide, 1-9 parts of coconut fatty acid sucrose ester, 25-40 parts of Chu's bark powder, 23-35 parts of wingceltis bark powder, reed
5-12 parts of straw powder, 6-11 parts of hydroxypropylβ-cyclodextrin, 5-14 parts of polylactic acid, 20-30 parts of mannitol, changes 0.5-3 parts of stabilizer
6-13 parts of polyvinyl acetate of property, 20-30 parts of herb liquid, 3-15 parts of methylcellulose；
The wherein described herb liquid Chinese medicine includes：12-28 parts of Chinese gall, 13-32 parts of dark plum, 13-25 parts of sea-buckthorn, eucalyptus leaves 15-36
Part, 14-32 parts of bush, 9-28 parts of granatum, 8-37 parts of peppermint, 11-29 parts of flos caryophylli；
The wherein described stabilizer is made from the following raw materials in parts by weight：3-5 parts of acrylic acid, 0.6-1.0 parts of carboxymethyl cellulose, three
0.3-0.5 parts of fluoropropyl methyl cyclotrisiloxane, 1.5-3 parts of sodium alginate, 0.2-2 parts of lauric monoglyceride, water 12-21
Part；The preparation method of stabilizer is that carboxymethyl cellulose is first added to the water stirring until be completely dissolved, be then added acrylic acid,
Sodium alginate and trifluoro propyl methyl cyclotrisiloxane 800-1000r/min stir 0.5-1h, are eventually adding remaining raw material 70-80
DEG C reaction 2-4h, it is cooling after up to stabilizer；
The wherein described modified polyvinyl acetate preparation method is：The modified polyvinyl acetate is modified by polyvinyl acetate,
Its method of modifying is：3-5 parts of turpentine oil, 0.5-1 parts of poly dimethyl allyl chlorinations are added into 15-20 parts of polyvinyl acetates
Ammonium, after being sufficiently mixed under microwave frequency 2450MHz, power 700W microwave treatment 5-30min, add 1-2 parts of hydrogenated castors
Oil, 0.5-1 parts of kayexalates and 0.5-1 parts of N methyldiethanol amines, continuation microwave treatment 5min, micro- after mixing
Wave after treatment is transferred to sealing and standing 3h in 0-5 DEG C of environment immediately, is then heated to 125-130 DEG C of heat preservation mixing 10-
6-8 parts of 0-5 DEG C of cold water are added into gained mixture, 1h is stood after being sufficiently mixed by 30min, are then heated to reflux state guarantor
Temperature mixing 5-30min, after by mixture as rotation volatilize distilling machinery in, disperse extra volatile ingredient, after naturally cool to
Room temperature is finally sent into spray dryer, and dry gained particle is modified polyvinyl acetate.
2. the inorganic agent according to claim 1 for preventing pure cotton textile pilling, it is characterised in that：Prevent pure cotton textile
The preparation method of the inorganic agent of pilling, includes the following steps：
(1) good Chinese gall, dark plum, sea-buckthorn, eucalyptus leaves, bush, granatum, peppermint, flos caryophylli is selected to be added to 10 times of water
10-30min is boiled in middle big fire heating, after switch to small fire and endure 12-24h slowly, postcooling to room temperature is stored at room temperature precipitates overnight, after
Abandoning precipitation takes supernatant 2000-3000rpm/min to centrifuge, and abandons precipitation and takes supernatant, it is 0.5-100 μm of ultra filtration that rear supernatant, which carries out aperture,
Membrane filtration takes filtrate to obtain herb liquid；
(2) 45-50% for taking above-mentioned herb liquid weight, and concavo-convex rod soil, ash wood, calper calcium peroxide, coconut fatty acid sucrose ester,
It is added in the stearic acid of 7-8 times of mixture weight, it is 30-50 minutes ultrasonic, it is sent into reaction kettle, is passed through nitrogen, increase temperature
It it is 60-97 DEG C, product is filtered, washed 3-4 times with ethyl alcohol, is placed in 40-50 DEG C of baking oven by insulation reaction 35-40 hours, discharging
Middle drying obtains material I to constant weight；
(3) camphor, stearic acid, volatile oil, Aloe Vera Gel, Chu's bark powder, wingceltis bark powder, reed straw powder are mixed, is added to
It is 30-60 minutes ultrasonic in the salicylic acid of 3-5 times of mixture weight, it is sent into reaction kettle, is passed through nitrogen, raising temperature is 68-70
DEG C, product is filtered, is washed 3-4 times with ethyl alcohol by insulation reaction 3.5-4 hours, discharging, is placed in 70-80 DEG C of baking oven dry
To constant weight, material II is obtained；
(4) stabilizer, hydroxypropylβ-cyclodextrin, mannitol are taken, is added in the polylactic acid of its weight 17-20%, is stirred 20-
30 minutes, the acetic acid solution of a concentration of 0.3-0.6mol/L is added dropwise, adjusting pH is 6.5-7.0, is passed through nitrogen, is heated to 25-35
DEG C keep 30-60min, discharge to obtain material III；
(5) above-mentioned material I, material II, material III are mixed, is preheated 40-60 minutes at 27-35 DEG C, 30-40 points of insulated and stirred
Clock is filtered to remove big impurity material and obtains inorganic agent basis bottom material；
(6) above-mentioned inorganic agent basis bottom material is mixed with remaining herb liquid, modified polyvinyl acetate, methylcellulose, stirring is equal
Even, homogeneous, emulsification preheats 25-35 DEG C, and heat refining 2-5h is up to inorganic agent.
3. the inorganic agent according to claim 1 for preventing pure cotton textile pilling, it is characterised in that：The present invention prevents pure cotton
The inorganic agent application method of textile pilling is：
(1) the pure cotton textile prepared is first prewetted and is heated to 50-60 DEG C, humidity is maintained at 45-65%, and keeps the temperature 30-
60min；
(2) inorganic agent by above-mentioned preparation is diluted with water, dilution ratio 2-5:10, and the dilution inorganic agent after dilution is heated to
60-80℃；
(3) temperature control can be immersed in 50-60 DEG C of pure cotton textile in 60-80 DEG C of dilution inorganic agent after, or will be dilute
It releases inorganic agent and sprays pure cotton textile surrounded surface rapidly, keep temperature, pure cotton textile and inorganic agent interaction 60-
120min, after by pure cotton textile taking-up room temperature be cooled to 25-30 DEG C；
(4) at room temperature, pure cotton textile is positioned on weaving friction machine, unfolds flat pure cotton textile surface and makes pure cotton
Textile further cures fabric fiber and cotton yarn.
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| CN201810297430.2A CN108486872A (en) | 2018-04-04 | 2018-04-04 | A kind of inorganic agent preventing pure cotton textile pilling |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810297430.2A CN108486872A (en) | 2018-04-04 | 2018-04-04 | A kind of inorganic agent preventing pure cotton textile pilling |
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| CN108486872A true CN108486872A (en) | 2018-09-04 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113089151A (en) * | 2021-04-07 | 2021-07-09 | 罗莱生活科技股份有限公司 | Three-dimensional antibacterial yarn containing cotton fibers, preparation method of three-dimensional antibacterial yarn and towel product |
| WO2022221057A1 (en) * | 2021-04-15 | 2022-10-20 | Terasaki Institute For Biomedical Innovation | Antimicrobial articles, methods of making and using same |
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| CN101545207A (en) * | 2009-04-01 | 2009-09-30 | 江南大学 | Anti-pilling finishing agent for pure cotton knitted fabrics and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113089151A (en) * | 2021-04-07 | 2021-07-09 | 罗莱生活科技股份有限公司 | Three-dimensional antibacterial yarn containing cotton fibers, preparation method of three-dimensional antibacterial yarn and towel product |
| CN113089151B (en) * | 2021-04-07 | 2022-06-17 | 罗莱生活科技股份有限公司 | Three-dimensional antibacterial yarn containing cotton fibers, preparation method of three-dimensional antibacterial yarn and towel product |
| WO2022221057A1 (en) * | 2021-04-15 | 2022-10-20 | Terasaki Institute For Biomedical Innovation | Antimicrobial articles, methods of making and using same |
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