CN104988741A - Fragrance easy-care treating method of cotton shirt - Google Patents
Fragrance easy-care treating method of cotton shirt Download PDFInfo
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- CN104988741A CN104988741A CN201510318482.XA CN201510318482A CN104988741A CN 104988741 A CN104988741 A CN 104988741A CN 201510318482 A CN201510318482 A CN 201510318482A CN 104988741 A CN104988741 A CN 104988741A
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- champignon
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- ironing
- ready
- mesoporous tio
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- 229920000742 Cotton Polymers 0.000 title claims abstract description 38
- 238000000034 method Methods 0.000 title claims abstract description 35
- 239000003205 fragrance Substances 0.000 title abstract description 17
- 239000002245 particle Substances 0.000 claims abstract description 53
- 239000000341 volatile oil Substances 0.000 claims abstract description 36
- 239000011347 resin Substances 0.000 claims abstract description 28
- 229920005989 resin Polymers 0.000 claims abstract description 28
- 238000001035 drying Methods 0.000 claims abstract description 23
- 239000007788 liquid Substances 0.000 claims abstract description 22
- 238000003825 pressing Methods 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000005406 washing Methods 0.000 claims abstract description 13
- 238000001816 cooling Methods 0.000 claims abstract description 11
- 238000007598 dipping method Methods 0.000 claims abstract description 6
- 235000001674 Agaricus brunnescens Nutrition 0.000 claims description 106
- 238000010409 ironing Methods 0.000 claims description 69
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 56
- 239000003054 catalyst Substances 0.000 claims description 38
- 239000012530 fluid Substances 0.000 claims description 37
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 30
- 239000000835 fiber Substances 0.000 claims description 27
- 241000196324 Embryophyta Species 0.000 claims description 21
- 125000003118 aryl group Chemical group 0.000 claims description 21
- 239000000243 solution Substances 0.000 claims description 21
- 239000003795 chemical substances by application Substances 0.000 claims description 20
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 17
- 229910052742 iron Inorganic materials 0.000 claims description 17
- 239000011814 protection agent Substances 0.000 claims description 15
- -1 softener Substances 0.000 claims description 15
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical group [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 14
- 239000002131 composite material Substances 0.000 claims description 12
- 230000008569 process Effects 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 10
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 claims description 8
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims description 8
- 239000000839 emulsion Substances 0.000 claims description 7
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 229920001296 polysiloxane Polymers 0.000 claims description 7
- 229920002635 polyurethane Polymers 0.000 claims description 7
- 239000004814 polyurethane Substances 0.000 claims description 7
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 239000002184 metal Substances 0.000 claims description 6
- 238000012545 processing Methods 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 6
- 238000006424 Flood reaction Methods 0.000 claims description 5
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims description 5
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims description 5
- 239000004113 Sepiolite Substances 0.000 claims description 5
- FPCJKVGGYOAWIZ-UHFFFAOYSA-N butan-1-ol;titanium Chemical compound [Ti].CCCCO.CCCCO.CCCCO.CCCCO FPCJKVGGYOAWIZ-UHFFFAOYSA-N 0.000 claims description 5
- 238000005352 clarification Methods 0.000 claims description 5
- 230000003750 conditioning effect Effects 0.000 claims description 5
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims description 5
- 238000012986 modification Methods 0.000 claims description 5
- 230000004048 modification Effects 0.000 claims description 5
- 239000003002 pH adjusting agent Substances 0.000 claims description 5
- 229920002689 polyvinyl acetate Polymers 0.000 claims description 5
- 239000011118 polyvinyl acetate Substances 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 238000002390 rotary evaporation Methods 0.000 claims description 5
- 229910052624 sepiolite Inorganic materials 0.000 claims description 5
- 235000019355 sepiolite Nutrition 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- 229920001817 Agar Polymers 0.000 claims description 4
- 241000207199 Citrus Species 0.000 claims description 4
- 239000008272 agar Substances 0.000 claims description 4
- 125000003368 amide group Chemical group 0.000 claims description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims description 4
- 125000002091 cationic group Chemical group 0.000 claims description 4
- 235000020971 citrus fruits Nutrition 0.000 claims description 4
- 229920001285 xanthan gum Polymers 0.000 claims description 4
- 239000011592 zinc chloride Substances 0.000 claims description 4
- 235000005074 zinc chloride Nutrition 0.000 claims description 4
- ONDPHDOFVYQSGI-UHFFFAOYSA-N zinc nitrate Chemical compound [Zn+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ONDPHDOFVYQSGI-UHFFFAOYSA-N 0.000 claims description 4
- NNTWKXKLHMTGBU-UHFFFAOYSA-N 4,5-dihydroxyimidazolidin-2-one Chemical compound OC1NC(=O)NC1O NNTWKXKLHMTGBU-UHFFFAOYSA-N 0.000 claims description 3
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 3
- 238000005576 amination reaction Methods 0.000 claims description 3
- 239000007853 buffer solution Substances 0.000 claims description 3
- 238000004132 cross linking Methods 0.000 claims description 3
- 239000003921 oil Substances 0.000 claims description 3
- 239000007981 phosphate-citrate buffer Substances 0.000 claims description 3
- 229920000570 polyether Polymers 0.000 claims description 3
- 229920005638 polyethylene monopolymer Polymers 0.000 claims description 3
- 235000019260 propionic acid Nutrition 0.000 claims description 3
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 239000007974 sodium acetate buffer Substances 0.000 claims description 3
- BHZOKUMUHVTPBX-UHFFFAOYSA-M sodium acetic acid acetate Chemical compound [Na+].CC(O)=O.CC([O-])=O BHZOKUMUHVTPBX-UHFFFAOYSA-M 0.000 claims description 3
- FYKDNWHPKQOZOT-UHFFFAOYSA-M sodium;dihydrogen phosphate;2-hydroxypropane-1,2,3-tricarboxylic acid Chemical compound [Na+].OP(O)([O-])=O.OC(=O)CC(O)(C(O)=O)CC(O)=O FYKDNWHPKQOZOT-UHFFFAOYSA-M 0.000 claims description 3
- XPFJYKARVSSRHE-UHFFFAOYSA-K trisodium;2-hydroxypropane-1,2,3-tricarboxylate;2-hydroxypropane-1,2,3-tricarboxylic acid Chemical compound [Na+].[Na+].[Na+].OC(=O)CC(O)(C(O)=O)CC(O)=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O XPFJYKARVSSRHE-UHFFFAOYSA-K 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 2
- 241000222519 Agaricus bisporus Species 0.000 claims 26
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 5
- 239000004408 titanium dioxide Substances 0.000 abstract description 4
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 244000251953 Agaricus brunnescens Species 0.000 description 80
- 239000004744 fabric Substances 0.000 description 22
- 239000003094 microcapsule Substances 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 4
- 238000009987 spinning Methods 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 3
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- 238000010792 warming Methods 0.000 description 3
- 238000009941 weaving Methods 0.000 description 3
- 238000011161 development Methods 0.000 description 2
- 238000002074 melt spinning Methods 0.000 description 2
- 235000019198 oils Nutrition 0.000 description 2
- 238000012805 post-processing Methods 0.000 description 2
- 238000004513 sizing Methods 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 239000004823 Reactive adhesive Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
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- 238000003490 calendering Methods 0.000 description 1
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- 239000004567 concrete Substances 0.000 description 1
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- 230000008020 evaporation Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000009992 mercerising Methods 0.000 description 1
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- 244000045947 parasite Species 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 238000009936 smoking Methods 0.000 description 1
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- 230000001954 sterilising effect Effects 0.000 description 1
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- 238000012360 testing method Methods 0.000 description 1
- 230000010148 water-pollination Effects 0.000 description 1
Landscapes
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a fragrance easy-care treating method of a cotton shirt. The method comprises dipping, primary pre-drying, liquid feeding, secondary pre-drying, pressing, baking, cooling, water washing drying and the like. First fragrance easy-care treating liquid and second fragrance easy-care treating liquid are used for treating a finished shirt respectively, through the steps of pressing, baking and the like, mesoporous titanium dioxide fragrance particles can be completely wrapped in easy-care resin, the mesoporous titanium dioxide fragrance particles slowly release fragrance under normal temperature and normal pressure, the absorption effect of a mesoporous titanium dioxide hole way can restrain essential oil volatilization loss, and fragrance retaining is complete.
Description
Technical field
The present invention relates to the post-processing approach of shirt, be specifically related to a kind of champignon no-iron treatment method of cotton shirt.
Background technology
Be mainly or all cotton fiber in the face liber composition of cotton shirt.Cotton fiber has good hygroscopicity, and under normal conditions, fiber can absorb moisture in peripherad air, and its moisture content is 8-10%, so the skin of its contact people, makes people feel soft and not stiff.If cotton humidity increases, environment temperature is higher, and the amount of moisture contained in fiber can all leave in evaporation, makes fabric keep water equilibrated state, makes people feel comfortable.Therefore, compared with chemical fiber plus material, cotton fabric shirt has excellent moisture absorbability and moisture retentivity.But along with the progress and development of society and improving constantly of people's living standard, contemporary clothes have been not only for hiding body, the warming and general decoration of work, but to high-qualityization, stylishization, comfortableization future development.
In order to give fabric lasting fragrance, conventional method has employing essence pad Final finishing, spices and spinning material melt spinning and adhere to the means such as microcapsules at textile surface.A kind of manufacture craft of aromatic fabrics is disclosed in CN 103556480A.Comprise the following steps: 1) prepare microencapsulated flavor; 2) weaving face fabric of the additional microencapsulated flavor of preparation, weaving face fabric selects Quality Pure Cotton Yarn Production, and this Quality Pure Cotton Yarn Production, after comb and parallel cotton fibers prior to spinning, spinning, sizing operation, uses reactive adhesive, softener, auxiliary agent to cement on cotton yarn by microencapsulated flavor; 3) fabric post processing, mainly comprise singe, destarch, dye fixing, wash, bake and bank up with earth, mercerising, calendering and finished product sizing.The method procedure arrangement is reasonable, is easy to implement, and obtained fabric has antibacterial expelling parasite, covering smell, the effect that makes body and mind comfortable, meets the demand of people to enjoying type, health fabric.A kind of fragrant body thermal fabric is disclosed in CN 102168335A, this fabric is obtained by weaving by fragrant body fiber and warming fabric fiber, described fragrant body fiber is obtained by spining technology by slow-release type microcapsule and synthetic fiber, and described warming fabric fiber adopts natural textile fibers.This fabric utilizes slow-release type microcapsule storing plant sesame oil and ensures its slow releasing, make this fabric can discharge natural plant fragrance when wearing, and by spining technology, slow-release type microcapsule is reasonably added in fabric fibre, improve mechanical strength and the fastness to washing of fabric.The character of microcapsules and its composition closely related, poor heat resistance, and spices and spinning material melt spinning gained fiber are chemical fibre, it is soft and smooth far away from cotton fiber to wear sense of touch, and above-mentioned reason limits the marketization of aromatic fabric to a certain extent.
Summary of the invention
The object of the invention is to overcome the defect existed in prior art, provide a kind of champignon no-iron treatment method of cotton shirt, cotton shirt free from extraneous odour, the environmental protection of the method process, fabric flatness is high and feel is smooth.
For realizing above-mentioned technique effect, technical scheme of the present invention is: a kind of champignon no-iron treatment method of cotton shirt, is characterized in that, comprise the steps:
S1: dipping, is immersed in ready-made clothes in the non-ironing treatment fluid of the first champignon with mesoporous TiO 2 champignon particle and fully floods;
S2: preliminary drying, puts into baking oven and carries out first time and be dried to 3 ~ 6 one-tenth in advance and do by the ready-made clothes after padding;
S3: upper liquid, the non-ironing treatment fluid of atomized spray second champignon, evenly applying the non-ironing treatment fluid of the second champignon to ready-made clothes liquid carrying rate to ready-made clothes is 50 ~ 80%;
S4: secondary preliminary drying, carries out secondary preliminary drying to upper liquid gained ready-made clothes, and pre-baked ready-made clothes is 5 ~ 9 one-tenth to be done;
S5: pressing, carries out pressing respectively to each position of secondary preliminary drying gained ready-made clothes;
S6: bake, bakes process to the ready-made clothes after pressing;
S7: cooling, proceeds in refrigerating chamber carry out cooling processing by baking the ready-made clothes after process;
S8: washing is dried, and obtains the non-ironing cotton shirt of champignon.
In order to ensure uniform at each position of shirt of champignon particle, make champignon particle can be embedded in fiber gap the fragrance that volatilizees lastingly, preferred technical scheme is, the component of the non-ironing treatment fluid of described first champignon comprises 5 ~ 25 parts, mesoporous TiO 2 champignon particle, polyvinyl acetate 5 ~ 40 parts, hydroxyethylcellulose 3 ~ 15 parts, no-ironing resin 20 ~ 50 parts, catalyst 2 ~ 10 parts, 200 ~ 400 parts, water;
Described mesoporous TiO 2 champignon particle is made up of the fixing embedding in the duct aromatic plant essential oil of mesoporous TiO 2, and the particle diameter of described mesoporous TiO 2 is 0.1 ~ 30 micron.
Non-ironing effect is had concurrently in order to make this cotton shirt, no-ironing resin is formed effectively coated to champignon particle, preferred technical scheme is, in the non-ironing treatment fluid of second champignon key component be no-ironing resin, fiber protection agent, softener, catalyst, PH conditioning agent, champignon particle adjust release agent and water, the parts by weight of key component are: no-ironing resin 52 ~ 118 parts, fiber protection agent 10 ~ 55 parts, softener 11 ~ 58 parts, catalyst 3 ~ 23 parts, champignon particle are adjusted and released agent 3 ~ 10 parts, 400 ~ 800 parts, water, and the pH value of the non-ironing treatment fluid of described second champignon is 5 ~ 6; Described fiber protection agent is be selected from least one in the silicone emulsion of elastic polyurethane and the common emulsion of oxidized polyethylene homopolymers and amido silicon oil; Described pH adjusting agent is be selected from the one in citric acid-sodium citrate buffer solution, acetic acid-sodium acetate buffer solution and sodium dihydrogen phosphate-citrate buffer solution, and described softener is be selected from least one containing in the amination polysiloxanes of polyether group and polyurethane-base cationic hydrophilic amido organosilicon softener.
In order to ensure that no-ironing resin adapts to the characteristic of cotton fiber, and ensure the hydrophily of resin, preferred technical scheme is, described no-ironing resin is be selected from least one in modification bishydroxymethyl dihydroxy ethylene urea, nano-dispersed self-crosslinking polyether-polyurethane, modified alkyl dihydroxy ethylene urea.
More stable in order to make aromatic essential oil embed in mesoporous TiO 2 duct, preferred technical scheme is, described mesoporous TiO 2 champignon particle is prepared from according to following steps:
Butyl titanate is joined in ethanol, leave standstill under 28 ~ 30 DEG C of conditions after stirring, every 10min by uncovered for solution placement 1min, solution has clarification to become muddy gradually, turbid solution is placed in the centrifugal 10 ~ 15min of centrifuge, by the product supersound washing in ethanol after centrifugal, obtain mesoporous TiO 2;
Be dissolved in ethanol by aromatic plant essential oil, add mesoporous TiO 2 wherein, the weight ratio of essential oil and mesoporous TiO 2 is 1:(2 ~ 4), stir 6h, rotary evaporation obtains mesoporous TiO 2 champignon particle.
In order to ensure that no-ironing resin is thoroughly crosslinked, microcapsules well can be coated on wherein, preferred technical scheme is, described catalyst is magnesium chloride, or is composite catalyst; Described composite catalyst is composited by metal salt catalyst and hydroxycarboxylic acid, described metal salt catalyst is be selected from least one in magnesium chloride, magnesium nitrate, zinc chloride, zinc nitrate, described hydroxycarboxylic acid is citric acid, dihydromethyl propionic acid, 2, at least one in 3-dyhydrobutanedioic acid, in described composite catalyst, the percentage by weight of metal salt catalyst is 50 ~ 60%.
In order to ensure that crosslinked thoroughly preferred technical scheme can also be no-ironing resin, and described baking temperature is 85 ~ 115 DEG C, described in bake the time be 20 ~ 50min.
In order to regulate aromatic essential oil from the release in mesoporous TiO 2 duct, preferred technical scheme is, described champignon particle is adjusted and released agent is be selected from least one in xanthans and agar.
In order to absorb the peculiar smell that wearer produces because of activities such as smokings, ensure that shirt fragrance is more complete, preferred technical scheme is, also containing 5 ~ 10 parts, Nano sepiolite powder end in the non-ironing treatment fluid of described second champignon.
Preferred technical scheme is, aromatic plant essential oil is be selected from the mixture of at least two kinds in citrus essential oil, flowers and plants class essential oil and wooden class essential oil.
Advantage of the present invention and beneficial effect are:
The present invention is processing with the non-ironing treatment fluid of the first champignon and the non-ironing treatment fluid of the second champignon respectively to shirt ready-made clothes, by steps such as pressing bake, mesoporous TiO 2 champignon particle can be coated in no-ironing resin completely, mesoporous TiO 2 champignon particle is stable at normal temperatures and pressures discharges fragrance slowly, and the suction-operated in mesoporous TiO 2 duct can suppress essential oil volatilization loss, fragrance retains complete;
Compared with conventional aromatic micro-capsule, mesoporous TiO 2 particle diameter is little, be coated in no-ironing resin, and titanium dioxide has uvioresistant and biocidal efficacies, and champignon shirt can be made to have uvioresistant and sterilizing function concurrently more easily by Final finishing is stable.
Detailed description of the invention
Below in conjunction with embodiment, the specific embodiment of the present invention is further described.Following examples only for technical scheme of the present invention is clearly described, and can not limit the scope of the invention with this.
Embodiment 1
The champignon no-iron treatment method of the cotton shirt of embodiment 1, comprises the steps:
S1: dipping, is immersed in ready-made clothes in the non-ironing treatment fluid of the first champignon with mesoporous TiO 2 champignon particle and fully floods;
S2: preliminary drying, puts into baking oven and carries out first time and be dried to 3 ~ 6 one-tenth in advance and do by the ready-made clothes after padding;
S3: upper liquid, the non-ironing treatment fluid of atomized spray second champignon, evenly applying the non-ironing treatment fluid of the second champignon to ready-made clothes liquid carrying rate to ready-made clothes is 50%;
S4: secondary preliminary drying, carries out secondary preliminary drying to upper liquid gained ready-made clothes, and pre-baked ready-made clothes is 5 ~ 9 one-tenth to be done;
S5: pressing, carries out pressing respectively to each position of secondary preliminary drying gained ready-made clothes;
S6: bake, bakes process to the ready-made clothes after pressing;
S7: cooling, proceeds in refrigerating chamber carry out cooling processing by baking the ready-made clothes after process;
S8: washing is dried, and obtains the non-ironing cotton shirt of champignon.
The component of the non-ironing treatment fluid of the first champignon comprises 5 parts, mesoporous TiO 2 champignon particle, polyvinyl acetate 5 parts, hydroxyethylcellulose 3 parts, no-ironing resin 20 parts, catalyst 2 parts, 200 parts, water;
Mesoporous TiO 2 champignon particle is made up of the fixing embedding in the duct aromatic plant essential oil of mesoporous TiO 2, and the particle diameter of mesoporous TiO 2 is 0.1 ~ 30 micron.
In the non-ironing treatment fluid of second champignon key component be no-ironing resin, fiber protection agent, softener, catalyst, PH conditioning agent, champignon particle adjust release agent and water, the parts by weight of key component are: no-ironing resin 52 parts, fiber protection agent 10 parts, softener 11 parts, catalyst 3 parts, champignon particle are adjusted and released agent 3 parts, 400 parts, water, and the pH value of the non-ironing treatment fluid of the second champignon is 5; Fiber protection agent is the silicone emulsion of elastic polyurethane; PH adjusting agent is citric acid-sodium citrate buffer solution, and softener is the amination polysiloxanes containing polyether group.
No-ironing resin is modification bishydroxymethyl dihydroxy ethylene urea.
Mesoporous TiO 2 champignon particle is prepared from according to following steps:
Butyl titanate is joined in ethanol, leave standstill under 28 DEG C of conditions after stirring, every 10min by uncovered for solution placement 1min, solution has clarification to become muddy gradually, turbid solution is placed in the centrifugal 10min of centrifuge, by the product supersound washing in ethanol after centrifugal, obtain mesoporous TiO 2;
Be dissolved in ethanol by aromatic plant essential oil, add mesoporous TiO 2 wherein, the weight ratio of essential oil and mesoporous TiO 2 is 1:2, and stir 6h, rotary evaporation obtains mesoporous TiO 2 champignon particle.
Catalyst is magnesium chloride; Baking temperature is 85 DEG C, and the time of baking is 20min.
Champignon particle is adjusted and released agent is xanthans.
Also containing 5 parts, Nano sepiolite powder end in the non-ironing treatment fluid of second champignon.
Aromatic plant essential oil is two kinds of mixing in citrus essential oil.
Embodiment 2
The champignon no-iron treatment method of embodiment 2 cotton shirt, comprises the steps:
S1: dipping, is immersed in ready-made clothes in the non-ironing treatment fluid of the first champignon with mesoporous TiO 2 champignon particle and fully floods;
S2: preliminary drying, puts into baking oven and carries out first time and be dried to 6 one-tenth in advance and do by the ready-made clothes after padding;
S3: upper liquid, the non-ironing treatment fluid of atomized spray second champignon, evenly applying the non-ironing treatment fluid of the second champignon to ready-made clothes liquid carrying rate to ready-made clothes is 80%;
S4: secondary preliminary drying, carries out secondary preliminary drying to upper liquid gained ready-made clothes, and pre-baked ready-made clothes is 9 one-tenth to be done;
S5: pressing, carries out pressing respectively to each position of secondary preliminary drying gained ready-made clothes;
S6: bake, bakes process to the ready-made clothes after pressing;
S7: cooling, proceeds in refrigerating chamber carry out cooling processing by baking the ready-made clothes after process;
S8: washing is dried, and obtains the non-ironing cotton shirt of champignon.
The component of the non-ironing treatment fluid of the first champignon comprises 25 parts, mesoporous TiO 2 champignon particle, polyvinyl acetate 40 parts, hydroxyethylcellulose 15 parts, no-ironing resin 50 parts, catalyst 10 parts, 400 parts, water;
Mesoporous TiO 2 champignon particle is made up of the fixing embedding in the duct aromatic plant essential oil of mesoporous TiO 2, and the particle diameter of mesoporous TiO 2 is 0.1 ~ 30 micron.
In the non-ironing treatment fluid of second champignon key component be no-ironing resin, fiber protection agent, softener, catalyst, PH conditioning agent, champignon particle adjust release agent and water, the parts by weight of key component are: no-ironing resin 118 parts, fiber protection agent 55 parts, softener 58 parts, catalyst 23 parts, champignon particle are adjusted and released agent 10 parts, 800 parts, water, and the pH value of the non-ironing treatment fluid of the second champignon is 6; Fiber protection agent is the common emulsion of oxidized polyethylene homopolymers and amido silicon oil; PH adjusting agent is acetic acid-sodium acetate buffer solution, and softener is polyurethane-base cationic hydrophilic amido organosilicon softener.
No-ironing resin is nano-dispersed self-crosslinking polyether-polyurethane.
Mesoporous TiO 2 champignon particle is prepared from according to following steps:
Butyl titanate is joined in ethanol, leave standstill under 30 DEG C of conditions after stirring, every 10min by uncovered for solution placement 1min, solution has clarification to become muddy gradually, turbid solution is placed in the centrifugal 15min of centrifuge, by the product supersound washing in ethanol after centrifugal, obtain mesoporous TiO 2;
Be dissolved in ethanol by aromatic plant essential oil, add mesoporous TiO 2 wherein, the weight ratio of essential oil and mesoporous TiO 2 is 1:4, and stir 6h, rotary evaporation obtains mesoporous TiO 2 champignon particle.
Catalyst is for being composite catalyst; Composite catalyst magnesium chloride and dihydromethyl propionic acid composition, in composite catalyst, the percentage by weight of magnesium chloride is 50%.
Institute's baking temperature is 115 DEG C, and the time of baking is 50min.
Champignon particle is adjusted and released agent is agar.
Also containing 10 parts, Nano sepiolite powder end in the non-ironing treatment fluid of second champignon.
Aromatic plant essential oil is the mixture being selected from citrus essential oil and flowers and plants class essential oil.
Embodiment 3
The champignon no-iron treatment method of embodiment 3 cotton shirt, comprises the steps:
S1: dipping, is immersed in ready-made clothes in the non-ironing treatment fluid of the first champignon with mesoporous TiO 2 champignon particle and fully floods;
S2: preliminary drying, puts into baking oven and carries out first time and be dried to 4 one-tenth in advance and do by the ready-made clothes after padding;
S3: upper liquid, the non-ironing treatment fluid of atomized spray second champignon, evenly applying the non-ironing treatment fluid of the second champignon to ready-made clothes liquid carrying rate to ready-made clothes is 65%;
S4: secondary preliminary drying, carries out secondary preliminary drying to upper liquid gained ready-made clothes, and pre-baked ready-made clothes is 5 ~ 9 one-tenth to be done;
S5: pressing, carries out pressing respectively to each position of secondary preliminary drying gained ready-made clothes;
S6: bake, bakes process to the ready-made clothes after pressing;
S7: cooling, proceeds in refrigerating chamber carry out cooling processing by baking the ready-made clothes after process;
S8: washing is dried, and obtains the non-ironing cotton shirt of champignon.
The component of the non-ironing treatment fluid of the first champignon comprises 15 parts, mesoporous TiO 2 champignon particle, polyvinyl acetate 22 parts, hydroxyethylcellulose 9 parts, no-ironing resin 35 parts, catalyst 6 parts, 300 parts, water;
Mesoporous TiO 2 champignon particle is made up of the fixing embedding in the duct aromatic plant essential oil of mesoporous TiO 2, and the particle diameter of mesoporous TiO 2 is 0.1 ~ 30 micron.
In the non-ironing treatment fluid of second champignon key component be no-ironing resin, fiber protection agent, softener, catalyst, PH conditioning agent, champignon particle adjust release agent and water, the parts by weight of key component are: no-ironing resin 85 parts, fiber protection agent 32 parts, softener 11 ~ 58 parts, catalyst 13 parts, champignon particle are adjusted and released agent 7 parts, 600 parts, water, and the pH value of the non-ironing treatment fluid of the second champignon is 5.5; Fiber protection agent is the silicone emulsion of elastic polyurethane; PH adjusting agent is sodium dihydrogen phosphate-citrate buffer solution, and softener is polyurethane-base cationic hydrophilic amido organosilicon softener.
No-ironing resin is modified alkyl dihydroxy ethylene urea.
Mesoporous TiO 2 champignon particle is prepared from according to following steps:
Butyl titanate is joined in ethanol, leave standstill under 29 DEG C of conditions after stirring, every 10min by uncovered for solution placement 1min, solution has clarification to become muddy gradually, turbid solution is placed in the centrifugal 12min of centrifuge, by the product supersound washing in ethanol after centrifugal, obtain mesoporous TiO 2;
Be dissolved in ethanol by aromatic plant essential oil, add mesoporous TiO 2 wherein, the weight ratio of essential oil and mesoporous TiO 2 is 1:3, and stir 6h, rotary evaporation obtains mesoporous TiO 2 champignon particle.
Catalyst is composite catalyst; Composite catalyst is formed by magnesium nitrate, zinc chloride and citric acid in combination, and in composite catalyst, the weight sum percentage of magnesium nitrate, zinc chloride is 55%.
Baking temperature is 100 DEG C, and the time of baking is 35min.
Champignon particle is adjusted and released agent is be selected from least one in xanthans and agar.
Also containing 8 parts, Nano sepiolite powder end in the non-ironing treatment fluid of second champignon.
Aromatic plant essential oil is the mixture of flowers and plants class essential oil and wooden class essential oil.
Prove through test, the champignon cotton shirt of embodiment 1-3 can maintain fragrance and reach nearly a year and a half, still has fragrance after washing 40 times.And the persistence of fragrance is also relevant with the concrete kind of the aromatic essential oil selected.
The pressure of one square centimeter that pressing pressure: 1kg refers to.1kg/cm
2=9.8N/cm
2
Liquid carrying rate, also known as pick-up, pick-up rate is the number of webbing liquid measure after mangle.
Liquid carrying rate computing formula is: fabric heavy * 100% before pick-up rate=(after mangle before fabric weight-mangle fabric weight)/mangle
The representation of a few Cheng Gan refers to that the amount of moisture that band liquid ready-made clothes has dried accounts for the one-tenth number that should dry the component that anhydrates when being dried to dry ready-made clothes.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (10)
1. a champignon no-iron treatment method for cotton shirt, is characterized in that, comprise the steps:
S1: dipping, is immersed in ready-made clothes in the non-ironing treatment fluid of the first champignon with mesoporous TiO 2 champignon particle and fully floods;
S2: preliminary drying, puts into baking oven and carries out first time and be dried to 3 ~ 6 one-tenth in advance and do by the ready-made clothes after padding;
S3: upper liquid, the non-ironing treatment fluid of atomized spray second champignon, evenly applying the non-ironing treatment fluid of the second champignon to ready-made clothes liquid carrying rate to ready-made clothes is 50 ~ 80%;
S4: secondary preliminary drying, carries out secondary preliminary drying to upper liquid gained ready-made clothes, and pre-baked ready-made clothes is 5 ~ 9 one-tenth to be done;
S5: pressing, carries out pressing respectively to each position of secondary preliminary drying gained ready-made clothes;
S6: bake, bakes process to the ready-made clothes after pressing;
S7: cooling, proceeds in refrigerating chamber carry out cooling processing by baking the ready-made clothes after process;
S8: washing is dried, and obtains the non-ironing cotton shirt of champignon.
2. the champignon no-iron treatment method of cotton shirt according to claim 1, it is characterized in that, the component of the non-ironing treatment fluid of described first champignon comprises 5 ~ 25 parts, mesoporous TiO 2 champignon particle, polyvinyl acetate 5 ~ 40 parts, hydroxyethylcellulose 3 ~ 15 parts, no-ironing resin 20 ~ 50 parts, catalyst 2 ~ 10 parts, 200 ~ 400 parts, water;
Described mesoporous TiO 2 champignon particle is made up of the fixing embedding in the duct aromatic plant essential oil of mesoporous TiO 2, and the particle diameter of described mesoporous TiO 2 is 0.1 ~ 30 micron.
3. the champignon no-iron treatment method of cotton shirt according to claim 2, it is characterized in that, in the non-ironing treatment fluid of second champignon key component be no-ironing resin, fiber protection agent, softener, catalyst, PH conditioning agent, champignon particle adjust release agent and water, the parts by weight of key component are: no-ironing resin 52 ~ 118 parts, fiber protection agent 10 ~ 55 parts, softener 11 ~ 58 parts, catalyst 3 ~ 23 parts, champignon particle are adjusted and released agent 3 ~ 10 parts, 400 ~ 800 parts, water, and the pH value of the non-ironing treatment fluid of described second champignon is 5 ~ 6; Described fiber protection agent is be selected from least one in the silicone emulsion of elastic polyurethane and the common emulsion of oxidized polyethylene homopolymers and amido silicon oil; Described pH adjusting agent is be selected from the one in citric acid-sodium citrate buffer solution, acetic acid-sodium acetate buffer solution and sodium dihydrogen phosphate-citrate buffer solution, and described softener is be selected from least one containing in the amination polysiloxanes of polyether group and polyurethane-base cationic hydrophilic amido organosilicon softener.
4. the champignon no-iron treatment method of the cotton shirt according to Claims 2 or 3, it is characterized in that, described no-ironing resin is be selected from least one in modification bishydroxymethyl dihydroxy ethylene urea, nano-dispersed self-crosslinking polyether-polyurethane, modified alkyl dihydroxy ethylene urea.
5. the champignon no-iron treatment method of cotton shirt according to claim 2, is characterized in that, described mesoporous TiO 2 champignon particle is prepared from according to following steps:
Butyl titanate is joined in ethanol, leave standstill under 28 ~ 30 DEG C of conditions after stirring, every 10min by uncovered for solution placement 1min, solution has clarification to become muddy gradually, turbid solution is placed in the centrifugal 10 ~ 15min of centrifuge, by the product supersound washing in ethanol after centrifugal, obtain mesoporous TiO 2;
Be dissolved in ethanol by aromatic plant essential oil, add mesoporous TiO 2 wherein, the weight ratio of essential oil and mesoporous TiO 2 is 1:(2 ~ 4), stir 6h, rotary evaporation obtains mesoporous TiO 2 champignon particle.
6. the champignon no-iron treatment method of the cotton shirt according to Claims 2 or 3, is characterized in that, described catalyst is magnesium chloride, or is composite catalyst; Described composite catalyst is composited by metal salt catalyst and hydroxycarboxylic acid, described metal salt catalyst is be selected from least one in magnesium chloride, magnesium nitrate, zinc chloride, zinc nitrate, described hydroxycarboxylic acid is citric acid, dihydromethyl propionic acid, 2, at least one in 3-dyhydrobutanedioic acid, in described composite catalyst, the percentage by weight of metal salt catalyst is 50 ~ 60%.
7. the champignon no-iron treatment method of cotton shirt according to claim 1, is characterized in that, described baking temperature is 85 ~ 115 DEG C, described in bake the time be 20 ~ 50min.
8. the champignon no-iron treatment method of cotton shirt according to claim 3, is characterized in that, described champignon particle is adjusted and released agent is be selected from least one in xanthans and agar.
9. the champignon no-iron treatment method of cotton shirt according to claim 3, is characterized in that, also containing 5 ~ 10 parts, Nano sepiolite powder end in the non-ironing treatment fluid of described second champignon.
10. the champignon no-iron treatment method of cotton shirt according to claim 2, is characterized in that, described aromatic plant essential oil is be selected from the mixture of at least two kinds in citrus essential oil, flowers and plants class essential oil and wooden class essential oil.
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| EP3409832A1 (en) * | 2017-06-02 | 2018-12-05 | AVA-organic ep.mode GmbH | Method and device for the treatment of textiles made from fibres, and textiles made of natural or synthetic fibres |
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| CN111849336A (en) * | 2020-08-26 | 2020-10-30 | 长沙三思新材料科技有限公司 | Odorless aromatic two-component waterborne polyurethane coating |
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| CN110761068B (en) * | 2019-12-03 | 2022-05-10 | 福建省晋江新德美化工有限公司 | Low-strength-loss high-performance environment-friendly non-ironing finishing method for cotton fabric |
| CN111849336A (en) * | 2020-08-26 | 2020-10-30 | 长沙三思新材料科技有限公司 | Odorless aromatic two-component waterborne polyurethane coating |
| CN116427179A (en) * | 2023-04-27 | 2023-07-14 | 江苏阳光集团有限公司 | Microcapsule aromatherapy ready-made garment non-ironing shirt |
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