CN109826005A - A kind of antibacterial fabric finishing method of moisture absorbing and sweat releasing - Google Patents
A kind of antibacterial fabric finishing method of moisture absorbing and sweat releasing Download PDFInfo
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- CN109826005A CN109826005A CN201910081926.0A CN201910081926A CN109826005A CN 109826005 A CN109826005 A CN 109826005A CN 201910081926 A CN201910081926 A CN 201910081926A CN 109826005 A CN109826005 A CN 109826005A
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- moisture absorbing
- sweat releasing
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- finishing method
- antibacterial
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Abstract
The invention discloses a kind of antibacterial fabric finishing methods of moisture absorbing and sweat releasing, it arranges dacron by synthesis moisture control agent to improve its moisture absorbing and sweat releasing performance, it is obviously improved in moisture absorbing and sweat releasing performance by the fabric after handled by self-control finishing fluid, solve the problems, such as that the moisture absorbing and sweat releasing performance of polyester fiber is poor, and improve the anti-microbial property of fabric, so that fabric is especially when being made as sportswear used in hot summer, because being difficult to perspire, heat extraction, bacterium etc. is bred, enables a wearer to lead to the problem of feeling of oppression and heat and smelly.
Description
Technical field
The invention belongs to fabric printing technical fields, and in particular to a kind of antibacterial fabric finishing method of moisture absorbing and sweat releasing.
Background technique
It is most of to have hydrophily poor, it is difficult to quickly in our some traditional, common synthetic fibers used in everyday
The disadvantages of moisture absorption, these disadvantages perhaps do not protrude in people's Working Life usually, but once when human body carry out it is violent
When movement, the secretion sweat and a large amount of heat that the sweat gland on skin can accelerate, and surface skin is volatilized at this moment
Aqueous vapor out is but difficult by these fibers adsorptions and quickly exhales from fabric surface, therefore holds very much in this case
Discomfort that is sultry, being stained with body is easily generated during exercise.
Although also possessing excellent sucting wet air permeability there are also pure cotton product in common fabric, theoretically for can also be with
Good comfort is brought while movement to people, but this kind of pure cotton fabric is some other especially crease-resistant in nature
Conformality and transmissibility are very poor, and the rate that fabric itself is dried is very slow, so when pure cotton fabric largely absorbs water simultaneously
And phenomenon will be expanded when moisture absorption (water) excess, to can still generate the problems such as sultry.
The porous and big surface area of fabric is easy to adhere to pathogen, and sweat and the scurf of aging of human secretory etc. give disease
Opportunistic pathogen provides nutriment abundant, it is suitable under the conditions of microbes index increase, common fabric cannot prevent invading for pathogen
Enter, threaten the health of human body and brings offending smell.
Summary of the invention
The purpose of this section is to summarize some aspects of the embodiment of the present invention and briefly introduce some preferable implementations
Example.It may do a little simplified or be omitted to avoid our department is made in this section and the description of the application and the title of the invention
Point, the purpose of abstract of description and denomination of invention it is fuzzy, and this simplification or omit and cannot be used for limiting the scope of the invention.
In view of above-mentioned technological deficiency, the present invention is proposed.
Therefore, as one aspect of the present invention, the present invention overcomes the deficiencies in the prior art, provides a kind of suction
The wet antibacterial fabric finishing method perspired.
In order to solve the above technical problems, the present invention provides the following technical scheme that
A kind of antibacterial fabric finishing method of moisture absorbing and sweat releasing comprising: triethylamine, chloropropene, ethyl acetate, stirring is added
Heating, revolving；With acetone washing, decompression is filtered, and obtains product 1；Trimethoxy silane and isopropanol mixture is added, stirring adds
Heat；Platinum catalyst is added, after isothermal reaction, vacuum distillation；Ethyl acetate solution, freeze overnight, vacuum filtration is added；Add water,
AgNO is added3, obtain solution 1；Fabric is immersed in soda bath, concussion is dried after cleaning；The fabric is immersed into the solution
In 1, drying；The fabric is immersed in NaOH solution, dries, bake, clean and dries.
A kind of preferred embodiment of antibacterial fabric finishing method as moisture absorbing and sweat releasing of the present invention: the triethylamine, chlorine
The molar ratio of propylene is 1:3；The molar ratio of the trimethoxy silane and product 1 is 1:1.
A kind of preferred embodiment of antibacterial fabric finishing method as moisture absorbing and sweat releasing of the present invention: the soda bath is dense
Degree is 20g/L；The AgNO3Solution concentration is 0.1mol/L；The NaOH solution concentration is 0.1mol/L.
A kind of preferred embodiment of antibacterial fabric finishing method as moisture absorbing and sweat releasing of the present invention: three second of the addition
Amine, chloropropene, ethyl acetate, agitating and heating, revolving, being heated to temperature is 30 DEG C；The addition trimethoxy silane and different
Propanol mixture, agitating and heating, being heated to temperature is 70 DEG C.
A kind of preferred embodiment of antibacterial fabric finishing method as moisture absorbing and sweat releasing of the present invention: the addition platinum catalysis
Agent, after isothermal reaction, vacuum distillation, temperature is 70 DEG C, reaction time 3h.
A kind of preferred embodiment of antibacterial fabric finishing method as moisture absorbing and sweat releasing of the present invention: described by the fabric
It immerses in the solution 1, dries, impregnation method is that three leachings three are rolled, pick-up 100%；Its drying condition is 90 DEG C, the time
For 5min.
A kind of preferred embodiment of antibacterial fabric finishing method as moisture absorbing and sweat releasing of the present invention: described to immerse fabric
In soda bath, concussion is dried after cleaning, and concussion temperature is 90 DEG C, and the concussion time is 1h, is dried after cleaning, temperature is
60℃。
A kind of preferred embodiment of antibacterial fabric finishing method as moisture absorbing and sweat releasing of the present invention: described by the fabric
It is immersed in NaOH solution, dries, bakes, cleans and dry, it is 5min that the time is immersed in NaOH solution, and drying temperature is
100 DEG C, drying time 10min, baking temperature is 160 DEG C, and baking the time is 5min, and cleaning way is that ultrasound is clear
It washes, scavenging period 5min, drying temperature is 100 DEG C, drying time 30min.
As another aspect of the present invention, the present invention overcomes the deficiencies in the prior art, provides the moisture absorption row
The antibiotic fabric of moisture absorbing and sweat releasing is made in the antibacterial fabric finishing method of sweat.
In order to solve the above technical problems, the present invention provides the following technical scheme that with the antibiotic fabric of the moisture absorbing and sweat releasing
Method for sorting be made moisture absorbing and sweat releasing antibiotic fabric, in which: the antibiotic fabric water droplet of moisture absorbing and sweat releasing spread completely used in the time be
59s, moisture evaporating completely time can be down to 19 ' 34.
A kind of preferred embodiment of antibiotic fabric as moisture absorbing and sweat releasing obtained, in which: the antibacterial of the moisture absorbing and sweat releasing is knitted
The antibiotic rate of object is 99.7%.
Beneficial effects of the present invention: the present invention arranges dacron by synthesis moisture control agent to improve
Its moisture absorbing and sweat releasing performance is obviously improved in moisture absorbing and sweat releasing performance by the fabric after handled by self-control finishing fluid,
It solves the problems, such as that the moisture absorbing and sweat releasing performance of polyester fiber is poor, and improves the anti-microbial property of fabric, so that fabric is especially
When being made as sportswear used in hot summer, because being difficult to perspire, heat extraction, growth bacterium etc. enables a wearer to generate
Feeling of oppression and heat and smelly problem.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, required use in being described below to embodiment
Attached drawing be briefly described, it should be apparent that, drawings in the following description are only some embodiments of the invention, for this
For the those of ordinary skill of field, without any creative labor, it can also be obtained according to these attached drawings other
Attached drawing.Wherein:
Fig. 1 is preparation flow of the invention.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, right combined with specific embodiments below
A specific embodiment of the invention is described in detail.
In the following description, numerous specific details are set forth in order to facilitate a full understanding of the present invention, but the present invention can be with
Implemented using other than the one described here other way, those skilled in the art can be without prejudice to intension of the present invention
In the case of do similar popularization, therefore the present invention is not limited by the specific embodiments disclosed below.
Secondly, " one embodiment " or " embodiment " referred to herein, which refers to, may be included at least one realization side of the invention
A particular feature, structure, or characteristic in formula." in one embodiment " that different places occur in the present specification not refers both to
The same embodiment, nor the individual or selective embodiment mutually exclusive with other embodiments.
Embodiment 1:
Equipped with mercurial thermometer, nitrogen protection device, reflux condensing tube dry cleansing three-necked flask in, be added
0.1moL triethylamine and 0.3moL chloropropene, 0.5moL ethyl acetate are uniformly mixed, and lead to N2Protection is to slowly warm up to 30 DEG C, perseverance
Temperature reaction for 24 hours, stands cooling, obtains white solid after revolving.For several times with acetone washing white solid, then with dehydrated alcohol, acetic acid
Acetate mixed solvent recrystallizes 2 times, freeze overnight, and decompression filters, and is dried in vacuo to obtain product.
In the dry three-necked flask of the cleaning equipped with mercurial thermometer, nitrogen protection device, reflux condensing tube, it is added
The above-mentioned product of 0.1moL, 0.1moL trimethoxy silane, 0.75mol isopropanol and appropriate platinum catalyst are uniformly mixed, and lead to N2It protects
Shield, is to slowly warm up to 70 DEG C, constant temperature is stirred to react 3h, is evaporated under reduced pressure to product.Product is cooled to room temperature, with ethyl acetate weight
Crystallization 2 times, decompression filter, and are dried in vacuo to obtain white crystal.
Embodiment 2:
It is cleaned by ultrasonic dacron 5min, dries 30min in 60 DEG C of electric drying oven with forced convections.Terylene after cleaning is knitted
Object immerses in 20g/L soda bath, concussion processing 1h under the conditions of 90 DEG C.After treatment finally exists fabric washing to neutrality
30min is dried in 60 DEG C of electric drying oven with forced convection, the dacron after being roughened.Dacron after roughening is cut into small
Sample cloth is made after block number.
5min, three leachings are arranged in the finisher solution that concentration is 20g/L, 15g/L, 10g/L, 5g/L respectively by sample cloth 1~4
Three roll, pick-up 100%, then 100 DEG C of drying 10min, then 160 DEG C bake 5min.By the sample ultrasonic cleaning after arrangement
5min is cleaned up, and is finally putting into 60 DEG C of electric drying oven with forced convections and is dried 30min.
According to GB/T 21655.1-2008, the moisture absorbing and sweat releasing performance of test gained fabric, test data is as follows:
The moisture absorbing and sweat releasing performance test data of the not same cloth of table 1
It can be seen from the data in the table that former dacron is after carrying out roughening treatment by soda bath, water droplet is spread completely
Time used significantly reduces, and the time used in moisture evaporating completely also reduces accordingly；And after finishing fluid is processed
Fabric, although on the time that water droplet is spread completely slightly rise and fall, all in all still relative to the fabric before arrangement
Significantly reduce, and the time used in treated fabric evaporation water obviously than being obviously shortened before processing, compared with original
It is furnished with conspicuousness variation.It can be seen that sample cloth exists in the data of the terylene sample cloth arranged from 4 by various concentration finishing fluid
The time used in moisture evaporating completely is most short when finishing fluid concentration is 20g/L, and successively decreasing with concentration, and the time used is slowly
It is elongated；And to spread the time used completely most fast for water droplet in concentration 20g/L.
Embodiment 3:
5min is arranged in the finisher solution that concentration is 20g/L by sample cloth 5~14, three leachings three are rolled, pick-up 100%.
Referring to embodiment 2 drying bake, baking step, after sample cloth 5~12 after arrangement are submerged initially in AgNO3Concentration is
5min in the solution of 0.1mol/L, then immerse the NaOH solution 5min of 0.1mol/L.It is set for drying according to following table after taking-up
It does, bake, the time is respectively 10min, 5min.Finally it is cleaned by ultrasonic 5min in pure water, then is rinsed and done with a large amount of ultrapure waters
Only, in 100 DEG C of drying 30min.
The moisture absorbing and sweat releasing performance data of the not same cloth of table 2
It knows to work as roasting under identical finishing fluid concentration, identical padding process, identical drying temperature from the data in table
Drying temperature is that water droplet diffusion and moisture evaporation time used are minimum on 160 DEG C of fabrics, and the moisture absorbing and sweat releasing effect of fabric is best.
Antibiotic property test is carried out to fabric according to AATCC 100-2012, measures fabric to staphylococcus aureus and large intestine
The antibiotic rate of bacillus.
The bacteriostasis property of the not same cloth of table 3
As can be seen from the table, the antibacterial effect of sample cloth 8 is best, i.e., bakes under the conditions of 160 DEG C under 5min processing, terylene
Fabric can obtain best fungistatic effect, reach 99% or more to the antibiotic rate of staphylococcus aureus and Escherichia coli, think
Than having extremely significant raising in sample cloth 1~4.
The preferred reaction condition of finishing agent of the present invention, is hydrolyzed by siloxanes and generates silanol, since silanol has chelating
Effect, can adhesiving metal Ag+, by metal Ag+Arrange on fabric, make treated fabric have good moisture absorbing and sweat releasing and
Fungistatic effect.
It should be noted that the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, although referring to preferable
Embodiment describes the invention in detail, those skilled in the art should understand that, it can be to technology of the invention
Scheme is modified or replaced equivalently, and without departing from the spirit and scope of the technical solution of the present invention, should all be covered in this hair
In bright scope of the claims.
Claims (10)
1. a kind of antibacterial fabric finishing method of moisture absorbing and sweat releasing characterized by comprising
Triethylamine, chloropropene, ethyl acetate, agitating and heating, revolving is added；
With acetone washing, decompression is filtered, and obtains product 1；
Trimethoxy silane and isopropanol mixture, agitating and heating is added；
Platinum catalyst is added, after isothermal reaction, vacuum distillation；
Ethyl acetate solution, freeze overnight, vacuum filtration is added；
Add water, AgNO is added3, obtain solution 1；
Fabric is immersed in soda bath, concussion is dried after cleaning；
The fabric is immersed in the solution 1, drying；
The fabric is immersed in NaOH solution, dries, bake, clean and dries.
2. the antibacterial fabric finishing method of moisture absorbing and sweat releasing as described in claim 1, it is characterised in that: the triethylamine, chloropropene
Molar ratio be 1:3；The molar ratio of the trimethoxy silane and product 1 is 1:1.
3. the antibacterial fabric finishing method of moisture absorbing and sweat releasing as claimed in claim 1 or 2, it is characterised in that: the soda bath is dense
Degree is 20g/L；The AgNO3Solution concentration is 0.1mol/L；The NaOH solution concentration is 0.1mol/L.
4. the antibacterial fabric finishing method of moisture absorbing and sweat releasing as claimed in claim 3, it is characterised in that: the addition triethylamine, chlorine
Propylene, ethyl acetate, agitating and heating, revolving, being heated to temperature is 30 DEG C；The addition trimethoxy silane and isopropanol are mixed
Object is closed, agitating and heating, being heated to temperature is 70 DEG C.
5. claim 1,2 or 4 it is any as described in moisture absorbing and sweat releasing antibacterial fabric finishing method, it is characterised in that: the addition
Platinum catalyst, after isothermal reaction, vacuum distillation, temperature is 70 DEG C, reaction time 3h.
6. the antibacterial fabric finishing method of moisture absorbing and sweat releasing as claimed in claim 5, it is characterised in that: described to immerse the fabric
In the solution 1, drying, impregnation method is that three leachings three are rolled, pick-up 100%；Its drying condition is 90 DEG C, and the time is
5min。
7. claim 1,2 or 6 it is any as described in moisture absorbing and sweat releasing antibacterial fabric finishing method, it is characterised in that: it is described to knit
Object immerses in soda bath, and concussion is dried after cleaning, and concussion temperature is 90 DEG C, and the concussion time is 1h, dries after cleaning,
Temperature is 60 DEG C.
8. the antibacterial fabric finishing method of moisture absorbing and sweat releasing as claimed in claim 7, it is characterised in that: described to immerse the fabric
It in NaOH solution, dries, bake, clean and dries, it is 5min, drying temperature 100 that the time is immersed in NaOH solution
DEG C, drying time 10min, baking temperature is 160 DEG C, and baking the time is 5min, and cleaning way is ultrasonic cleaning,
Its scavenging period is 5min, and drying temperature is 100 DEG C, drying time 30min.
9. the antibacterial of moisture absorbing and sweat releasing made from the antibacterial fabric finishing method of the moisture absorbing and sweat releasing prepared using claim 1~8 is knitted
Object, it is characterised in that: it is 59s, moisture evaporating completely time that the antibiotic fabric water droplet of moisture absorbing and sweat releasing spreads the time used completely
It can be down to 19 ' 34.
10. the antibiotic fabric of moisture absorbing and sweat releasing obtained as claimed in claim 9, it is characterised in that: the antibacterial of the moisture absorbing and sweat releasing
The antibiotic rate of fabric is 99.7%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910081926.0A CN109826005A (en) | 2019-01-28 | 2019-01-28 | A kind of antibacterial fabric finishing method of moisture absorbing and sweat releasing |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910081926.0A CN109826005A (en) | 2019-01-28 | 2019-01-28 | A kind of antibacterial fabric finishing method of moisture absorbing and sweat releasing |
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Cited By (2)
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| CN114808238A (en) * | 2022-04-22 | 2022-07-29 | 安徽凌晨纺织科技有限公司 | Production process of polyester linen-like fabric |
| CN118812581A (en) * | 2024-06-19 | 2024-10-22 | 商洛学院 | An organic silicon compound and its preparation method and application |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114808238A (en) * | 2022-04-22 | 2022-07-29 | 安徽凌晨纺织科技有限公司 | Production process of polyester linen-like fabric |
| CN118812581A (en) * | 2024-06-19 | 2024-10-22 | 商洛学院 | An organic silicon compound and its preparation method and application |
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Application publication date: 20190531 |