CN111501356A - Preparation method of crease-resistant suit fabric - Google Patents
Preparation method of crease-resistant suit fabric Download PDFInfo
- Publication number
- CN111501356A CN111501356A CN202010363395.7A CN202010363395A CN111501356A CN 111501356 A CN111501356 A CN 111501356A CN 202010363395 A CN202010363395 A CN 202010363395A CN 111501356 A CN111501356 A CN 111501356A
- Authority
- CN
- China
- Prior art keywords
- parts
- crease
- fabric
- uniformly mixing
- heating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000004744 fabric Substances 0.000 title claims abstract description 114
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000001035 drying Methods 0.000 claims abstract description 60
- 230000001153 anti-wrinkle effect Effects 0.000 claims abstract description 59
- 239000011248 coating agent Substances 0.000 claims abstract description 37
- 238000000576 coating method Methods 0.000 claims abstract description 37
- 239000000835 fiber Substances 0.000 claims abstract description 34
- 239000000853 adhesive Substances 0.000 claims abstract description 24
- 230000001070 adhesive effect Effects 0.000 claims abstract description 24
- 229920000742 Cotton Polymers 0.000 claims abstract description 9
- 229920000728 polyester Polymers 0.000 claims abstract description 8
- 239000011492 sheep wool Substances 0.000 claims abstract description 8
- 238000002791 soaking Methods 0.000 claims abstract description 8
- 238000003825 pressing Methods 0.000 claims abstract description 7
- 238000009941 weaving Methods 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims description 78
- 238000010438 heat treatment Methods 0.000 claims description 75
- 230000004048 modification Effects 0.000 claims description 52
- 238000012986 modification Methods 0.000 claims description 52
- 238000003756 stirring Methods 0.000 claims description 47
- 238000001816 cooling Methods 0.000 claims description 46
- 239000000463 material Substances 0.000 claims description 41
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 38
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 36
- 239000012752 auxiliary agent Substances 0.000 claims description 36
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- ZFOZVQLOBQUTQQ-UHFFFAOYSA-N Tributyl citrate Chemical compound CCCCOC(=O)CC(O)(C(=O)OCCCC)CC(=O)OCCCC ZFOZVQLOBQUTQQ-UHFFFAOYSA-N 0.000 claims description 20
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- 239000002025 wood fiber Substances 0.000 claims description 10
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims description 9
- 238000005406 washing Methods 0.000 claims description 9
- GGAUUQHSCNMCAU-ZXZARUISSA-N (2s,3r)-butane-1,2,3,4-tetracarboxylic acid Chemical compound OC(=O)C[C@H](C(O)=O)[C@H](C(O)=O)CC(O)=O GGAUUQHSCNMCAU-ZXZARUISSA-N 0.000 claims description 8
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- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 claims description 8
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- KWSLGOVYXMQPPX-UHFFFAOYSA-N 5-[3-(trifluoromethyl)phenyl]-2h-tetrazole Chemical compound FC(F)(F)C1=CC=CC(C2=NNN=N2)=C1 KWSLGOVYXMQPPX-UHFFFAOYSA-N 0.000 claims description 8
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- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims description 8
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- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 6
- 238000010992 reflux Methods 0.000 claims description 6
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- 102000004190 Enzymes Human genes 0.000 description 2
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- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
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- 230000002401 inhibitory effect Effects 0.000 description 2
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M17/00—Producing multi-layer textile fabrics
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- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
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- C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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Abstract
The application discloses a preparation method of crease-resistant suit fabric, which comprises the following steps: s1, weaving sheep wool into a surface fabric, coating the anti-wrinkle coating on the surface of the surface fabric for anti-wrinkle treatment, and then placing the surface fabric into an oven for primary drying treatment; s2, preparing the polyester fiber into a middle layer fabric; s3, preparing the natural cotton into inner fabric; s4, bonding and pressing the surface fabric, the middle fabric and the inner fabric by using a modified adhesive, then soaking the fabric in a softener, and then placing the fabric into an oven to carry out secondary drying treatment to obtain the crease-resistant suit fabric. The western-style clothes prepared by the preparation method of the crease-resistant suit have excellent crease-resistant performance.
Description
Technical Field
The invention belongs to the technical field of garment materials, and particularly relates to a preparation method of an anti-wrinkle suit material.
Background
Western-style clothes are also called western-style clothes and American style clothes. Western-style clothes have been experienced over 200 years of history since birth till now, are still constantly circulated and perfected, become a regular outfit for people to wear in daily life, and can be almost worn in both formal occasions and informal occasions, so that the Western-style clothes spread from Europe to the whole international society, become common instructive clothes in public occasions of the international society, and are known as 'international clothes'. The development of society brings the evolution of clothing culture, the fashion market popularity is constantly changing, and the trend of fashion and leisure fashion in the fashion is gradually popular in the domestic men's clothing world. Adopts the leisure style of cotton, hemp and other fabrics. When the existing western-style clothes are worn, the existing western-style clothes are easy to wrinkle after being washed or stored, and the appearance of the western-style clothes is seriously influenced.
Chinese patent application document "a processing method of a novel crease-resistant suit (publication number: CN 106913000A)" discloses a processing method of a novel crease-resistant suit, which is to weave rabbit hair and sheep wool into surface fabric; preparing polyester fiber into a middle layer fabric; supporting the inner layer fabric with natural cotton; bonding the surface layer fabric, the middle layer fabric and the inner layer fabric by adopting an adhesive to press the surface layer fabric, the middle layer fabric and the inner layer fabric into a synthetic fabric; and (3) soaking the prepared fabric in a softener, drying at constant temperature after soaking, and cutting to prepare the western-style clothes. Compared with the prior art, the crease-resistant fabric is provided with multiple layers of fabrics, is prepared by the special adhesive and the special softener, improves the crease-resistant capability of the fabric of the suit, and has popularization and application values. But the anti-wrinkle performance of the paint can not meet the requirement in actual use.
Disclosure of Invention
The invention aims to provide a preparation method of crease-resistant suit fabric, and aims to solve the problem of how to optimize components, dosage, methods and the like and improve crease-resistant performance of suit on the basis of a novel crease-resistant suit processing method disclosed in patent application document 'a novel crease-resistant suit processing method (publication number: CN 106913000A').
In order to solve the technical problems, the invention adopts the following technical scheme:
a preparation method of anti-wrinkle suit fabric comprises the following steps:
s1, weaving sheep wool into a surface fabric, coating the anti-wrinkle coating on the surface of the surface fabric for anti-wrinkle treatment, and then placing the surface fabric into an oven for primary drying treatment;
s2, preparing the polyester fiber into a middle layer fabric;
s3, preparing the natural cotton into inner fabric;
s4, bonding and pressing the surface fabric, the middle fabric and the inner fabric by using a modified adhesive, then soaking the fabric in a softener, and then placing the fabric into an oven to carry out secondary drying treatment to obtain the crease-resistant suit fabric.
Further, in S1, the anti-wrinkle coating comprises the following raw materials in parts by weight: 80-120 parts of waterborne polyurethane, 20-30 parts of montmorillonite, 15-25 parts of distilled water, 12-24 parts of anti-wrinkle modification auxiliary agent and 15-25 parts of antibacterial modification auxiliary agent.
Further, in the anti-wrinkle coating material in S1, the anti-wrinkle modification auxiliary agent comprises the following raw materials in parts by weight: 40-60 parts of bamboo fiber powder, 50-80 parts of distilled water, 4-9 parts of sodium hypophosphite, 3-6 parts of butane tetracarboxylic acid, 2-8 parts of wood fiber powder, 1-5 parts of jute fiber, 2-5 parts of penetrating agent, 4-8 parts of nano titanium dioxide, 3-9 parts of 2, 4-toluene diisocyanate, KH-5602-6 parts of silane coupling agent, 1-5 parts of sodium sulfite, 4-8 parts of polyether polyol and 2-5 parts of ammonium persulfate.
Further, in the anti-wrinkle coating material in S1, the anti-wrinkle modification auxiliary agent is prepared according to the following process: under the protection of nitrogen, uniformly mixing bamboo fiber powder, distilled water and sodium hypophosphite, heating to 80-90 ℃, preserving heat for 10-30min, adding ammonium persulfate, uniformly mixing, stirring for 5-15min, adding butanetetracarboxylic acid, uniformly mixing, stirring at the rotating speed of 850-1250r/min for 50-70min, heating to 85-95 ℃, extracting for 40-50h, drying to constant weight in a vacuum oven at the temperature of 65-75 ℃, and cooling to room temperature to obtain a material a; uniformly mixing wood fiber powder, jute fiber, a penetrating agent, nano titanium dioxide and 2, 4-toluene diisocyanate, carrying out ultrasonic treatment for 1-3h, adding a material a, a silane coupling agent KH-560, sodium sulfite and polyether polyol, uniformly mixing, stirring at the rotating speed of 650-850r/min for 20-40min, heating to 80-90 ℃, refluxing for 20-30h, and cooling to room temperature to obtain the anti-wrinkle modification auxiliary agent.
Further, in the anti-wrinkle coating material in S1, the antibacterial modification auxiliary is prepared according to the following process: uniformly mixing 40-50 parts of chitosan, 20-30 parts of diatomite powder, 5-15 parts of polyvinylpyrrolidone and 8-16 parts of deionized water according to parts by weight, grinding for 20-40min, heating to 80-90 ℃, keeping the temperature for 20-30min, adding 2-5 parts of sodium chloride and 1-6 parts of defoaming agent, stirring, continuously heating to 80-90 ℃, keeping the temperature for 5-15min, adding 4-8 parts of aluminum nitrate and 3-9 parts of zinc oxide, uniformly mixing, heating in a water bath for 1-2h, cooling to room temperature, adding 2-5 parts of diammonium hydrogen phosphate, uniformly mixing, aging, filtering, washing, drying, and cooling to room temperature after calcination to obtain the antibacterial modification aid.
Further, in S1, the anti-wrinkle paint is prepared according to the following process: uniformly mixing the waterborne polyurethane, the montmorillonite and the distilled water, heating to the temperature of 110-.
Further, in S1, the modified adhesive comprises the following raw materials in parts by weight: 20-30 parts of polyurethane, 4-8 parts of ethanol cellosolve acetate, 3-9 parts of butyl cellosolve acetate, 2-6 parts of ethyl cellosolve, 2-5 parts of ethyl cellulose, 4-8 parts of polyvinyl acetate, 2-8 parts of hydroxyethyl methacrylate, 1-5 parts of isooctyl acrylate, 4-8 parts of ammonium persulfate, 3-6 parts of sodium bisulfite, 2-5 parts of tributyl citrate, 4-8 parts of itaconic acid and 1-8 parts of nano zinc oxide.
Further, in S1, the modified adhesive is prepared by the following process: uniformly mixing polyurethane, ethanol cellosolve acetate, butyl cellosolve acetate and ethyl cellosolve, heating to 60-90 ℃, preserving heat for 20-30min, stirring at the rotating speed of 650 plus 850r/min for 1-2h, and cooling to room temperature to obtain a material A; uniformly mixing ethyl cellulose, polyvinyl acetate, hydroxyethyl methacrylate, isooctyl acrylate, ammonium persulfate, sodium bisulfite, tributyl citrate, itaconic acid and nano zinc oxide, heating to 85-95 ℃, preserving heat for 30-50min, stirring at the rotating speed of 1500-2500r/min for 10-30min, and cooling to room temperature to obtain a material B; heating the material B to 90-110 ℃, then adding the material A to be uniformly mixed, continuously heating to 120-.
Further, in S1, the temperature of the primary drying treatment is 40-50 ℃, and the time of the primary drying treatment is 1-2 h.
Further, in S4, the temperature of the secondary drying treatment is 80-90 ℃, and the time of the secondary drying treatment is 30-60 min.
The invention has the following beneficial effects: the crease-resistant adsorption of the invention is based on crease-resistant treatment on surface fabric, and two-step drying is carried out in the process of synthesizing the fabric, the primary drying is carried out for a long time at low temperature, finally the drying is carried out for quick drying at high temperature, finally the pressed fabric is soaked in softener, the finally obtained western-style clothes have excellent crease-resistant performance, the excellent crease-resistant performance is based on crease-resistant coating coated in the crease-resistant treatment, the crease-resistant coating adopts crease-resistant modification auxiliary agent which takes bamboo fiber powder, wood fiber powder and jute fiber as toughness basic filler, and nano titanium dioxide as antibacterial agent, the surface area of the toughness basic filler is increased through the graft modification of silane coupling agent KH-560, the molecular structure of the whole crease-resistant modification auxiliary agent is extended, so that the ductility and elasticity of the crease-resistant coating are better, and is not easy to wrinkle.
In addition, the antibacterial modification auxiliary agent is prepared by uniformly mixing chitosan, diatomite powder, polyvinylpyrrolidone and deionized water, grinding, heating, preserving heat, adding sodium chloride and a defoaming agent, stirring, continuously heating, preserving heat, adding aluminum nitrate and zinc oxide, uniformly mixing, heating in a water bath, cooling to room temperature, adding diammonium hydrogen phosphate, uniformly mixing, aging, filtering, washing, drying, calcining, cooling to room temperature, obtaining the antibacterial modification auxiliary agent, wherein the chitosan has strong affinity to fibers, has positive charges in water, is easily adsorbed by the fibers, and can enhance the adsorption capacity of the fibers to negative-charge active dyes, direct dyes and the like, in addition, the chitosan is easily dissolved in a weak acid solvent, the dissolved solution contains amino groups, and the amino groups are combined with bacteria by combining negative electrons to enable the bacteria to generate structural change or energy transfer to cause bacterial death, thereby realizing the function of inhibiting bacteria and realizing the osmosis function of the aqueous polyurethane. In addition, hydroxyl on the surfaces of the chitosan and the diatomite powder and amino in the hydrolyzed solution inhibit the activity of respiratory enzymes on the surfaces of bacteria by combining negative electrons, so that the bacteria are inactivated and are obtained under the coagulation action of polyvinylpyrrolidone, and in a reinforcing system, under the graft modification action of a silane coupling agent KH-560, the hydroxyl on the surfaces of the chitosan and the diatomite powder is combined with unsaturated bonds on the surfaces of waterborne polyurethane, so that excellent antibacterial performance is finally endowed to the surface fabric.
Furthermore, the modified adhesive takes ethyl cellulose, polyvinyl acetate and hydroxyethyl methacrylate as high molecular resin, isooctyl acrylate, ammonium persulfate and tributyl citrate as organic solvent, nano zinc oxide and sodium bisulfite as thixotropic agent, wherein the ethyl cellulose and the hydroxyethyl methacrylate have thixotropic property, the surfaces of the ethyl cellulose, the polyvinyl acetate and the hydroxyethyl methacrylate contain a large amount of hydrogen bonds, a network structure with weak acting force can be formed, the thermal motion of molecular chain segments and metal micro particles is prevented, the viscosity is increased, the nano zinc oxide and the sodium bisulfite are used as the thixotropic agent, the ethyl cellulose and the hydroxyethyl methacrylate have thixotropic property, the synthesized organic adhesive has good thixotropy, namely, the viscosity of the sizing agent is reduced under the action of the external force, the viscosity is restored after the external force action disappears, so that the electrode can be plump after the end is soaked, a certain thickness is kept, the edge interface is clear, the flowing is avoided, and meanwhile, the settlement of metal particles can be avoided in the fabric placing process, and the agglomeration is prevented. The ethyl cellulose is used as a thickening agent, improves the viscosity and plasticity of the slurry, has a net structure and groups with stronger polarity, can be dissolved by an organic solvent at normal temperature in a solid powder state, and forms a firm film at a certain temperature.
Detailed Description
In order to facilitate a better understanding of the invention, the following examples are given to illustrate, but not to limit the scope of the invention.
In an embodiment, the preparation method of the crease-resistant suit fabric comprises the following steps:
s1, weaving sheep wool into a surface fabric, coating an anti-wrinkle coating on the surface of the surface fabric for anti-wrinkle treatment, and then placing the surface fabric into an oven for primary drying treatment, wherein the temperature of the primary drying treatment is 40-50 ℃, and the time of the primary drying treatment is 1-2 hours;
s2, preparing the polyester fiber into a middle layer fabric;
s3, preparing the natural cotton into inner fabric;
s4, bonding and pressing the surface fabric, the middle fabric and the inner fabric by using a modified adhesive, then putting the obtained product into a softener for soaking, and then putting the product into an oven for secondary drying treatment to obtain the crease-resistant suit fabric, wherein the temperature of the secondary drying treatment is 80-90 ℃, and the time of the secondary drying treatment is 30-60 min.
The anti-wrinkle coating comprises the following raw materials in parts by weight: 80-120 parts of waterborne polyurethane, 20-30 parts of montmorillonite, 15-25 parts of distilled water, 12-24 parts of anti-wrinkle modification auxiliary agent and 15-25 parts of antibacterial modification auxiliary agent.
The anti-wrinkle modification auxiliary agent is prepared by the following process: under the protection of nitrogen, uniformly mixing 40-60 parts by weight of bamboo fiber powder, 50-80 parts by weight of distilled water and 4-9 parts by weight of sodium hypophosphite, heating to 80-90 ℃, keeping the temperature for 10-30min, then adding ammonium persulfate, uniformly mixing, stirring for 5-15min, then adding 3-6 parts by weight of butanetetracarboxylic acid, uniformly mixing, stirring for 50-70min at the rotating speed of 850-1250r/min, heating to 85-95 ℃, extracting for 40-50h, then drying to constant weight at 65-75 ℃ in a vacuum oven, and cooling to room temperature to obtain a material a; uniformly mixing 2-8 parts of wood fiber powder, 1-5 parts of jute fiber, 2-5 parts of penetrating agent, 4-8 parts of nano titanium dioxide and 3-9 parts of 2, 4-toluene diisocyanate, carrying out ultrasonic treatment for 1-3h, then adding a material a, 2-6 parts of silane coupling agent KH-560, 1-5 parts of sodium sulfite and 4-8 parts of polyether polyol, uniformly mixing, stirring at the rotating speed of 650 plus 850r/min for 20-40min, then heating to 80-90 ℃, refluxing for 20-30h, and cooling to room temperature to obtain the anti-wrinkle modification aid.
The antibacterial modified additive is prepared by the following process: uniformly mixing 40-50 parts of chitosan, 20-30 parts of diatomite powder, 5-15 parts of polyvinylpyrrolidone and 8-16 parts of deionized water according to parts by weight, grinding for 20-40min, heating to 80-90 ℃, keeping the temperature for 20-30min, adding 2-5 parts of sodium chloride and 1-6 parts of defoaming agent, stirring, continuously heating to 80-90 ℃, keeping the temperature for 5-15min, adding 4-8 parts of aluminum nitrate and 3-9 parts of zinc oxide, uniformly mixing, heating in a water bath for 1-2h, cooling to room temperature, adding 2-5 parts of diammonium hydrogen phosphate, uniformly mixing, aging, filtering, washing, drying, and cooling to room temperature after calcination to obtain the antibacterial modification aid.
The anti-wrinkle coating is prepared by the following process: uniformly mixing the waterborne polyurethane, the montmorillonite and the distilled water, heating to the temperature of 110-.
The modified adhesive is prepared by the following process: uniformly mixing 20-30 parts of polyurethane, 4-8 parts of ethanol cellosolve acetate, 3-9 parts of butyl cellosolve acetate and 2-6 parts of ethyl cellosolve according to the parts by weight, heating to 60-90 ℃, preserving heat for 20-30min, stirring at the rotating speed of 650 plus 850r/min for 1-2h, and cooling to room temperature to obtain a material A; uniformly mixing 2-5 parts of ethyl cellulose, 4-8 parts of polyvinyl acetate, 2-8 parts of hydroxyethyl methacrylate, 1-5 parts of isooctyl acrylate, 4-8 parts of ammonium persulfate, 3-6 parts of sodium bisulfite, 2-5 parts of tributyl citrate, 4-8 parts of itaconic acid and 1-8 parts of nano zinc oxide, heating to 85-95 ℃, preserving heat for 30-50min, stirring at the rotating speed of 1500-2500r/min for 10-30min, and cooling to room temperature to obtain a material B; heating the material B to 90-110 ℃, then adding the material A to be uniformly mixed, continuously heating to 120-.
Example 1
A preparation method of anti-wrinkle suit fabric comprises the following steps:
s1, weaving sheep wool into a surface fabric, coating an anti-wrinkle coating on the surface of the surface fabric for anti-wrinkle treatment, and then placing the surface fabric into an oven for primary drying treatment, wherein the temperature of the primary drying treatment is 45 ℃, and the time of the primary drying treatment is 1.5 h;
s2, preparing the polyester fiber into a middle layer fabric;
s3, preparing the natural cotton into inner fabric;
s4, bonding and pressing the surface fabric, the middle fabric and the inner fabric by using a modified adhesive, then putting the obtained product into a softener to soak, and then putting the product into an oven to carry out secondary drying treatment to obtain the crease-resistant suit fabric, wherein the temperature of the secondary drying treatment is 85 ℃, and the time of the secondary drying treatment is 45 min.
The anti-wrinkle coating comprises the following raw materials in parts by weight: 100 parts of waterborne polyurethane, 25 parts of montmorillonite, 20 parts of distilled water, 18 parts of anti-wrinkle modification auxiliary agent and 20 parts of antibacterial modification auxiliary agent.
The anti-wrinkle modification auxiliary agent is prepared by the following process: under the protection of nitrogen, uniformly mixing 50 parts by weight of bamboo fiber powder, 65 parts by weight of distilled water and 6.5 parts by weight of sodium hypophosphite, heating to 85 ℃, keeping the temperature for 20min, adding ammonium persulfate, uniformly mixing, stirring for 10min, adding 4.5 parts by weight of butanetetracarboxylic acid, uniformly mixing, stirring at the rotating speed of 1050r/min for 60min, heating to 90 ℃, extracting for 45h, drying in a vacuum oven at the temperature of 70 ℃ to constant weight, and cooling to room temperature to obtain a material a; uniformly mixing 5 parts of wood fiber powder, 3 parts of jute fiber, 3.5 parts of penetrating agent, 6 parts of nano titanium dioxide and 6 parts of 2, 4-toluene diisocyanate, carrying out ultrasonic treatment for 2 hours, then adding a material a, 4 parts of silane coupling agent KH-560, 3 parts of sodium sulfite and 6 parts of polyether polyol, uniformly mixing, stirring at the rotating speed of 750r/min for 30 minutes, then heating to 85 ℃, refluxing for 25 hours, and cooling to room temperature to obtain the anti-wrinkle modification aid.
The antibacterial modified additive is prepared by the following process: uniformly mixing 45 parts of chitosan, 25 parts of diatomite powder, 10 parts of polyvinylpyrrolidone and 12 parts of deionized water in parts by weight, grinding for 30min, heating to 85 ℃, keeping the temperature for 25min, adding 3.5 parts of sodium chloride and 3.5 parts of defoaming agent, stirring, continuously heating to 85 ℃, keeping the temperature for 10min, adding 6 parts of aluminum nitrate and 6 parts of zinc oxide, uniformly mixing, heating in a water bath for 1.5h, cooling to room temperature, adding 3.5 parts of diammonium hydrogen phosphate, uniformly mixing, aging, filtering, washing, drying, calcining, and cooling to room temperature to obtain the antibacterial modification aid.
The anti-wrinkle coating is prepared by the following process: uniformly mixing the waterborne polyurethane, the montmorillonite and the distilled water, heating to 125 ℃, preserving heat for 1.5h, stirring at the rotating speed of 2000r/min for 30min, adding the anti-wrinkle modification auxiliary agent and the antibacterial modification auxiliary agent, uniformly mixing, continuously heating to 170 ℃, preserving heat for 45min, stirring at the rotating speed of 950r/min for 40min, and cooling to room temperature to obtain the modified montmorillonite-based antibacterial polyurethane.
The modified adhesive is prepared by the following process: uniformly mixing 25 parts of polyurethane, 6 parts of ethanol cellosolve acetate, 6 parts of butyl cellosolve acetate and 4 parts of ethyl cellosolve according to parts by weight, heating to 75 ℃, keeping the temperature for 25min, stirring at the rotating speed of 750r/min for 1.5h, and cooling to room temperature to obtain a material A; uniformly mixing 3.5 parts of ethyl cellulose, 6 parts of polyvinyl acetate, 5 parts of hydroxyethyl methacrylate, 3 parts of isooctyl acrylate, 6 parts of ammonium persulfate, 4.5 parts of sodium bisulfite, 3.5 parts of tributyl citrate, 6 parts of itaconic acid and 4.5 parts of nano zinc oxide, heating to 90 ℃, preserving heat for 40min, stirring at the rotating speed of 2000r/min for 20min, and cooling to room temperature to obtain a material B; heating the material B to 100 ℃, then adding the material A, uniformly mixing, continuously heating to 125 ℃, keeping the temperature for 1-3h, stirring at the rotating speed of 2000r/min for 30min, and cooling to room temperature to obtain the modified adhesive.
Example 2
A preparation method of anti-wrinkle suit fabric comprises the following steps:
s1, weaving sheep wool into a surface fabric, coating an anti-wrinkle coating on the surface of the surface fabric for anti-wrinkle treatment, and then placing the surface fabric into an oven for primary drying treatment, wherein the temperature of the primary drying treatment is 40 ℃, and the time of the primary drying treatment is 2 hours;
s2, preparing the polyester fiber into a middle layer fabric;
s3, preparing the natural cotton into inner fabric;
s4, bonding and pressing the surface fabric, the middle fabric and the inner fabric by using a modified adhesive, then putting the obtained product into a softener to soak, and then putting the product into an oven to carry out secondary drying treatment to obtain the crease-resistant suit fabric, wherein the temperature of the secondary drying treatment is 80 ℃, and the time of the secondary drying treatment is 60 min.
The anti-wrinkle coating comprises the following raw materials in parts by weight: 80 parts of waterborne polyurethane, 30 parts of montmorillonite, 15 parts of distilled water, 24 parts of anti-wrinkle modification auxiliary agent and 15 parts of antibacterial modification auxiliary agent.
The anti-wrinkle modification auxiliary agent is prepared by the following process: under the protection of nitrogen, uniformly mixing 40 parts by weight of bamboo fiber powder, 80 parts by weight of distilled water and 4 parts by weight of sodium hypophosphite, heating to 90 ℃, preserving heat for 10min, adding ammonium persulfate, uniformly mixing, stirring for 15min, adding 3 parts by weight of butanetetracarboxylic acid, uniformly mixing, stirring at the rotating speed of 1250r/min for 50min, heating to 95 ℃, extracting for 40h, drying in a vacuum oven at the temperature of 75 ℃ to constant weight, and cooling to room temperature to obtain a material a; uniformly mixing 2 parts of wood fiber powder, 5 parts of jute fiber, 2 parts of penetrating agent, 8 parts of nano titanium dioxide and 3 parts of 2, 4-toluene diisocyanate, carrying out ultrasonic treatment for 3 hours, adding a material a, 2 parts of silane coupling agent KH-560, 5 parts of sodium sulfite and 4 parts of polyether polyol, uniformly mixing, stirring at the rotating speed of 850r/min for 20 minutes, heating to 90 ℃, refluxing for 20 hours, and cooling to room temperature to obtain the anti-wrinkle modification aid.
The antibacterial modified additive is prepared by the following process: uniformly mixing 40 parts of chitosan, 30 parts of diatomite powder, 5 parts of polyvinylpyrrolidone and 16 parts of deionized water in parts by weight, grinding for 20min, heating to 90 ℃, keeping the temperature for 20min, adding 5 parts of sodium chloride and 1 part of defoaming agent, stirring, continuously heating to 90 ℃, keeping the temperature for 5min, adding 8 parts of aluminum nitrate and 3 parts of zinc oxide, uniformly mixing, heating in a water bath for 2h, cooling to room temperature, adding 2 parts of diammonium hydrogen phosphate, uniformly mixing, aging, filtering, washing, drying, calcining, and cooling to room temperature to obtain the antibacterial modification aid.
The anti-wrinkle coating is prepared by the following process: uniformly mixing waterborne polyurethane, montmorillonite and distilled water, heating to 110 ℃, preserving heat for 2h, stirring at the rotating speed of 1500r/min for 40min, adding the anti-wrinkle modification auxiliary agent and the antibacterial modification auxiliary agent, uniformly mixing, continuously heating to 160 ℃, preserving heat for 60min, stirring at the rotating speed of 850r/min for 50min, and cooling to room temperature to obtain the anti-wrinkle modified montmorillonite/montmorillonite modified montmorillonite-montmorillonite antibacterial modified montmorillonite-modified montmorillonite-.
The modified adhesive is prepared by the following process: uniformly mixing 20 parts of polyurethane, 8 parts of ethanol cellosolve acetate, 3 parts of butyl cellosolve acetate and 6 parts of ethyl cellosolve according to parts by weight, heating to 60 ℃, preserving heat for 30min, stirring at the rotating speed of 650r/min for 2h, and cooling to room temperature to obtain a material A; uniformly mixing 2 parts of ethyl cellulose, 8 parts of polyvinyl acetate, 2 parts of hydroxyethyl methacrylate, 5 parts of isooctyl acrylate, 4 parts of ammonium persulfate, 6 parts of sodium bisulfite, 2 parts of tributyl citrate, 8 parts of itaconic acid and 1 part of nano zinc oxide, heating to 95 ℃, preserving heat for 30min, stirring at the rotating speed of 2500r/min for 10min, and cooling to room temperature to obtain a material B; heating the material B to 110 ℃, then adding the material A, uniformly mixing, continuously heating to 120 ℃, keeping the temperature for 3 hours, stirring at the rotating speed of 1500r/min for 40 minutes, and cooling to room temperature to obtain the modified adhesive.
Example 3
A preparation method of anti-wrinkle suit fabric comprises the following steps:
s1, weaving sheep wool into a surface fabric, coating an anti-wrinkle coating on the surface of the surface fabric for anti-wrinkle treatment, and then placing the surface fabric into an oven for primary drying treatment, wherein the temperature of the primary drying treatment is 50 ℃, and the time of the primary drying treatment is 1 hour;
s2, preparing the polyester fiber into a middle layer fabric;
s3, preparing the natural cotton into inner fabric;
s4, bonding and pressing the surface fabric, the middle fabric and the inner fabric by using a modified adhesive, then putting the obtained product into a softener for soaking, and then putting the product into an oven for secondary drying treatment to obtain the crease-resistant suit fabric, wherein the temperature of the secondary drying treatment is 90 ℃, and the time of the secondary drying treatment is 30 min.
The anti-wrinkle coating comprises the following raw materials in parts by weight: 120 parts of waterborne polyurethane, 20 parts of montmorillonite, 25 parts of distilled water, 12 parts of anti-wrinkle modification auxiliary agent and 25 parts of antibacterial modification auxiliary agent.
The anti-wrinkle modification auxiliary agent is prepared by the following process: under the protection of nitrogen, uniformly mixing 60 parts of bamboo fiber powder, 50 parts of distilled water and 9 parts of sodium hypophosphite in parts by weight, heating to 80 ℃, keeping the temperature for 30min, adding ammonium persulfate, uniformly mixing, stirring for 5min, adding 6 parts of butanetetracarboxylic acid, uniformly mixing, stirring at the rotating speed of 850r/min for 70min, heating to 85 ℃, extracting for 50h, drying in a vacuum oven at the temperature of 65 ℃ to constant weight, and cooling to room temperature to obtain a material a; uniformly mixing 8 parts of wood fiber powder, 1 part of jute fiber, 5 parts of penetrating agent, 4 parts of nano titanium dioxide and 9 parts of 2, 4-toluene diisocyanate, carrying out ultrasonic treatment for 1h, then adding a material a, 6 parts of silane coupling agent KH-560, 1 part of sodium sulfite and 8 parts of polyether polyol, uniformly mixing, stirring at the rotating speed of 650r/min for 40min, then heating to 80 ℃, refluxing for 30h, and cooling to room temperature to obtain the anti-wrinkle modification aid.
The antibacterial modified additive is prepared by the following process: uniformly mixing 50 parts of chitosan, 20 parts of diatomite powder, 15 parts of polyvinylpyrrolidone and 8 parts of deionized water in parts by weight, grinding for 40min, heating to 80 ℃, keeping the temperature for 30min, adding 2 parts of sodium chloride and 6 parts of defoaming agent, stirring, continuously heating to 80 ℃, keeping the temperature for 15min, adding 4 parts of aluminum nitrate and 9 parts of zinc oxide, uniformly mixing, heating in a water bath for 1h, cooling to room temperature, adding 5 parts of diammonium hydrogen phosphate, uniformly mixing, aging, filtering, washing, drying, and cooling to room temperature after calcination to obtain the antibacterial modification aid.
The anti-wrinkle coating is prepared by the following process: uniformly mixing waterborne polyurethane, montmorillonite and distilled water, heating to 140 ℃, preserving heat for 1h, stirring at the rotating speed of 2500r/min for 20min, adding an anti-wrinkle modification auxiliary agent and an antibacterial modification auxiliary agent, uniformly mixing, continuously heating to 180 ℃, preserving heat for 30min, stirring at the rotating speed of 1050r/min for 30min, and cooling to room temperature to obtain the anti-wrinkle modified montmorillonite/montmorillonite modified montmorillonite-based antibacterial composite material.
The modified adhesive is prepared by the following process: uniformly mixing 30 parts of polyurethane, 4 parts of ethanol cellosolve acetate, 9 parts of butyl cellosolve acetate and 2 parts of ethyl cellosolve according to parts by weight, heating to 90 ℃, preserving heat for 20min, stirring at the rotating speed of 850r/min for 1h, and cooling to room temperature to obtain a material A; uniformly mixing 5 parts of ethyl cellulose, 4 parts of polyvinyl acetate, 8 parts of hydroxyethyl methacrylate, 1 part of isooctyl acrylate, 8 parts of ammonium persulfate, 3 parts of sodium bisulfite, 5 parts of tributyl citrate, 4 parts of itaconic acid and 8 parts of nano zinc oxide, heating to 85 ℃, preserving heat for 50min, stirring at the rotating speed of 1500r/min for 30min, and cooling to room temperature to obtain a material B; heating the material B to 90 ℃, then adding the material A, uniformly mixing, continuously heating to 130 ℃, keeping the temperature for 1h, stirring at the rotating speed of 2500r/min for 20min, and cooling to room temperature to obtain the modified adhesive.
Comparative example
The suit is produced by adopting a Chinese patent application document 'a novel processing method of crease-resistant suit (publication number: CN 106913000A)'.
Experimental data on wrinkle recovery angle, breaking strength retention rate, washing size change rate, and dry-cleaning size change rate of the western-style clothes fabrics manufactured in examples 1 to 3 and comparative example are shown in table 1 below.
Table 1:
from table 1 above, it can be seen that:
the crease-resistant adsorption is based on crease-resistant treatment on surface fabric, the fabric is dried in two steps in the process of synthesizing the fabric, the primary drying is carried out at low temperature for a long time, the drying is carried out at high temperature for quick drying, the fabric pressed finally is added into a softener for soaking, the finally obtained western-style clothes have excellent crease-resistant performance, the excellent crease-resistant performance is based on crease-resistant coating coated in the crease-resistant treatment, and crease-resistant modification auxiliary agents are adopted in the crease-resistant coating, the anti-wrinkle modification auxiliary agent takes bamboo fiber powder, wood fiber powder and jute fiber as toughness basic filler, and nanometer titanium dioxide is added as an antibacterial agent, and the surface area of the toughness basic filler is increased through the graft modification of a silane coupling agent KH-560, so that the molecular structure of the whole anti-wrinkle modification auxiliary agent is expanded, and the anti-wrinkle coating has better ductility and elasticity and is not easy to wrinkle.
In addition, the antibacterial modification auxiliary agent is obtained by uniformly mixing chitosan, diatomite powder, polyvinylpyrrolidone and deionized water, grinding, heating, preserving heat, adding sodium chloride and a defoaming agent, stirring, continuously heating, preserving heat, then adding aluminum nitrate and zinc oxide, uniformly mixing, heating in a water bath, cooling to room temperature, then adding diammonium hydrogen phosphate, uniformly mixing, aging, filtering, washing, drying, calcining, and cooling to room temperature, the chitosan has strong affinity to fiber, has positive charges in water, is easily adsorbed by the fiber, and can enhance the adsorption capacity of the fiber to negative-charge active dyes, direct dyes and the like, in addition, the chitosan is easily dissolved in a weak acid solvent, the dissolved solution contains amino groups, and the amino groups are combined with bacteria by combining negative electrons, so that the bacteria generate structural change or energy transfer to cause bacterial death, thereby realizing the function of inhibiting bacteria and realizing the osmosis function of the aqueous polyurethane. In addition, hydroxyl on the surfaces of the chitosan and the diatomite powder and amino in the hydrolyzed solution inhibit the activity of respiratory enzymes on the surfaces of bacteria by combining negative electrons, so that the bacteria are inactivated and are obtained under the coagulation action of polyvinylpyrrolidone, and in a reinforcing system, under the graft modification action of a silane coupling agent KH-560, the hydroxyl on the surfaces of the chitosan and the diatomite powder is combined with unsaturated bonds on the surfaces of waterborne polyurethane, so that excellent antibacterial performance is finally endowed to the surface fabric.
Furthermore, the modified adhesive takes ethyl cellulose, polyvinyl acetate and hydroxyethyl methacrylate as high molecular resin, isooctyl acrylate, ammonium persulfate and tributyl citrate as organic solvent, nano zinc oxide and sodium bisulfite as thixotropic agent, wherein the ethyl cellulose and the hydroxyethyl methacrylate have thixotropic property, the surfaces of the ethyl cellulose, the polyvinyl acetate and the hydroxyethyl methacrylate contain a large amount of hydrogen bonds, a network structure with weak acting force can be formed, the thermal motion of molecular chain segments and metal micro particles is prevented, the viscosity is increased, the nano zinc oxide and the sodium bisulfite are used as the thixotropic agent, the ethyl cellulose and the hydroxyethyl methacrylate have thixotropic property, the synthesized organic adhesive has good thixotropy, namely, the viscosity of the sizing agent is reduced under the action of the external force, the viscosity is restored after the external force action disappears, so that the electrode can be plump after the end is soaked, a certain thickness is kept, the edge interface is clear, the flowing is avoided, and meanwhile, the settlement of metal particles can be avoided in the fabric placing process, and the agglomeration is prevented. The ethyl cellulose is used as a thickening agent, improves the viscosity and plasticity of the slurry, has a net structure and groups with stronger polarity, can be dissolved by an organic solvent at normal temperature in a solid powder state, and forms a firm film at a certain temperature.
The above description should not be taken as limiting the invention to the embodiments, but rather, as will be apparent to those skilled in the art to which the invention pertains, numerous simplifications or substitutions may be made without departing from the spirit of the invention, which shall be deemed to fall within the scope of the invention as defined by the claims appended hereto.
Claims (10)
1. The preparation method of the crease-resistant suit fabric is characterized by comprising the following steps:
s1, weaving sheep wool into a surface fabric, coating the anti-wrinkle coating on the surface of the surface fabric for anti-wrinkle treatment, and then placing the surface fabric into an oven for primary drying treatment;
s2, preparing the polyester fiber into a middle layer fabric;
s3, preparing the natural cotton into inner fabric;
s4, bonding and pressing the surface fabric, the middle fabric and the inner fabric by using a modified adhesive, then soaking the fabric in a softener, and then placing the fabric into an oven to carry out secondary drying treatment to obtain the crease-resistant suit fabric.
2. The preparation method of the crease-resistant suit fabric according to claim 1, wherein in S1, the crease-resistant coating comprises the following raw materials in parts by weight: 80-120 parts of waterborne polyurethane, 20-30 parts of montmorillonite, 15-25 parts of distilled water, 12-24 parts of anti-wrinkle modification auxiliary agent and 15-25 parts of antibacterial modification auxiliary agent.
3. The preparation method of the crease-resistant suit fabric according to claim 2, wherein in the crease-resistant coating, the crease-resistant modification auxiliary comprises the following raw materials in parts by weight: 40-60 parts of bamboo fiber powder, 50-80 parts of distilled water, 4-9 parts of sodium hypophosphite, 3-6 parts of butane tetracarboxylic acid, 2-8 parts of wood fiber powder, 1-5 parts of jute fiber, 2-5 parts of penetrating agent, 4-8 parts of nano titanium dioxide, 3-9 parts of 2, 4-toluene diisocyanate, KH-5602-6 parts of silane coupling agent, 1-5 parts of sodium sulfite, 4-8 parts of polyether polyol and 2-5 parts of ammonium persulfate.
4. The method for preparing the crease-resistant suit fabric according to claim 2, wherein in the crease-resistant coating, the crease-resistant modification auxiliary agent is prepared according to the following process in S1: under the protection of nitrogen, uniformly mixing bamboo fiber powder, distilled water and sodium hypophosphite, heating to 80-90 ℃, preserving heat for 10-30min, adding ammonium persulfate, uniformly mixing, stirring for 5-15min, adding butanetetracarboxylic acid, uniformly mixing, stirring at the rotating speed of 850-1250r/min for 50-70min, heating to 85-95 ℃, extracting for 40-50h, drying to constant weight in a vacuum oven at the temperature of 65-75 ℃, and cooling to room temperature to obtain a material a; uniformly mixing wood fiber powder, jute fiber, a penetrating agent, nano titanium dioxide and 2, 4-toluene diisocyanate, carrying out ultrasonic treatment for 1-3h, adding a material a, a silane coupling agent KH-560, sodium sulfite and polyether polyol, uniformly mixing, stirring at the rotating speed of 650-850r/min for 20-40min, heating to 80-90 ℃, refluxing for 20-30h, and cooling to room temperature to obtain the anti-wrinkle modification auxiliary agent.
5. The method for preparing the crease-resistant suit fabric according to claim 2, wherein in the crease-resistant coating, the antibacterial modification auxiliary agent is prepared according to the following process in S1: uniformly mixing 40-50 parts of chitosan, 20-30 parts of diatomite powder, 5-15 parts of polyvinylpyrrolidone and 8-16 parts of deionized water according to parts by weight, grinding for 20-40min, heating to 80-90 ℃, keeping the temperature for 20-30min, adding 2-5 parts of sodium chloride and 1-6 parts of defoaming agent, stirring, continuously heating to 80-90 ℃, keeping the temperature for 5-15min, adding 4-8 parts of aluminum nitrate and 3-9 parts of zinc oxide, uniformly mixing, heating in a water bath for 1-2h, cooling to room temperature, adding 2-5 parts of diammonium hydrogen phosphate, uniformly mixing, aging, filtering, washing, drying, and cooling to room temperature after calcination to obtain the antibacterial modification aid.
6. The method for preparing the crease-resistant suit fabric according to claim 2, wherein in S1, the crease-resistant coating is prepared according to the following process: uniformly mixing the waterborne polyurethane, the montmorillonite and the distilled water, heating to the temperature of 110-.
7. The method for preparing crease-resistant suit fabric according to claim 1, wherein in S1, the modified adhesive comprises the following raw materials in parts by weight: 20-30 parts of polyurethane, 4-8 parts of ethanol cellosolve acetate, 3-9 parts of butyl cellosolve acetate, 2-6 parts of ethyl cellosolve, 2-5 parts of ethyl cellulose, 4-8 parts of polyvinyl acetate, 2-8 parts of hydroxyethyl methacrylate, 1-5 parts of isooctyl acrylate, 4-8 parts of ammonium persulfate, 3-6 parts of sodium bisulfite, 2-5 parts of tributyl citrate, 4-8 parts of itaconic acid and 1-8 parts of nano zinc oxide.
8. The method for preparing crease-resistant suit fabric according to claim 7, wherein in S1, the modified adhesive is prepared by the following process: uniformly mixing polyurethane, ethanol cellosolve acetate, butyl cellosolve acetate and ethyl cellosolve, heating to 60-90 ℃, preserving heat for 20-30min, stirring at the rotating speed of 650 plus 850r/min for 1-2h, and cooling to room temperature to obtain a material A; uniformly mixing ethyl cellulose, polyvinyl acetate, hydroxyethyl methacrylate, isooctyl acrylate, ammonium persulfate, sodium bisulfite, tributyl citrate, itaconic acid and nano zinc oxide, heating to 85-95 ℃, preserving heat for 30-50min, stirring at the rotating speed of 1500-2500r/min for 10-30min, and cooling to room temperature to obtain a material B; heating the material B to 90-110 ℃, then adding the material A to be uniformly mixed, continuously heating to 120-.
9. The method for preparing the crease-resistant suit fabric according to claim 1, wherein in S1, the temperature of the primary drying treatment is 40-50 ℃, and the time of the primary drying treatment is 1-2 h.
10. The method for preparing crease-resistant suit fabric according to claim 1, wherein in S4, the temperature of the secondary drying treatment is 80-90 ℃, and the time of the secondary drying treatment is 30-60 min.
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