CN112998024A - Insecticidal composition containing fenoxycarb and application thereof - Google Patents
Insecticidal composition containing fenoxycarb and application thereof Download PDFInfo
- Publication number
- CN112998024A CN112998024A CN201911322906.4A CN201911322906A CN112998024A CN 112998024 A CN112998024 A CN 112998024A CN 201911322906 A CN201911322906 A CN 201911322906A CN 112998024 A CN112998024 A CN 112998024A
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- CN
- China
- Prior art keywords
- fenoxycarb
- bait
- percent
- accounts
- metaflumizone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000005898 Fenoxycarb Substances 0.000 title claims abstract description 89
- 239000000203 mixture Substances 0.000 title claims abstract description 88
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- 230000000749 insecticidal effect Effects 0.000 title claims abstract description 21
- 239000005914 Metaflumizone Substances 0.000 claims abstract description 50
- MIFOMMKAVSCNKQ-HWIUFGAZSA-N Metaflumizone Chemical compound C1=CC(OC(F)(F)F)=CC=C1NC(=O)N\N=C(C=1C=C(C=CC=1)C(F)(F)F)\CC1=CC=C(C#N)C=C1 MIFOMMKAVSCNKQ-HWIUFGAZSA-N 0.000 claims abstract description 47
- 239000005907 Indoxacarb Substances 0.000 claims abstract description 27
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- VBCVPMMZEGZULK-NRFANRHFSA-N indoxacarb Chemical compound C([C@@]1(OC2)C(=O)OC)C3=CC(Cl)=CC=C3C1=NN2C(=O)N(C(=O)OC)C1=CC=C(OC(F)(F)F)C=C1 VBCVPMMZEGZULK-NRFANRHFSA-N 0.000 claims abstract description 27
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/12—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/22—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom rings with more than six members
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/38—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< where at least one nitrogen atom is part of a heterocyclic ring; Thio analogues thereof
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a composition and application thereof, the composition comprises an active component A and an active component B, the A is fenoxycarb, the active component B is one selected from indoxacarb, metaflumizone, spinosad and spinetoram, the insecticidal spectrum and the application field are expanded through the synergistic effect of the active compounds, the insect state of each stage of the whole life cycle of pests can be effectively controlled, the pesticide dosage is reduced, and the drug resistance is delayed.
Description
Technical Field
The invention relates to an insecticidal composition, in particular to a compound insecticidal composition containing fenoxycarb, which is used for preventing and treating pests in the health, forestry and invasion.
Technical Field
The invention belongs to the technical field of pest control, and also belongs to the technical field of pest control in sanitation, forestry and invasion. The active composition of the invention is used for preventing and controlling pests in the health, forestry and invasion.
CN201210095190.0 relates to an ultra-low volume liquid containing metaflumizone and insect growth regulator insecticide, wherein the insect growth regulator is selected from chlorfluazuron, hexaflumuron, chlorbenzuron, diflubenzuron, buprofezin, fenoxycarb, tebufenozide and the like, and the ultra-low volume liquid is used for preventing and controlling crop pests such as rice planthopper, chilo suppressalis, peach fruit borer, thrips and the like. CN201210095190.0 does not disclose a compound composition of fenoxycarb and metaflumizone.
EP2010064995W relates to a polymeric granule for improving the soil migration of pesticides, the granule active ingredient being selected from at least one of the following sparingly soluble pesticides: fipronil, allethrin, bifenthrin, pyrethrum, chlorantraniliprole, fluxapyroxad, cyantraniliprole, cyfluthrin, cypermethrin, deltamethrin, ethofenprox, fenoxycarb, flufenoxuron, hydramethylnon, imidacloprid, pyriproxyfen, metaflumizone, tetrabromthrin and the like, and is used for controlling underground pests. EP2010064995W does not disclose a combination of fenoxycarb and metaflumizone.
Fenoxycarb (fenoxycarb) is an insect growth regulator which is marketed in the 80 th of the 20 th century, belongs to bionic juvenile hormone (IRAC 7B), controls the growth and development of pests, interferes the peeling of early-aged larvae, inhibits the larvae from becoming adults, and produces physiological deformity to make the larvae die because of not maturing; also has strong ovicidal activity. Fenoxycarb has high activity on many larvae of lepidoptera, coleoptera, diptera, hymenoptera and other pests, has poor activity on adult pests, has slow drug effect, has low toxicity on mammals and has little influence on the environment.
The indoxacarb, metaflumizone, spinosad and other compounds act on nerves/muscles or breath, the drug effect is quick, the ovicidal activity is poor, and the drug resistance is easy to generate after long-term use; the active compound has low toxicity, and can be used for preventing and treating pests in the fields of hygiene, forestry and the like. The prior art does not disclose the combination of fenoxycarb with these insecticides and the applicants have unexpectedly found that when these two classes of insecticidal active ingredients are combined, there is an excellent synergistic effect.
Disclosure of Invention
The invention provides an efficient and environment-friendly insecticidal composition applied to the non-agricultural fields of sanitation, forestry, invasive biology and the like.
The invention also aims to provide a preparation formula and application of the composition.
The above object of the present invention is achieved by the following technical solutions:
the insecticidal composition is characterized in that: the composition comprises an active component A and an active component B, wherein the A is fenoxycarb, and the active component B is one selected from indoxacarb, metaflumizone, spinosad and spinetoram in a mass ratio of 1: 99-99: 1.
The insecticidal composition is characterized in that: the active component B is one of indoxacarb, metaflumizone and pleocidin.
The insecticidal composition is characterized in that: the mass ratio of the active component A to the active component B is 1: 99-99: 1, preferably 1: 40-40: 1, and more preferably 1: 10-10: 1.
The invention also provides a formulation of the insecticidal composition. The preparation formula comprises an active composition and auxiliary components.
The insecticidal composition is prepared into various formulations according to a conventional method, including but not limited to suspending agents, missible oil, aqueous emulsion, micro-emulsion, oil suspending agents, microcapsule suspension-suspending agents, soluble solutions, wettable powder, water dispersible granules, baits, powder and aerosol. The appropriate dosage form is selected according to actual conditions.
The auxiliary components can be wetting agent, dispersant, emulsifier, disintegrant, antifreezing agent, attractant, preservative, defoaming agent, thickening agent, acid-base regulator, binder, solvent, granule carrier, bait, filler, etc.
The wetting agent includes, but is not limited to, one or more of fatty alcohol polyoxyethylene ether, alkylphenol polyoxyethylene ether, alkyl sulfate, naphthalene sulfonate, alkyl succinate sulfonate and alkylphenol polyoxyethylene ether formaldehyde condensate sulfonate;
the dispersant includes but IS not limited to one or more of polyether phosphate and its salt, alkylphenol polyoxyethylene ether formaldehyde condensate sulfonate, polycarboxylate, block polyether, phenethylphenol polyoxyethylene ether phosphate triethanolamine salt, naphthalene sulfonate formaldehyde condensate, lignosulfonate, nekal, NNO, MF and IS dispersing;
the emulsifier includes but is not limited to one or more of polyether phosphate, T-60, calcium dodecylbenzene sulfonate, ethylene oxide propylene oxide block copolymer, fatty alcohol polyoxyethylene ether, castor oil polyoxyethylene ether, alkylphenol polyoxyethylene ether, calcium alkyl benzene sulfonate and block polyether;
the disintegrant includes, but is not limited to, one or more of ammonium sulfate, sodium sulfate, glucose, corn starch, ammonium chloride, bentonite, urea, and sodium bicarbonate;
the antifreeze agent comprises but is not limited to one or more of ethylene glycol, propylene glycol, glycerol, sodium chloride, urea, cellosolve, sorbitol, polyvinylpyrrolidone and calcium chloride;
the attractant comprises but is not limited to animal and vegetable oil, lard, soybean oil, peanut oil, rapeseed oil, sesame oil, corn oil, cottonseed oil and wheat germ oil; sugar, glucose, sucrose, fructose, brown sugar, and Mel.
The preservative includes but is not limited to one or more of sodium benzoate, potassium sorbate, sodium dehydroacetate, sodium diacetate, cason, paraben or their sodium salts, bronopol, pentanediol and sodium salicylate;
the antifoaming agent includes, but is not limited to, one or more of silicone compounds, lower alcohols, silicone oils, phosphate esters, and fatty acids and fatty acid esters;
the thickening agent includes but is not limited to xanthan gum, gas phase SiO2One or more of bentonite, aluminum stearate, gelatine powder, polyvinyl alcohol, modified cellulose, magnesium aluminium silicate, acacia, gum, gelatin, guar gum, alginic acid, agar, and tall oil;
the pH modifier includes, but is not limited to, one or more of citric acid, oxalic acid, ammonium chloride, tartaric acid and succinic acid;
the solvent includes but is not limited to C6-C30One or more of isoparaffin or dearomatized solvent oil, low-toxicity tasteless monoester such as methyl laurate, diethyl maleate, tributyl phosphate and the like, diester or triester solvents, diisooctyl phthalate, trans-2-hexenol, diesel oil, diisopropyl diacid, dimethyl phthalate, vegetable oil, engine oil and dimethyl sulfoxide;
the granule carrier comprises but is not limited to one or more of attapulgite particles, volcanic rock particles, red brick particles, coal gangue particles, medical stone particles, zeolite particles, corncob particles and walnut shell particles with better adsorption performance;
the bait comprises but is not limited to one or more of wheat flour, soybean flour, corn flour, potato flour, biscuit flour, grain flour and peanut flour;
the filler includes but is not limited to one or more of kaolin, white carbon black, china clay, bentonite, attapulgite, diatomite, white carbon black and light calcium carbonate;
the preparation prepared from the composition is used directly or after being diluted by a solvent, and the application method is selected according to the properties of the composition according to the purpose to be achieved and the environment, and the pests or the habitats thereof are treated by spraying, ultralow volume, retention spraying, hot smoke, spraying, powder spraying, broadcasting, feeding, watering and the like.
The insecticidal composition is suitable for controlling sanitary pests, in particular for controlling sanitary pests in the places of environmental sanitation, families, public places, commercial places, production places, farms, warehouses, public transportation and the like.
Wherein the hygiene pests include, but are not limited to, mosquitoes (e.g., Aedes aegypti, Aedes albopictus, Aedes spinosa, Culex fatigues, Culex pallens, Culex haranthii, Culex pipiens, Culex muricatus, Culex gambiae, Anopheles arabica, Anopheles nigricans, Anopheles minutus, Anopheles macrolepis, Anopheles schoensis, Anopheles sinensis, Anopheles anthropophagus, etc.); flies (houseflies, commond flies, maggot-causing flies, bovines, blowflies, dermatoglyphos, gastrointestinal flies, trypanosoma anthropophagi, etc.); biting midges (e.g., Culicoides), gnats (e.g., gnats); blatta Seu Periplaneta (such as Blattella germanica, Periplaneta americana, Periplaneta australis, Periplaneta fusca, Periplaneta fuliginosa, etc.); ants (such as black ant, little yellow ant, etc.); fleas (e.g., manfleas, xenorhabdus, ctenocephalides canis, ctenocephalides felis, etc.); lice (e.g., pediculus humanus, lice of swine, lice of sheep and livestock, etc.); bed bugs (e.g., cimex fusca, rhynchophorus ferrugineus, etc.); ticks (e.g., scleroderma ricini, scleroderma acrosus, Boophilus microplus, Ornithoides africana, Rhipicephalus columba, etc.); mites (e.g., sarcoptidosis, Dermanychus gallinae, Dermatophagoides farinae, Farnesh mites, etc.).
The insecticidal composition is suitable for controlling forestry pests, including but not limited to fall webworms, pine moths (such as pine caterpillar, larch caterpillar, masson pine caterpillar and the like), moths (such as gypsy moth, willow moth and the like), boat moths (such as poplars and poplarch boat moths and the like), scale moths (such as wood inchworm, large bridgeworm, pear scale moths and the like), longicorn (such as celesta chinensis, monochamus alternatus, longicorn, and the like).
The insecticidal composition is suitable for controlling solenopsis invicta as an invading organism, and is particularly suitable for controlling solenopsis invicta in places such as parks, schools, factories, greenbelts, lawns, forest lands, farmlands, orchards, wastelands and the like.
Compared with the prior art, the invention has the beneficial effects that:
(1) the insect growth regulator is compounded with the insecticide acting on nerve/muscle/breath, has complementary advantages, can effectively control the insect state of each stage of the whole life cycle of pests, reduces the using amount of the insecticide and delays the drug resistance.
(2) The active components of the invention have large difference of action mechanism, and have obvious synergistic effect on pests such as mosquitoes, fleas, fall webworms, red imported fire ants and the like after being compounded.
(3) The insecticidal composition of the invention has low toxicity, high efficiency and environmental protection, and is suitable for preventing and treating pests in the non-agricultural fields of sanitation, forestry, grassland and the like.
Detailed Description
The present invention is further illustrated by the following examples, which are not intended to limit the invention to these embodiments. It will be appreciated by those skilled in the art that the present invention encompasses all alternatives, modifications and equivalents as may be included within the scope of the claims.
Bait formulation example 1: fenoxycarb bait (0.1%)
The bait agent of the embodiment takes fenoxycarb as an active ingredient, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the active ingredient fenoxycarb accounts for 0.1 percent, the bait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the preservative potassium sorbate accounts for 0.5 percent in percentage by weight.
Bait example 2: fenoxycarb metaflumizone bait (total content 0.1%, 99:1)
The bait agent takes fenoxycarb and metaflumizone as active ingredients, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the metaflumizone (99:1) as the active ingredients accounts for 0.1 percent, the content of the cyhalothrin soybean meal accounts for 64.4 percent, the content of the attractant mixture accounts for 35 percent, and the content of the potassium sorbate as the preservative accounts for 0.5 percent.
Bait example 3: fenoxycarb metaflumizone bait (total content 0.1%, 40:1)
The bait agent takes fenoxycarb and metaflumizone as active ingredients, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the total content of the active ingredients of fenoxycarb and metaflumizone (40:1) is 0.1 percent, the content of the cyhalothrin soybean meal is 64.4 percent, the content of the attractant mixture is 35 percent, and the preservative of the potassium sorbate is 0.5 percent by weight.
Bait example 4: fenoxycarb metaflumizone bait (total content 0.1%, 10:1)
The bait agent takes fenoxycarb and metaflumizone as active ingredients, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the metaflumizone (10:1) as the active ingredients accounts for 0.1 percent, the content of the cyhalothrin soybean meal accounts for 64.4 percent, the content of the attractant mixture accounts for 35 percent, and the content of the potassium sorbate as the preservative accounts for 0.5 percent.
Bait example 5: fenoxycarb metaflumizone bait (total content 0.1%, 5:1)
The bait agent takes fenoxycarb and metaflumizone as active ingredients, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the total content of the active ingredients of fenoxycarb and metaflumizone (5:1) is 0.1 percent, the content of the cyhalothrin soybean meal is 64.4 percent, the content of the attractant mixture is 35 percent, and the preservative of the potassium sorbate is 0.5 percent by weight.
Bait example 6: fenoxycarb metaflumizone bait (total content 0.1%, 1:1)
The bait agent takes fenoxycarb and metaflumizone as active ingredients, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the metaflumizone (1:1) as the active ingredients accounts for 0.1 percent, the content of the cyhalothrin soybean meal accounts for 64.4 percent, the content of the attractant mixture accounts for 35 percent, and the content of the potassium sorbate as the preservative accounts for 0.5 percent.
Bait example 7: fenoxycarb metaflumizone bait (total content 0.1%, 1:5)
The bait agent takes fenoxycarb and metaflumizone as active ingredients, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the total content of the active ingredients, fenoxycarb and metaflumizone (1:5), is 0.1 percent, the content of the cyhalothrin soybean meal is 64.4 percent, the content of the attractant mixture is 35 percent, and the preservative, potassium sorbate, is 0.5 percent.
Bait example 8: fenoxycarb metaflumizone bait (total content 0.1%, 1:10)
The bait agent takes fenoxycarb and metaflumizone as active ingredients, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the metaflumizone (1:10) as the active ingredients accounts for 0.1 percent, the content of the cyhalothrin soybean meal accounts for 64.4 percent, the content of the attractant mixture accounts for 35 percent, and the content of the potassium sorbate as the preservative accounts for 0.5 percent.
Bait example 9: fenoxycarb metaflumizone bait (total content 0.1%, 1:40)
The bait agent takes fenoxycarb and metaflumizone as active ingredients, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the metaflumizone (1:40) as the active ingredients accounts for 0.1 percent, the content of the cyhalothrin soybean meal accounts for 64.4 percent, the content of the attractant mixture accounts for 35 percent, and the content of the potassium sorbate as the preservative accounts for 0.5 percent.
Bait example 10: fenoxycarb metaflumizone bait (total content 0.1%, 1:99)
The bait agent takes fenoxycarb and metaflumizone as active ingredients, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as an attractant for solenopsis invicta, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the metaflumizone (1:99) as the active ingredients accounts for 0.1 percent, the content of the cyhalothrin soybean meal accounts for 64.4 percent, the content of the attractant mixture accounts for 35 percent, and the content of the potassium sorbate as the preservative accounts for 0.5 percent.
Bait example 11: metaflumizone bait (0.1%)
The bait agent takes metaflumizone as an active ingredient, soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the active ingredient is the metaflumizone accounting for 0.1 percent, the cyanogen bait soybean meal accounting for 64.4 percent, the attractant mixture accounting for 35 percent, and the preservative is the potassium sorbate accounting for 0.5 percent by weight.
Bait example 12: indoxacarb bait (0.1%)
The bait agent of the embodiment takes the indoxacarb as an active ingredient, the soybean meal as bait, a mixture (the mixing ratio is 1:0.2:2) of honey, peanut oil and cane sugar as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the indoxacarb accounts for 0.1 percent, the cyanogen bait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the preservative potassium sorbate accounts for 0.5 percent in percentage by weight.
Bait example 13: fenoxycarb indoxacarb bait (total content 0.1%, 40:1)
The bait agent of the embodiment takes fenoxycarb and indoxacarb as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the indoxacarb (40:1) as the active ingredients accounts for 0.1 percent, the cyanogen bait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Bait example 14: fenoxycarb indoxacarb bait (total content 0.1%, 10:1)
The bait agent of the embodiment takes fenoxycarb and indoxacarb as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the indoxacarb (10:1) as the active ingredients accounts for 0.1 percent, the cyanogen bait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Bait example 15: fenoxycarb indoxacarb bait (total content 0.1%, 1:1)
The bait agent of the embodiment takes fenoxycarb and indoxacarb as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the indoxacarb (1:1) as the active ingredients accounts for 0.1 percent, the cyanogen bait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Bait example 16: fenoxycarb indoxacarb bait (total content 0.1%, 1:10)
The bait agent of the embodiment takes fenoxycarb and indoxacarb as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the indoxacarb (1:10) as the active ingredients accounts for 0.1 percent, the cyanogen bait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Bait example 17: fenoxycarb indoxacarb bait (total content 0.1%, 1:40)
The bait agent of the embodiment takes fenoxycarb and indoxacarb as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the indoxacarb (1:40) as the active ingredients accounts for 0.1 percent, the cyanogen bait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Bait example 18: pleocidin bait agent (0.1%)
The bait agent of the embodiment takes the spinosad as an active ingredient, adopts the soybean meal as bait, adopts a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and adopts the potassium sorbate as a preservative, wherein the spinosad accounts for 0.1 percent, the cyanogen bait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the preservative potassium sorbate accounts for 0.5 percent in percentage by weight.
Bait example 19: fenoxycarb pleocidin bait (total content 0.1%, 10:1)
The bait agent takes fenoxycarb and spinosad as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the spinosad (10:1) as the active ingredients accounts for 0.1 percent, the cyhalocarb soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Bait example 20: fenoxycarb pleocidin bait (total content 0.1%, 5:1)
The bait agent takes fenoxycarb and spinosad as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the spinosad (5:1) as the active ingredients accounts for 0.1 percent, the cyanobait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Bait example 21: fenoxycarb pleocidin bait (total content 0.1%, 1:1)
The bait agent takes fenoxycarb and spinosad as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the spinosad (1:1) as the active ingredients accounts for 0.1 percent, the cyanobait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Bait example 22: fenoxycarb pleocidin bait (total content 0.1%, 1:5)
The bait agent takes fenoxycarb and spinosad as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the spinosad (1:5) as the active ingredients accounts for 0.1 percent, the cyanobait soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Bait example 23: fenoxycarb pleocidin bait (total content 0.1%, 1:10)
The bait agent takes fenoxycarb and spinosad as active ingredients, soybean meal as bait, a mixture of honey, peanut oil and cane sugar (the mixing ratio is 1:0.2:2) as a solenopsis invicta attractant, and potassium sorbate as a preservative, wherein the total content of the fenoxycarb and the spinosad (1:10) as the active ingredients accounts for 0.1 percent, the cyhalocarb soybean meal accounts for 64.4 percent, the attractant mixture accounts for 35 percent, and the potassium sorbate as the preservative accounts for 0.5 percent in percentage by weight.
Application example 1: indoor test of mosquito larvae
Test subjects: culex pipiens pallens, larvae of 3 years old, indoor sensitive strain.
Test agents: respectively weighing fenoxycarb, pleocidin, indoxacarb and metaflumizone, adding an appropriate amount of acetone for dissolving, adding distilled water to prepare mother liquor with a required concentration, and mixing the mother liquor according to a certain proportion to prepare mixed mother liquor.
The test method comprises the following steps: reference pesticide registration sanitary insecticide indoor efficacy test and evaluation part 5: the mosquito larva control agent NY/T1151.5-2014 is prepared by taking white porcelain pots with the diameter of 30cm and the depth of 10cm, putting 4L of clear water into the pots, putting 50 heads of 3-instar larvae of healthy culex pipiens pallens into each pot, adding the prepared agent according to the dosage according to the water area in the pots, observing the death and pupation conditions of the larvae every day, and taking the pupae out to observe the eclosion condition of the larvae. Three replicates were used and a blank control was set.
And (3) test results: referring to table 1, fenoxycarb compound medicament has killing effect on both larva and pupa by using different action mechanisms, and the prevention and treatment rate is higher than that of single medicament under the same dosage.
TABLE 1 killing effect of fenoxycarb compound on mosquito larvae and pupae
Application example 2: indoor test for fleas
Test subjects: cyperus bigelovii, ovum.
Reagent to be tested: dissolving fenoxycarb, indoxacarb, metaflumizone and spinetoram active compounds in absolute ethyl alcohol respectively, and diluting with water to prepare the required mother liquor.
The test method comprises the following steps: preparing the mother liquor into a series of concentrations by adopting an immersion method; transferring the eggs to a beaker with liquid medicine, treating the eggs with the liquid medicine, and transferring the eggs to a normal condition for culture; repeating for 3 times, and setting clear water control, wherein each cup contains 20 eggs; and (5) surveying and recording the number of hatched eggs and the number of dead eggs, and calculating the egg death rate.
The evaluation method comprises the following steps: the method is one of the classical methods for evaluating the effect of the mixture by adopting a Colby formula. The Colby formula is as follows: e ═ X + Y- (X × Y)/100.
Wherein X is the mortality in m ppm of active compound A, expressed as a percentage of the untreated control; y is the mortality rate at an application rate of n ppm of active compound B, expressed as a percentage of the untreated control, and E is the mortality rate at an application rate of m + n ppm of active compounds A and B, expressed as a percentage of the untreated control.
If the actual mortality rate of the target after the two active ingredients are mixed at a certain concentration is greater than the theoretical mortality rate E, the two active ingredients are judged to have synergistic effect when being mixed at a set concentration, otherwise, the two active ingredients are antagonistic.
And (3) test results: referring to Table 2, fenoxycarb and indoxacarb/flumizone/spinetoram combinations have synergistic effects on eggs of Trichoplusia.
TABLE 2 killing effect of fenoxycarb compound on eggs of paddlefish fleas
Application example 3: solenopsis invicta field control test
Test subject and test site: red imported fire ant, post-ant type; quanzhou Jinjiang inner hole town.
Test agents: bait examples 1-23.
Test protocol: reference pesticide field efficacy test criteria (second) section 149: the insecticide controls solenopsis invicta GB/T7980.149-2009, there were 7 treatments (examples 1-23) and 1 blank control in the test, 3 replicates, each treatment was preceded by a 3-5 meter spacer; the ground surface temperature is 20-35 ℃, the pesticide is applied when the ground surface is dry, the pesticide is annularly spread in a range of 30-100 cm away from the ant nest, the dosage of the preparation is 15-30 g/nest, and the preparation needs to be applied in a complementary manner when raining within 2 days after the pesticide is applied; the density of workers (fresh ham sausage sheet trapping method) was investigated 4 times before application, 7 days, 30 days and 45 days after application.
And (3) test results: in table 3, compared with a single dose, the fenoxycarb compound solenopsis invicta bait has a higher prevention and treatment rate and a longer effective period than the single dose under the same prevention and treatment dose.
TABLE 3 Figwort prevention and cure effect of fenoxycarb compound bait agent
Application example 4: laboratory test of fall webworm
Test subjects: fall webworm, 3 instar larva.
Reagent to be tested: dissolving fenoxycarb, spinosad, spinetoram and metaflumizone with absolute ethyl alcohol respectively, and preparing the required mother liquor by using an aqueous solution containing 0.1% of tween 80.
The test method comprises the following steps: preparing the mother liquor into a series of concentrations by adopting an immersion method; soaking fresh poplar leaves which are not polluted by the pesticide in the liquid medicine to be tested for 5s, taking out the poplar leaves, drying the poplar leaves in the shade, wrapping petioles with absorbent cotton, soaking the cotton leaves in clear water, putting the cotton leaves into a plastic cup, testing insects for 15 times in each cup, repeating the steps for 3 times, and establishing clear water contrast; the eggs are placed under the conditions of humidity of 75%, temperature of 24 ℃ and illumination of 14:10(L: D) for feeding, and the number of dead insects and the total number of insects are investigated and recorded after 72 hours.
Performing statistical analysis by POLO statistical analysis software to calculate LC of each medicine50And calculating the co-toxicity coefficient (CTC value) of the mixture according to the Sun Yunpei method.
Measured toxicity index (ATI) ═ standard medicament LC50Test agent LC50)×100。
Theoretical virulence index (TTI) ═ a agent virulence index x percent of a in the mixture + B agent virulence index x percent of B in the mixture.
Co-toxicity coefficient (CTC) × 100 [ measured toxicity index (ATI) of the mixture)/Theoretical Toxicity Index (TTI) of the mixture ].
According to NY/T1154.7-2006 pesticide combination division standard: the co-toxicity coefficient (CTC) is more than or equal to 120 and shows a synergistic effect; the co-toxicity coefficient (CTC) is less than or equal to 80, and the antagonism is shown; 80 < co-toxicity coefficient (CTC) < 120 showed additive effects.
And (3) test results: as shown in Table 4, when the ratio of fenoxycarb to spinosad is 99: 1-1: 99, the synergistic effect is shown, and when the ratio is 10: 1-1: 10, the co-toxicity coefficient is the highest and exceeds 167.75; when the ratio of fenoxycarb to metaflumizone/spinetoram is 40: 1-1: 40, the cotoxicity coefficients are all more than 120, and the synergistic effect is shown.
TABLE 4 indoor joint toxicity determination of fenoxycarb compound mixture to fall webworm
| Medicament and proportion | LC50(mg/L) | ATI | TTI | CTC |
| Fenoxycarb | 11.43 | 100.00 | — | — |
| Spinosad | 2.13 | 536.62 | — | — |
| Fenoxycarb-spinosad 99:1 | 8.22 | 138.99 | 104.37 | 133.17 |
| Fenoxycarb-pleocidin-40: 1 | 6.55 | 174.55 | 110.65 | 157.75 |
| Fenoxycarb-pleocidin-10: 1 | 4.34 | 263.62 | 139.69 | 188.72 |
| Fenoxycarb-pleocidin-5: 1 | 3.69 | 309.43 | 172.78 | 179.09 |
| Fenoxycarb-pleocidin-1: 1 | 2.12 | 541.64 | 318.31 | 170.16 |
| Fenoxycarb-pleocidin-1: 5 | 1.51 | 778.09 | 463.84 | 167.75 |
| Fenoxycarb-pleocidin-1: 10 | 1.17 | 978.60 | 496.93 | 196.93 |
| Fenoxycarb-spinosad 1:40 | 1.57 | 729.90 | 523.53 | 139.42 |
| Fenoxycarb-spinosad 1:99 | 1.74 | 656.74 | 532.25 | 123.39 |
| Spinetoram | 1.35 | 846.67 | — | — |
| Fenoxycarb-spinetoram 40:1 | 6.65 | 171.80 | 118.22 | 145.32 |
| Fenoxycarb-spinetoram-10: 1 | 3.72 | 307.62 | 167.87 | 183.25 |
| Fenoxycarb-spinetoram-1: 1 | 1.46 | 783.33 | 473.34 | 165.49 |
| Fenoxycarb-spinetoram-1: 5 | 1.00 | 1140.57 | 722.20 | 157.93 |
| Metaflumizone | 6.43 | 177.76 | — | — |
| Fenoxycarb-metaflumizone 40:1 | 8.23 | 138.90 | 101.90 | 136.31 |
| Fenoxycarb-metaflumizone 10:1 | 5.99 | 190.93 | 107.07 | 178.32 |
| Fenoxycarb-metaflumizone 1:1 | 5.20 | 219.64 | 138.88 | 158.15 |
| Fenoxycarb metaflumizone 1:10 | 4.00 | 285.41 | 170.69 | 167.21 |
| Fenoxycarb metaflumizone 1:40 | 5.03 | 227.46 | 175.86 | 129.34 |
The insecticidal composition containing methoprene and the application thereof have been described by specific examples, and other objects can be achieved by appropriate changes of raw materials and process conditions without departing from the invention, which is obvious for those skilled in the art and is considered to be included in the scope of the invention.
Claims (7)
1. An insecticidal composition characterized by: the composition comprises an active component A and an active component B, wherein the A is fenoxycarb, and the active component B is one selected from indoxacarb, metaflumizone, spinosad and spinetoram in a mass ratio of 1: 99-99: 1.
2. The insecticidal composition of claim 1, wherein: the active component B is further selected from one of indoxacarb, metaflumizone and spinosad.
3. The insecticidal composition according to claims 1-2, characterized in that: the mass ratio of the active component A to the active component B is preferably 1: 40-40: 1, and more preferably 1: 10-10: 1.
4. The field of application of pesticidal compositions according to claims 1-4 for controlling pests, characterized in that: the application field is prevention and control of pests in the health, forestry and invasion.
5. The field of use of insecticidal compositions according to claim 5 for the control of pests, characterized in that said hygiene pests include but are not limited to mosquitoes, flies, cockroaches, ants, fleas, lice, bed bugs, ticks, mites, further preferably mosquitoes, fleas.
6. The field of use of pesticidal compositions to control pests according to claim 5, characterized in that said forestry pests include but are not limited to fall webworm, pine moth, boat moth, foot moth, further preferably fall webworm.
7. The field of use of pesticidal compositions according to claim 5 for the control of pests, characterized in that said invading pest is solenopsis invicta.
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| CN116584504A (en) * | 2023-05-26 | 2023-08-15 | 河南农王实业有限公司 | A kind of agricultural composition containing fenoxycarb and spinosad |
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| CN102986712A (en) * | 2011-09-14 | 2013-03-27 | 山东康乔生物科技有限公司 | Insecticidal composition containing dinotefuran and abamectin |
| CN103385251A (en) * | 2012-05-12 | 2013-11-13 | 陕西韦尔奇作物保护有限公司 | Insecticidal composition comprising pyriproxyfen |
| CN105532714A (en) * | 2015-11-30 | 2016-05-04 | 浙江新安化工集团股份有限公司 | Safe, environment-friendly and efficient insecticidal composition and use thereof |
| CN107787977A (en) * | 2017-08-28 | 2018-03-13 | 南通功成精细化工有限公司 | A kind of hygienic biocide composition containing Nylar and its application |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102986712A (en) * | 2011-09-14 | 2013-03-27 | 山东康乔生物科技有限公司 | Insecticidal composition containing dinotefuran and abamectin |
| CN103385251A (en) * | 2012-05-12 | 2013-11-13 | 陕西韦尔奇作物保护有限公司 | Insecticidal composition comprising pyriproxyfen |
| CN105532714A (en) * | 2015-11-30 | 2016-05-04 | 浙江新安化工集团股份有限公司 | Safe, environment-friendly and efficient insecticidal composition and use thereof |
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| CN116584504A (en) * | 2023-05-26 | 2023-08-15 | 河南农王实业有限公司 | A kind of agricultural composition containing fenoxycarb and spinosad |
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