CN1141981A - Coating agent to make fabric stiff - Google Patents
Coating agent to make fabric stiff Download PDFInfo
- Publication number
- CN1141981A CN1141981A CN 95118068 CN95118068A CN1141981A CN 1141981 A CN1141981 A CN 1141981A CN 95118068 CN95118068 CN 95118068 CN 95118068 A CN95118068 A CN 95118068A CN 1141981 A CN1141981 A CN 1141981A
- Authority
- CN
- China
- Prior art keywords
- emulsion
- add
- polyvinyl alcohol
- coating agent
- acrylic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000004744 fabric Substances 0.000 title claims description 17
- 239000011248 coating agent Substances 0.000 title claims description 15
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 47
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 45
- 239000000839 emulsion Substances 0.000 claims abstract description 38
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 22
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 22
- 229920002678 cellulose Polymers 0.000 claims abstract description 17
- 239000001913 cellulose Substances 0.000 claims abstract description 17
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 9
- 239000010985 leather Substances 0.000 claims abstract description 9
- 239000002184 metal Substances 0.000 claims abstract description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims abstract 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 20
- 239000011230 binding agent Substances 0.000 claims description 19
- 241001465754 Metazoa Species 0.000 claims description 16
- 239000003760 tallow Substances 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 12
- 239000008367 deionised water Substances 0.000 claims description 10
- 229910021641 deionized water Inorganic materials 0.000 claims description 10
- 239000013530 defoamer Substances 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 4
- 235000013336 milk Nutrition 0.000 claims description 3
- 239000008267 milk Substances 0.000 claims description 3
- 210000004080 milk Anatomy 0.000 claims description 3
- 239000005018 casein Substances 0.000 claims description 2
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims description 2
- 235000021240 caseins Nutrition 0.000 claims description 2
- 235000020251 goat milk Nutrition 0.000 claims description 2
- 206010044565 Tremor Diseases 0.000 claims 1
- 239000004753 textile Substances 0.000 abstract 2
- 235000019737 Animal fat Nutrition 0.000 abstract 1
- 235000011187 glycerol Nutrition 0.000 abstract 1
- 239000002960 lipid emulsion Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 8
- 238000010792 warming Methods 0.000 description 5
- 238000009472 formulation Methods 0.000 description 4
- 238000005303 weighing Methods 0.000 description 4
- 238000005498 polishing Methods 0.000 description 3
- 239000000020 Nitrocellulose Substances 0.000 description 2
- 229920000180 alkyd Polymers 0.000 description 2
- 229920001220 nitrocellulos Polymers 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 235000019082 Osmanthus Nutrition 0.000 description 1
- 241000333181 Osmanthus Species 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 239000012296 anti-solvent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000675 fabric finishing Substances 0.000 description 1
- 238000009962 finishing (textile) Methods 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The finishing agent for making textile stiff comprises 20-50% propenoic acid systhesis emulsion, 10-30% of animal-fat emulsion, 3-8% of polyvinyl alcohol, 1-5% of cellulose, 0.5-4% of formaldehyde and 1-5% of glycerin, which can be used not only for textile but also for leather, metal anti-rust, flowers and plants and skin-care of humanbody etc.. Said finishing agent has the advantage of good brightness, protection function, and film-forming characteristics, heat-resisting, water-resisting and oil-resisting.
Description
The invention relates to a kind of fabric finishing agent, more particularly about a kind of coating agent to make fabric stiff and preparation method thereof.
In the prior art, various in style about the stiffening finishing agent of fabric, clothes.Usually, they all are made of as main body acrylic emulsion, polyurethane, oxirane etc., especially, also have to use and melt after the polyvinyl chloride heating on fabric and make fabric stiffening, but these and product of the present invention are completely different.Also there are many pieces of bibliographical informations to cross leather finishing agent, for example in CN-89105920, disclose a kind of aqueous emulsion type leather top finishing material, it has formations such as nitrocellulose, the non-dryness modified alkyd resin of medium oil, the common alkyd resins of the non-dryness of long oil, esters solvent, hydrocarbon diluent and surfactant, although they also can invest leather substance light and delustring, and lasting aroma retaining effect is arranged, but their proportioning and the present invention there is tangible difference.
The object of the present invention is to provide a kind of coating agent to make fabric stiff and preparation method thereof.
Second purpose of the present invention is to provide the polishing coating agent of a kind of leather and fur products, clothes.
These and other objects of the present invention will further embody and illustrate by following detailed description.
In the present invention, coating agent to make fabric stiff [weight] comprising:
Acrylic acid synthetic emulsion 20-50%
Animal tallow emulsion 10-30%
Glycerol 1-5%
Defoamer 0.5-2%
Essence 0.1-3%
Formaldehyde 0.5-4%
Polyvinyl alcohol 99 3-8%
Cellulose 1-5%
Surplus is a water.
Further, coating agent to make fabric stiff of the present invention comprises:
Acrylic acid synthetic emulsion 30-40%
Animal tallow emulsion 15-25%
Glycerol 1-3%
Defoamer 1-2%
Essence 1-3%
Formaldehyde 1-3%
Polyvinyl alcohol 99 4-7%
Cellulose 3-5%
Surplus is a water.
Wherein, the acrylic acid synthetic emulsion comprises:
77# binding agent 10-40%, 107# binding agent 1-30%, all the other are any one binding agent of 07#-10#.
In the present invention, the animal tallow emulsion can be milk, goat milk, mare's milk and casein etc.Water is deionized water preferably.
In the present invention, all percentages all are weight percentage, and all raw material comprise 77#, 107#, 07#-10# binding agent, glycerol, polyvinyl alcohol 99 etc. all can have been bought from the market, and defoamer and cellulose are that chemical industry is commonly used, can be CMC, nitrocellulose etc. as cellulose.Being applied as directly of product of the present invention smears, and measures the amount doesn't matterly, decides on individual demand.If be necessary, can add suitable gas, use to make aerosol can shape.
Stiffening finishing agent of the present invention prepares as follows:
At first in reactor, add entry, heat up then, add polyvinyl alcohol, being warming up to more than 95 ℃ makes polyvinyl alcohol dissolve into liquid, add cellulose then, ceaselessly stir and make it evenly to become thick slightly liquid, reduce to normal temperature then, low speed (40-90rpm) stirred 20-40 minute add glycerol, formaldehyde in reactor after, add acrylic acid synthetic emulsion and animal tallow emulsion then, (300-1000rpm) stirred 20 minutes at a high speed, and low speed (40-90rpm) stirred 10 minutes again, add essence, stir evenly slightly and get product.
Stiffening finishing agent of the present invention, powers and functions are not used for fabric, but also can be applicable to aspects such as leather, metal, flowers and plants, human body skin care.Formula for a product of the present invention is reasonable, technology is simple, easy operation control, constant product quality, have good especially light and protectiveness, and good, low temperature resistant, the anti-solvent of filming performance, water-fast, heat-resisting.
Below further specify the present invention by specific embodiment, embodiment only be used for the explanation but can not limit the scope of the invention.
Example 1
By following proportioning all compositions of weighing:
Acrylic acid synthetic emulsion 40kg glycerol 2kg
Animal tallow emulsion 15kg defoamer 0.6kg
Essence 1kg formaldehyde 2kg
Polyvinyl alcohol 99 7kg cellulose (CMC) 1kg
31.4kg deionized water.
The acrylic acid synthetic emulsion is pressed following formulation ratio:
77# binding agent 35kg 107# binding agent 25kg
07# binding agent 40kg.
At first add deionized water in reactor, heat up gradually then, add polyvinyl alcohol, be warming up to 95 ℃, stirring makes polyvinyl alcohol dissolve into liquid, adds cellulose then, ceaselessly stirs and makes it evenly to become thick slightly liquid, reduces to normal temperature then; Low speed (90rpm) stirred 40 minutes after adding glycerol, formaldehyde afterwards, add acrylic acid synthetic emulsion and animal tallow emulsion then, (800rpm) stirred 20 minutes at a high speed, low speed (90rpm) stirred 10 minutes again, adding essence stirs slightly and promptly gets product, and this product can be made coating agent to make fabric stiff and use.
Example 2
By following proportioning all compositions of weighing:
Acrylic acid synthetic emulsion 50kg glycerol 2kg
Animal tallow emulsion 10kg defoamer 0.6kg
Essence 1kg formaldehyde 2kg
Polyvinyl alcohol 99 7kg cellulose (CMC) 1kg
26.4kg deionized water.
The acrylic acid synthetic emulsion is pressed following formulation ratio:
77# binding agent 30kg 107# binding agent 25kg
08# binding agent 45kg.
At first add deionized water in reactor, heat up gradually then, add polyvinyl alcohol, be warming up to 95 ℃, stirring makes polyvinyl alcohol dissolve into liquid, adds cellulose then, ceaselessly stirs and makes it evenly to become thick slightly liquid, reduces to normal temperature then; Low speed (90rpm) stirred 40 minutes after adding glycerol, formaldehyde afterwards, add acrylic acid synthetic emulsion and animal tallow emulsion then, (800rpm) stirred 20 minutes at a high speed, low speed (90rpm) stirred 10 minutes again, adding essence stirs slightly and promptly gets product, and this product can be made leather polishing coating agent and use.
Example 3
By following proportioning all compositions of weighing:
Acrylic acid synthetic emulsion 30kg glycerol 3kg
Animal tallow emulsion 15kg defoamer 0.6kg
Essence 1kg formaldehyde 1kg
Polyvinyl alcohol 99 5kg cellulose (CMC) 1kg
39.4kg deionized water.
The acrylic acid synthetic emulsion is pressed following formulation ratio:
77# binding agent 35kg 107# binding agent 25kg
10# binding agent 40kg.
At first add deionized water in reactor, heat up gradually then, add polyvinyl alcohol, be warming up to 95 ℃, stirring makes polyvinyl alcohol dissolve into liquid, adds cellulose then, ceaselessly stirs and makes it evenly to become thick slightly liquid, reduces to normal temperature then; Low speed (90rpm) stirred 40 minutes after adding glycerol, formaldehyde afterwards, add acrylic acid synthetic emulsion and animal tallow emulsion then, (800rpm) stirred 20 minutes at a high speed, low speed (90rpm) stirred 10 minutes again, adding essence stirs slightly and promptly gets product, and this product can be made leather polishing coating agent and use.
Example 4
By following proportioning all compositions of weighing:
Acrylic acid synthetic emulsion 20kg glycerol 2kg
Animal tallow 10kg defoamer 0.6kg
Fragrant osmanthus 1kg formaldehyde 2kg
Polyvinyl alcohol 99 7kg cellulose (CMC) 1kg
56.4kg deionized water.
The acrylic acid synthetic emulsion is pressed following formulation ratio:
77# binding agent 35kg 107# binding agent 25kg
09# binding agent 40kg.
At first add deionized water in reactor, heat up gradually then, add polyvinyl alcohol, be warming up to 95 ℃, stirring makes polyvinyl alcohol dissolve into liquid, adds cellulose then, ceaselessly stirs and makes it evenly to become thick slightly liquid, reduces to normal temperature then; Low speed (90rpm) stirred 40 minutes after adding glycerol, formaldehyde afterwards, add acrylic acid synthetic emulsion and animal tallow emulsion then, (800rpm) stirred 20 minutes at a high speed, and low speed (90rpm) stirred 10 minutes again, adding essence stirs slightly and promptly gets product, and this product can be made skin care products and use.
Claims (7)
1, a kind of coating agent to make fabric stiff is characterized in that comprising (percentage by weight):
Acrylic acid synthetic emulsion 20-50%
Animal tallow emulsion 10-30%
Glycerol 1-5%
Defoamer 0.5-2%
Essence 0.1-3%
Formaldehyde 0.5-4%
Polyvinyl alcohol 99 3-8%
Cellulose 1-5%
Surplus is a water.
2, coating agent to make fabric stiff as claimed in claim 1 is characterized in that comprising (percentage by weight):
Acrylic acid synthetic emulsion 30-40%
Animal tallow emulsion 15-25%
Glycerol 1-3%
Defoamer 1-2%
Essence 1-3%
Formaldehyde 1-3%
Polyvinyl alcohol 99 4-7%
Cellulose 3-5%
Surplus is a water.
3, as claim 1,2 coating agent to make fabric stiff, it is characterized in that the acrylic acid synthetic emulsion comprises (percentage by weight):
77# binding agent 10-40%
107# binding agent 1-30%
All the other are the 07#-10# binding agent.
4, as claim 1,2 finishing agent, it is characterized in that the animal tallow emulsion can be milk, goat milk and casein etc.
5, as claim 1,2 finishing agent, it is characterized in that preferably deionized water of water.
6,, it is characterized in that at first in still, adding entry, and heat as the preparation method of claim 1,2 coating agent to make fabric stiff, add more than the polyvinyl alcohol to 95 ℃, make polyvinyl alcohol dissolve into liquid, add cellulose then, treat to reduce to normal temperature after it dissolves into liquid; Low speed (40-90rpm) stirred 20-40 minute add glycerol, formaldehyde in reactor after, add acrylic acid synthetic emulsion and animal tallow emulsion then, (300-1000rpm) stirs and trembles 20 minutes at a high speed, and low speed (40-90rpm) stirred 10 minutes again, add essence, promptly get product.
7, as claim 1,2 coating agent to make fabric stiff, it is characterized in that not only can be used on the fabric, but also can be applicable to aspects such as leather, metal rust preventing, flowers and plants are fresh-keeping, human body skin care.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95118068 CN1141981A (en) | 1995-10-28 | 1995-10-28 | Coating agent to make fabric stiff |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95118068 CN1141981A (en) | 1995-10-28 | 1995-10-28 | Coating agent to make fabric stiff |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1141981A true CN1141981A (en) | 1997-02-05 |
Family
ID=5081558
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 95118068 Pending CN1141981A (en) | 1995-10-28 | 1995-10-28 | Coating agent to make fabric stiff |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1141981A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100392176C (en) * | 2004-11-16 | 2008-06-04 | 江苏东升艾克科技股份有限公司 | Vapor-permeable anti-acid and alkali anti-oil and waterproof fabric finishing method |
| CN101302277B (en) * | 2008-06-16 | 2010-06-09 | 宁波润禾化学工业有限公司 | Functional fabric waterproof stiffener and preparation technology thereof |
| CN103757909A (en) * | 2013-12-21 | 2014-04-30 | 成都德美精英化工有限公司 | Non-ionic stiffening agent and preparation method thereof |
| CN105113235A (en) * | 2015-09-06 | 2015-12-02 | 上海应用技术学院 | Slow-release aromatic for leather and preparation method of slow-release aromatic |
| CN107201658A (en) * | 2017-05-31 | 2017-09-26 | 句容市恒鑫遮阳科技有限公司 | A kind of terylene use for window shutter post-finishing agent |
-
1995
- 1995-10-28 CN CN 95118068 patent/CN1141981A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100392176C (en) * | 2004-11-16 | 2008-06-04 | 江苏东升艾克科技股份有限公司 | Vapor-permeable anti-acid and alkali anti-oil and waterproof fabric finishing method |
| CN101302277B (en) * | 2008-06-16 | 2010-06-09 | 宁波润禾化学工业有限公司 | Functional fabric waterproof stiffener and preparation technology thereof |
| CN103757909A (en) * | 2013-12-21 | 2014-04-30 | 成都德美精英化工有限公司 | Non-ionic stiffening agent and preparation method thereof |
| CN103757909B (en) * | 2013-12-21 | 2015-11-25 | 成都德美精英化工有限公司 | A kind of nonionic stiffening agent and preparation method thereof |
| CN105113235A (en) * | 2015-09-06 | 2015-12-02 | 上海应用技术学院 | Slow-release aromatic for leather and preparation method of slow-release aromatic |
| CN107201658A (en) * | 2017-05-31 | 2017-09-26 | 句容市恒鑫遮阳科技有限公司 | A kind of terylene use for window shutter post-finishing agent |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |