CS195775B1 - Sposob delenia zmesi chloridu draselného, ftalimidu draselného, ftalimidu, N-(cyklohexylthio)ftalimidu, připadne s N-chlórftalimidom - Google Patents

Sposob delenia zmesi chloridu draselného, ftalimidu draselného, ftalimidu, N-(cyklohexylthio)ftalimidu, připadne s N-chlórftalimidom Download PDF

Info

Publication number: CS195775B1
Authority: CS; Czechoslovakia
Prior art keywords: phthalimide; potassium; cyclohexylthio; mixture; solution
Prior art date: 1978-07-28

Application number

CS500578A

Other languages

Czech (cs)

English (en)

Inventor

Robert Poor

Original Assignee

Robert Poor

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1978-07-28

Filing date

1978-07-28

Publication date

1980-02-29

1978-07-28 Application filed by Robert Poor filed Critical Robert Poor

1978-07-28 Priority to CS500578A priority Critical patent/CS195775B1/sk

1980-02-29 Publication of CS195775B1 publication Critical patent/CS195775B1/sk

Links

WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 title claims description 40
XKJCHHZQLQNZHY-UHFFFAOYSA-N phthalimide Chemical compound C1=CC=C2C(=O)NC(=O)C2=C1 XKJCHHZQLQNZHY-UHFFFAOYSA-N 0.000 title claims description 27
FYRHIOVKTDQVFC-UHFFFAOYSA-M potassium phthalimide Chemical compound [K+].C1=CC=C2C(=O)[N-]C(=O)C2=C1 FYRHIOVKTDQVFC-UHFFFAOYSA-M 0.000 title claims description 24
239000000203 mixture Substances 0.000 title claims description 22
239000001103 potassium chloride Substances 0.000 title claims description 20
235000011164 potassium chloride Nutrition 0.000 title claims description 20
238000000034 method Methods 0.000 title claims description 10
238000000926 separation method Methods 0.000 title description 2
UEZWYKZHXASYJN-UHFFFAOYSA-N cyclohexylthiophthalimide Chemical compound O=C1C2=CC=CC=C2C(=O)N1SC1CCCCC1 UEZWYKZHXASYJN-UHFFFAOYSA-N 0.000 claims description 27
239000000706 filtrate Substances 0.000 claims description 13
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 12
238000005406 washing Methods 0.000 claims description 12
WDRFYIPWHMGQPN-UHFFFAOYSA-N 2-chloroisoindole-1,3-dione Chemical compound C1=CC=C2C(=O)N(Cl)C(=O)C2=C1 WDRFYIPWHMGQPN-UHFFFAOYSA-N 0.000 claims description 11
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
239000002904 solvent Substances 0.000 claims description 8
XRFDWTWFFLOKAV-UHFFFAOYSA-N cyclohexyl thiohypochlorite Chemical compound ClSC1CCCCC1 XRFDWTWFFLOKAV-UHFFFAOYSA-N 0.000 claims description 6
238000004519 manufacturing process Methods 0.000 claims description 5
239000003960 organic solvent Substances 0.000 claims description 5
238000001914 filtration Methods 0.000 claims description 3
239000007787 solid Substances 0.000 claims description 3
239000002699 waste material Substances 0.000 claims description 3
APOAEMIYHVGWEZ-UHFFFAOYSA-N 4-chloroisoindole-1,3-dione Chemical compound ClC1=CC=CC2=C1C(=O)NC2=O APOAEMIYHVGWEZ-UHFFFAOYSA-N 0.000 claims 1
238000005191 phase separation Methods 0.000 claims 1
230000001172 regenerating effect Effects 0.000 claims 1
238000009833 condensation Methods 0.000 description 11
230000005494 condensation Effects 0.000 description 11
239000007790 solid phase Substances 0.000 description 11
VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 10
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 4
239000000460 chlorine Substances 0.000 description 4
229910052801 chlorine Inorganic materials 0.000 description 4
238000004073 vulcanization Methods 0.000 description 4
239000011541 reaction mixture Substances 0.000 description 3
ODHAQPXNQDBHSH-UHFFFAOYSA-N Dicyclohexyl disulfide Chemical compound C1CCCCC1SSC1CCCCC1 ODHAQPXNQDBHSH-UHFFFAOYSA-N 0.000 description 2
BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 description 2
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
238000006243 chemical reaction Methods 0.000 description 2
CMKBCTPCXZNQKX-UHFFFAOYSA-N cyclohexanethiol Chemical compound SC1CCCCC1 CMKBCTPCXZNQKX-UHFFFAOYSA-N 0.000 description 2
238000005516 engineering process Methods 0.000 description 2
239000012065 filter cake Substances 0.000 description 2
230000007935 neutral effect Effects 0.000 description 2
238000001556 precipitation Methods 0.000 description 2
238000003756 stirring Methods 0.000 description 2
BKRKXJVHGXPMQS-UHFFFAOYSA-N 7a-chloro-3ah-isoindole-1,3-dione Chemical compound C1=CC=CC2C(=O)NC(=O)C21Cl BKRKXJVHGXPMQS-UHFFFAOYSA-N 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
241000272194 Ciconiiformes Species 0.000 description 1
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
238000005660 chlorination reaction Methods 0.000 description 1
238000001816 cooling Methods 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
-1 cyclohexylthio Chemical group 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
239000012535 impurity Substances 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
239000003112 inhibitor Substances 0.000 description 1
238000002955 isolation Methods 0.000 description 1
239000010410 layer Substances 0.000 description 1
229920003052 natural elastomer Polymers 0.000 description 1
229920001194 natural rubber Polymers 0.000 description 1
239000012454 non-polar solvent Substances 0.000 description 1
239000012044 organic layer Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
239000011591 potassium Substances 0.000 description 1
229910052700 potassium Inorganic materials 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
239000000047 product Substances 0.000 description 1
238000000746 purification Methods 0.000 description 1
239000002994 raw material Substances 0.000 description 1
238000011084 recovery Methods 0.000 description 1
230000008929 regeneration Effects 0.000 description 1
238000011069 regeneration method Methods 0.000 description 1
239000011833 salt mixture Substances 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
239000011780 sodium chloride Substances 0.000 description 1
239000008247 solid mixture Substances 0.000 description 1
239000011877 solvent mixture Substances 0.000 description 1
229920003051 synthetic elastomer Polymers 0.000 description 1
239000005061 synthetic rubber Substances 0.000 description 1

Landscapes

Indole Compounds (AREA)

CS500578A 1978-07-28 1978-07-28 Sposob delenia zmesi chloridu draselného, ftalimidu draselného, ftalimidu, N-(cyklohexylthio)ftalimidu, připadne s N-chlórftalimidom CS195775B1 (sk)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
CS500578A CS195775B1 (sk)	1978-07-28	1978-07-28	Sposob delenia zmesi chloridu draselného, ftalimidu draselného, ftalimidu, N-(cyklohexylthio)ftalimidu, připadne s N-chlórftalimidom

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CS500578A CS195775B1 (sk)	1978-07-28	1978-07-28	Sposob delenia zmesi chloridu draselného, ftalimidu draselného, ftalimidu, N-(cyklohexylthio)ftalimidu, připadne s N-chlórftalimidom

Publications (1)

Publication Number	Publication Date
CS195775B1 true CS195775B1 (sk)	1980-02-29

Family

ID=5394067

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CS500578A CS195775B1 (sk)	1978-07-28	1978-07-28	Sposob delenia zmesi chloridu draselného, ftalimidu draselného, ftalimidu, N-(cyklohexylthio)ftalimidu, připadne s N-chlórftalimidom

Country Status (1)

Country	Link
CS (1)	CS195775B1 (sk)

1978
- 1978-07-28 CS CS500578A patent/CS195775B1/sk unknown

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