CS211004B1 - Preparation method of nickel catalyst on the carrier for selective hydrogenizations - Google Patents

Preparation method of nickel catalyst on the carrier for selective hydrogenizations Download PDF

Info

Publication number: CS211004B1
Authority: CS; Czechoslovakia
Prior art keywords: nickel; catalyst; preparation; selective; nickel catalyst
Prior art date: 1980-01-02

Application number

CS580A

Other languages

Czech (cs)

English (en)

Inventor

Vladimir Zapletal

Jaroslav Prchlik

Frantisek Uhlir

Jiri Cmolik

Jiri Ruzicka

Vaclav Spevacek

Vladimir Prochazka

Jiri Stuchlik

Original Assignee

Vladimir Zapletal

Jaroslav Prchlik

Frantisek Uhlir

Jiri Cmolik

Jiri Ruzicka

Vaclav Spevacek

Vladimir Prochazka

Jiri Stuchlik

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1980-01-02

Filing date

1980-01-02

Publication date

1982-01-29

1980-01-02 Application filed by Vladimir Zapletal, Jaroslav Prchlik, Frantisek Uhlir, Jiri Cmolik, Jiri Ruzicka, Vaclav Spevacek, Vladimir Prochazka, Jiri Stuchlik filed Critical Vladimir Zapletal

1980-01-02 Priority to CS580A priority Critical patent/CS211004B1/cs

1980-11-17 Priority to DD22529980A priority patent/DD157495A3/de

1980-11-17 Priority to BG4969280A priority patent/BG37550A1/xx

1980-11-25 Priority to SU807771477A priority patent/SU1142162A1/ru

1980-12-30 Priority to NO803956A priority patent/NO803956L/no

1980-12-30 Priority to DE19803049414 priority patent/DE3049414A1/de

1980-12-30 Priority to NL8007105A priority patent/NL8007105A/nl

1980-12-31 Priority to GB8041609A priority patent/GB2066690B/en

1980-12-31 Priority to FR8027899A priority patent/FR2472952A1/fr

1982-01-29 Publication of CS211004B1 publication Critical patent/CS211004B1/cs

Links

PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims description 22
238000002360 preparation method Methods 0.000 title claims description 5
238000000034 method Methods 0.000 claims description 7
229910052759 nickel Inorganic materials 0.000 claims description 7
238000005984 hydrogenation reaction Methods 0.000 claims description 6
239000003513 alkali Substances 0.000 claims description 5
BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 claims description 5
238000001556 precipitation Methods 0.000 claims description 5
150000001875 compounds Chemical class 0.000 claims description 4
229910052751 metal Inorganic materials 0.000 claims description 4
239000002184 metal Substances 0.000 claims description 4
229910000008 nickel(II) carbonate Inorganic materials 0.000 claims description 4
ZULUUIKRFGGGTL-UHFFFAOYSA-L nickel(ii) carbonate Chemical compound [Ni+2].[O-]C([O-])=O ZULUUIKRFGGGTL-UHFFFAOYSA-L 0.000 claims description 4
150000002894 organic compounds Chemical class 0.000 claims description 4
229910052776 Thorium Inorganic materials 0.000 claims description 3
229910052804 chromium Inorganic materials 0.000 claims description 3
229910052802 copper Inorganic materials 0.000 claims description 3
150000002815 nickel Chemical class 0.000 claims description 3
230000000737 periodic effect Effects 0.000 claims description 3
229910052702 rhenium Inorganic materials 0.000 claims description 3
229910052709 silver Inorganic materials 0.000 claims description 3
229910052718 tin Inorganic materials 0.000 claims description 3
229910052726 zirconium Inorganic materials 0.000 claims description 3
ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical compound [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 claims 1
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims 1
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims 1
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims 1
239000011651 chromium Substances 0.000 claims 1
239000010949 copper Substances 0.000 claims 1
WUAPFZMCVAUBPE-UHFFFAOYSA-N rhenium atom Chemical compound [Re] WUAPFZMCVAUBPE-UHFFFAOYSA-N 0.000 claims 1
239000004332 silver Substances 0.000 claims 1
239000003054 catalyst Substances 0.000 description 15
239000000243 solution Substances 0.000 description 11
WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 6
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
239000002244 precipitate Substances 0.000 description 4
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 3
238000001035 drying Methods 0.000 description 3
238000001914 filtration Methods 0.000 description 3
229910052708 sodium Inorganic materials 0.000 description 3
239000011734 sodium Substances 0.000 description 3
239000000725 suspension Substances 0.000 description 3
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
230000002378 acidificating effect Effects 0.000 description 2
229910052783 alkali metal Inorganic materials 0.000 description 2
150000001340 alkali metals Chemical class 0.000 description 2
125000004122 cyclic group Chemical group 0.000 description 2
125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
150000002739 metals Chemical class 0.000 description 2
KBJMLQFLOWQJNF-UHFFFAOYSA-N nickel(ii) nitrate Chemical compound [Ni+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O KBJMLQFLOWQJNF-UHFFFAOYSA-N 0.000 description 2
238000006722 reduction reaction Methods 0.000 description 2
239000000377 silicon dioxide Substances 0.000 description 2
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 2
229910000033 sodium borohydride Inorganic materials 0.000 description 2
239000012279 sodium borohydride Substances 0.000 description 2
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
241000102542 Kara Species 0.000 description 1
229910021586 Nickel(II) chloride Inorganic materials 0.000 description 1
101150003085 Pdcl gene Proteins 0.000 description 1
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
239000002253 acid Substances 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
150000001450 anions Chemical class 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000004913 cyclooctene Substances 0.000 description 1
125000000522 cyclooctenyl group Chemical group C1(=CCCCCCC1)* 0.000 description 1
230000000694 effects Effects 0.000 description 1
150000002170 ethers Chemical class 0.000 description 1
239000002638 heterogeneous catalyst Substances 0.000 description 1
230000036571 hydration Effects 0.000 description 1
238000006703 hydration reaction Methods 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
150000004679 hydroxides Chemical class 0.000 description 1
230000004941 influx Effects 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
238000005259 measurement Methods 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000000203 mixture Substances 0.000 description 1
239000012452 mother liquor Substances 0.000 description 1
QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 1
TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
239000002516 radical scavenger Substances 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
238000007363 ring formation reaction Methods 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
238000007873 sieving Methods 0.000 description 1
239000000741 silica gel Substances 0.000 description 1
229910002027 silica gel Inorganic materials 0.000 description 1
229910001961 silver nitrate Inorganic materials 0.000 description 1
239000002002 slurry Substances 0.000 description 1
229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
235000017557 sodium bicarbonate Nutrition 0.000 description 1
239000002904 solvent Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1
229910021653 sulphate ion Inorganic materials 0.000 description 1
239000002344 surface layer Substances 0.000 description 1
238000005406 washing Methods 0.000 description 1

Landscapes

Catalysts (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Steroid Compounds (AREA)

CS580A 1980-01-02 1980-01-02 Preparation method of nickel catalyst on the carrier for selective hydrogenizations CS211004B1 (en)

Priority Applications (9)

Application Number	Priority Date	Filing Date	Title
CS580A CS211004B1 (en)	1980-01-02	1980-01-02	Preparation method of nickel catalyst on the carrier for selective hydrogenizations
DD22529980A DD157495A3 (de)	1980-01-02	1980-11-17	Verfahren zur gewinnung eines nickelkatalysators fuer die selektive hydrierung
BG4969280A BG37550A1 (en)	1980-01-02	1980-11-17	Method for preparing nickel catalyst on carrier for selective hydrogenation
SU807771477A SU1142162A1 (ru)	1980-01-02	1980-11-25	Способ приготовлени катализатора на носителе дл процесса селективного гидрировани
NO803956A NO803956L (no)	1980-01-02	1980-12-30	Nikkelbasert, baaren katalysator og fremgangsmaate ved fremstilling derav.
DE19803049414 DE3049414A1 (de)	1980-01-02	1980-12-30	Hydrierkatalysatoren auf nickelbasis, ihrer herstellung und verwendung
NL8007105A NL8007105A (nl)	1980-01-02	1980-12-30	Op een drager aangebrachte katalysator op nikkelbasis, werkwijze ter bereiding ervan en toepassing bij een werkwijze voor hydrogenering van meervoudig onverzadigde organische verbindingen tot de overeenkomstige ten dele of geheel verzadigde verbindingen.
GB8041609A GB2066690B (en)	1980-01-02	1980-12-31	Supported nickel-based catalyst
FR8027899A FR2472952A1 (fr)	1980-01-02	1980-12-31	Catalyseur a base de nickel fixe sur un support et emploi de ce catalyseur dans un procede d'hydrogenation de composes organiques polyinsatures en les composes partiellement ou completement satures correspondants

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CS580A CS211004B1 (en)	1980-01-02	1980-01-02	Preparation method of nickel catalyst on the carrier for selective hydrogenizations

Publications (1)

Publication Number	Publication Date
CS211004B1 true CS211004B1 (en)	1982-01-29

Family

ID=5331436

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CS580A CS211004B1 (en)	1980-01-02	1980-01-02	Preparation method of nickel catalyst on the carrier for selective hydrogenizations

Country Status (4)

Country	Link
BG (1)	BG37550A1 (de)
CS (1)	CS211004B1 (de)
DD (1)	DD157495A3 (de)
SU (1)	SU1142162A1 (de)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US7408089B2 (en) *	2004-03-19	2008-08-05	Catalytic Distillation Technologies	Ni catalyst, process for making catalysts and selective hydrogenation process

1980
- 1980-01-02 CS CS580A patent/CS211004B1/cs unknown
- 1980-11-17 BG BG4969280A patent/BG37550A1/xx unknown
- 1980-11-17 DD DD22529980A patent/DD157495A3/de not_active IP Right Cessation
- 1980-11-25 SU SU807771477A patent/SU1142162A1/ru active

Also Published As

Publication number	Publication date
DD157495A3 (de)	1982-11-17
BG37550A1 (en)	1985-07-16
SU1142162A1 (ru)	1985-02-28

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