CS274796B2 - Method of pure crystalline d-arabinose preparation - Google Patents

Method of pure crystalline d-arabinose preparation

Info

Publication number: CS274796B2
Authority: CS; Czechoslovakia
Prior art keywords: solution; arabinose; addition; hypochlorite; concentration
Prior art date: 1990-02-26

Application number

CS88990A

Other languages

English (en)

Other versions

CS88990A2 (en

Inventor

Miroslav Ing Csc Bleha

Jaroslav Ing Csc Prchlik

Vera Ing Sumberova

Miroslav Ing Brda

Vladimir Dufek

Original Assignee

Ustav Makromolekularni Chemie

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1990-02-26

Filing date

1990-02-26

Publication date

1991-11-12

1990-02-26 Application filed by Ustav Makromolekularni Chemie filed Critical Ustav Makromolekularni Chemie

1990-02-26 Priority to CS90889A priority Critical patent/CS88990A2/cs

1991-11-12 Publication of CS274796B2 publication Critical patent/CS274796B2/cs

1991-11-12 Publication of CS88990A2 publication Critical patent/CS88990A2/cs

Links

PYMYPHUHKUWMLA-WDCZJNDASA-N arabinose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)C=O PYMYPHUHKUWMLA-WDCZJNDASA-N 0.000 title abstract 2
238000000034 method Methods 0.000 title abstract 2
238000002360 preparation method Methods 0.000 title abstract 2
PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 abstract 4
SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 abstract 4
WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 abstract 4
SRBFZHDQGSBBOR-OWMBCFKOSA-N L-ribopyranose Chemical compound O[C@H]1COC(O)[C@@H](O)[C@H]1O SRBFZHDQGSBBOR-OWMBCFKOSA-N 0.000 abstract 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
230000003647 oxidation Effects 0.000 abstract 2
238000007254 oxidation reaction Methods 0.000 abstract 2
239000011541 reaction mixture Substances 0.000 abstract 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 abstract 1
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
RGHNJXZEOKUKBD-SQOUGZDYSA-M D-gluconate Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O RGHNJXZEOKUKBD-SQOUGZDYSA-M 0.000 abstract 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract 1
239000005708 Sodium hypochlorite Substances 0.000 abstract 1
239000002253 acid Substances 0.000 abstract 1
239000003957 anion exchange resin Substances 0.000 abstract 1
239000003729 cation exchange resin Substances 0.000 abstract 1
239000000460 chlorine Substances 0.000 abstract 1
229910052801 chlorine Inorganic materials 0.000 abstract 1
239000012141 concentrate Substances 0.000 abstract 1
238000002425 crystallisation Methods 0.000 abstract 1
238000010612 desalination reaction Methods 0.000 abstract 1
150000003839 salts Chemical class 0.000 abstract 1
239000000176 sodium gluconate Substances 0.000 abstract 1
235000012207 sodium gluconate Nutrition 0.000 abstract 1
SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 abstract 1
MSXHSNHNTORCAW-GGLLEASOSA-M sodium;(2s,3s,4s,5r,6s)-3,4,5,6-tetrahydroxyoxane-2-carboxylate Chemical compound [Na+].O[C@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O MSXHSNHNTORCAW-GGLLEASOSA-M 0.000 abstract 1
230000008719 thickening Effects 0.000 abstract 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Separation Using Semi-Permeable Membranes (AREA)

CS90889A 1990-02-26 1990-02-26 Method of pure crystalline d-arabinose preparation CS88990A2 (en)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
CS90889A CS88990A2 (en)	1990-02-26	1990-02-26	Method of pure crystalline d-arabinose preparation

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CS90889A CS88990A2 (en)	1990-02-26	1990-02-26	Method of pure crystalline d-arabinose preparation

Publications (2)

Publication Number	Publication Date
CS274796B2 true CS274796B2 (en)	1991-11-12
CS88990A2 CS88990A2 (en)	1991-11-12

Family

ID=5341907

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CS90889A CS88990A2 (en)	1990-02-26	1990-02-26	Method of pure crystalline d-arabinose preparation

Country Status (1)

Country	Link
CS (1)	CS88990A2 (cs)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
RU2132878C1 (ru) *	1998-01-06	1999-07-10	Карпун Екатерина Васильевна	Способ получения солей глюконовой кислоты и лимонной кислоты
CN102850409A (zh) *	2012-09-26	2013-01-02	山东福田药业有限公司	D-阿拉伯糖的制备方法

1990
- 1990-02-26 CS CS90889A patent/CS88990A2/cs unknown

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
RU2132878C1 (ru) *	1998-01-06	1999-07-10	Карпун Екатерина Васильевна	Способ получения солей глюконовой кислоты и лимонной кислоты
CN102850409A (zh) *	2012-09-26	2013-01-02	山东福田药业有限公司	D-阿拉伯糖的制备方法

Also Published As

Publication number	Publication date
CS88990A2 (en)	1991-11-12

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Legal Events

Date	Code	Title	Description
2000-06-30	IF00	In force as of 2000-06-30 in czech republic