DD142642A5 - Verfahren zur herstellung von alkylsilanen - Google Patents

Verfahren zur herstellung von alkylsilanen Download PDF

Info

Publication number: DD142642A5
Authority: DD; German Democratic Republic
Prior art keywords: catalyst; reaction; allyl chloride; pressure; boiling
Prior art date: 1978-04-08

Application number

DD212005A

Other languages

German (de)

English (en)

Inventor

Claus-Dietrich Seiler

Hans-Joachim Vahlensieck

Original Assignee

Dynamit Nobel Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1978-04-08

Filing date

1979-04-04

Publication date

1980-07-09

1979-04-04 Application filed by Dynamit Nobel Ag filed Critical Dynamit Nobel Ag

1980-07-09 Publication of DD142642A5 publication Critical patent/DD142642A5/de

Links

238000000034 method Methods 0.000 title claims description 25
150000001343 alkyl silanes Chemical class 0.000 title claims description 7
238000002360 preparation method Methods 0.000 title claims description 4
239000003054 catalyst Substances 0.000 claims description 34
101000588924 Anthopleura elegantissima Delta-actitoxin-Ael1a Proteins 0.000 claims description 13
238000009835 boiling Methods 0.000 claims description 10
239000000203 mixture Substances 0.000 claims description 10
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 10
239000000376 reactant Substances 0.000 claims description 10
238000007259 addition reaction Methods 0.000 claims description 5
KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims description 4
229910052697 platinum Inorganic materials 0.000 claims description 4
239000012876 carrier material Substances 0.000 claims description 3
239000000463 material Substances 0.000 claims description 3
230000001174 ascending effect Effects 0.000 claims description 2
229910052763 palladium Inorganic materials 0.000 claims description 2
125000000217 alkyl group Chemical group 0.000 claims 1
OSDWBNJEKMUWAV-UHFFFAOYSA-N Allyl chloride Chemical compound ClCC=C OSDWBNJEKMUWAV-UHFFFAOYSA-N 0.000 description 21
238000006243 chemical reaction Methods 0.000 description 17
239000011521 glass Substances 0.000 description 14
ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 14
239000005052 trichlorosilane Substances 0.000 description 12
QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 8
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 8
239000007795 chemical reaction product Substances 0.000 description 7
238000001816 cooling Methods 0.000 description 7
OOXSLJBUMMHDKW-UHFFFAOYSA-N trichloro(3-chloropropyl)silane Chemical compound ClCCC[Si](Cl)(Cl)Cl OOXSLJBUMMHDKW-UHFFFAOYSA-N 0.000 description 7
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
238000002474 experimental method Methods 0.000 description 6
238000010438 heat treatment Methods 0.000 description 6
VZGLVCFVUREVDP-UHFFFAOYSA-N 3-chlorobut-1-ene Chemical compound CC(Cl)C=C VZGLVCFVUREVDP-UHFFFAOYSA-N 0.000 description 5
239000007789 gas Substances 0.000 description 5
YWAKXRMUMFPDSH-UHFFFAOYSA-N pentene Chemical compound CCCC=C YWAKXRMUMFPDSH-UHFFFAOYSA-N 0.000 description 5
239000007858 starting material Substances 0.000 description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
229910000831 Steel Inorganic materials 0.000 description 4
ZGEGCLOFRBLKSE-UHFFFAOYSA-N methylene hexane Natural products CCCCCC=C ZGEGCLOFRBLKSE-UHFFFAOYSA-N 0.000 description 4
239000010959 steel Substances 0.000 description 4
VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 3
BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 3
DSVGQVZAZSZEEX-UHFFFAOYSA-N [C].[Pt] Chemical class [C].[Pt] DSVGQVZAZSZEEX-UHFFFAOYSA-N 0.000 description 3
150000001336 alkenes Chemical class 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 3
229910052736 halogen Inorganic materials 0.000 description 3
229910052739 hydrogen Inorganic materials 0.000 description 3
239000001257 hydrogen Substances 0.000 description 3
125000004435 hydrogen atom Chemical class [H]* 0.000 description 3
239000000047 product Substances 0.000 description 3
238000010992 reflux Methods 0.000 description 3
239000005049 silicon tetrachloride Substances 0.000 description 3
238000010626 work up procedure Methods 0.000 description 3
MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 2
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
239000006227 byproduct Substances 0.000 description 2
238000003776 cleavage reaction Methods 0.000 description 2
239000000498 cooling water Substances 0.000 description 2
239000012043 crude product Substances 0.000 description 2
HGCIXCUEYOPUTN-UHFFFAOYSA-N cyclohexene Chemical compound C1CCC=CC1 HGCIXCUEYOPUTN-UHFFFAOYSA-N 0.000 description 2
238000004821 distillation Methods 0.000 description 2
150000002367 halogens Chemical class 0.000 description 2
-1 hydrogen silanes Chemical class 0.000 description 2
229910052757 nitrogen Inorganic materials 0.000 description 2
239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 description 2
125000001424 substituent group Chemical group 0.000 description 2
239000000758 substrate Substances 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical group FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 1
SDRZFSPCVYEJTP-UHFFFAOYSA-N 1-ethenylcyclohexene Chemical compound C=CC1=CCCCC1 SDRZFSPCVYEJTP-UHFFFAOYSA-N 0.000 description 1
KWKAKUADMBZCLK-UHFFFAOYSA-N 1-octene Chemical compound CCCCCCC=C KWKAKUADMBZCLK-UHFFFAOYSA-N 0.000 description 1
BKOOMYPCSUNDGP-UHFFFAOYSA-N 2-methylbut-2-ene Chemical group CC=C(C)C BKOOMYPCSUNDGP-UHFFFAOYSA-N 0.000 description 1
239000005046 Chlorosilane Substances 0.000 description 1
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
239000005977 Ethylene Substances 0.000 description 1
206010061926 Purulence Diseases 0.000 description 1
239000004809 Teflon Substances 0.000 description 1
229920006362 Teflon® Polymers 0.000 description 1
XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
125000003342 alkenyl group Chemical group 0.000 description 1
HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
229940045985 antineoplastic platinum compound Drugs 0.000 description 1
150000001722 carbon compounds Chemical class 0.000 description 1
KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical compound Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 description 1
238000004587 chromatography analysis Methods 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
239000002826 coolant Substances 0.000 description 1
YQGOWXYZDLJBFL-UHFFFAOYSA-N dimethoxysilane Chemical compound CO[SiH2]OC YQGOWXYZDLJBFL-UHFFFAOYSA-N 0.000 description 1
125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000011049 filling Methods 0.000 description 1
238000000227 grinding Methods 0.000 description 1
230000020169 heat generation Effects 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid group Chemical group C(CCCCCCC\C=C/CCCCCCCC)(=O)O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
125000000962 organic group Chemical group 0.000 description 1
150000001282 organosilanes Chemical class 0.000 description 1
HVAMZGADVCBITI-UHFFFAOYSA-M pent-4-enoate Chemical compound [O-]C(=O)CCC=C HVAMZGADVCBITI-UHFFFAOYSA-M 0.000 description 1
229930015698 phenylpropene Natural products 0.000 description 1
150000003058 platinum compounds Chemical class 0.000 description 1
HJWLCRVIBGQPNF-UHFFFAOYSA-N prop-2-enylbenzene Chemical compound C=CCC1=CC=CC=C1 HJWLCRVIBGQPNF-UHFFFAOYSA-N 0.000 description 1
238000010926 purge Methods 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
230000007017 scission Effects 0.000 description 1
229910000077 silane Inorganic materials 0.000 description 1
125000005372 silanol group Chemical class 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
239000010703 silicon Substances 0.000 description 1
FLPXNJHYVOVLSD-UHFFFAOYSA-N trichloro(2-chloroethyl)silane Chemical compound ClCC[Si](Cl)(Cl)Cl FLPXNJHYVOVLSD-UHFFFAOYSA-N 0.000 description 1
KWDQAHIRKOXFAV-UHFFFAOYSA-N trichloro(pentyl)silane Chemical compound CCCCC[Si](Cl)(Cl)Cl KWDQAHIRKOXFAV-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/12—Organo silicon halides
- C07F7/14—Preparation thereof from optionally substituted halogenated silanes and hydrocarbons hydrosilylation reactions

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)

DD212005A 1978-04-08 1979-04-04 Verfahren zur herstellung von alkylsilanen DD142642A5 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE2815316A DE2815316C2 (de)	1978-04-08	1978-04-08	Verfahren zur Herstellung von Alkylsilanen

Publications (1)

Publication Number	Publication Date
DD142642A5 true DD142642A5 (de)	1980-07-09

Family

ID=6036520

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DD212005A DD142642A5 (de)	1978-04-08	1979-04-04	Verfahren zur herstellung von alkylsilanen

Country Status (9)

Country	Link
US (1)	US4224233A (fr)
JP (1)	JPS54138520A (fr)
BE (1)	BE875378A (fr)
CA (1)	CA1137504A (fr)
DD (1)	DD142642A5 (fr)
DE (1)	DE2815316C2 (fr)
FR (1)	FR2421908A1 (fr)
GB (1)	GB2018268B (fr)
NL (1)	NL187686C (fr)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2815978C2 (de) *	1978-04-13	1980-05-22	Dynamit Nobel Ag, 5210 Troisdorf	Verfahren zur Herstellung von Athylsilanen
DE3404703A1 (de) *	1984-02-10	1985-09-05	Degussa Ag, 6000 Frankfurt	Verfahren zur herstellung von 3-chlorpropyltrichlorsilan
DE4119994A1 (de) *	1991-06-18	1992-12-24	Huels Chemische Werke Ag	Verfahren zur herstellung von 3-chlorpropylsilanen
US5559264A (en) *	1994-02-24	1996-09-24	Osi Specialities, Inc.	Process for making chloroorganosilicon compounds
DE19632157A1 (de) *	1996-08-09	1998-02-12	Huels Chemische Werke Ag	Verfahren zur kontinuierlichen Herstellung von 3-Halogen-Propyl-Organosilanen
JP3161354B2 (ja) *	1997-02-07	2001-04-25	日本電気株式会社	半導体装置及びその製造方法
DE102004059375A1 (de)	2004-12-09	2006-06-22	Consortium für elektrochemische Industrie GmbH	Auf nanoskaligem Titandioxid geträgerte Platin-Katalysatoren, deren Verwendung in der Hydrosilylierung, ein Hydrosilylierungsverfahren mit solchen Katalysatoren und Zusammensetzungen enthaltend solche Katalysatoren
RU2320667C1 (ru) *	2007-01-09	2008-03-27	Открытое акционерное общество "Химпром"	Способ получения 3-хлорпропилсилана
WO2012061058A2 (fr) *	2010-10-25	2012-05-10	Shell Oil Company	Procédé de préparation d'un composé à base d'alkylsilane
CN111481745A (zh) *	2019-01-25	2020-08-04	南方医科大学	可视化人工肛门封堵器的3d打印组分及其制备方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3706777A (en) *	1970-03-14	1972-12-19	Dynamit Nobel Ag	Process for the production of alkyl silanes

1978
- 1978-04-08 DE DE2815316A patent/DE2815316C2/de not_active Expired
1979
- 1979-04-03 US US06/026,633 patent/US4224233A/en not_active Expired - Lifetime
- 1979-04-04 DD DD212005A patent/DD142642A5/de not_active IP Right Cessation
- 1979-04-04 GB GB7911753A patent/GB2018268B/en not_active Expired
- 1979-04-05 FR FR7908683A patent/FR2421908A1/fr active Granted
- 1979-04-06 CA CA000325053A patent/CA1137504A/fr not_active Expired
- 1979-04-06 NL NLAANVRAGE7902723,A patent/NL187686C/xx not_active IP Right Cessation
- 1979-04-06 JP JP4114279A patent/JPS54138520A/ja active Granted
- 1979-04-06 BE BE0/194449A patent/BE875378A/fr not_active IP Right Cessation

Also Published As

Publication number	Publication date
GB2018268A (en)	1979-10-17
JPS6252756B2 (fr)	1987-11-06
DE2815316C2 (de)	1980-03-27
NL187686B (nl)	1991-07-16
GB2018268B (en)	1982-10-06
FR2421908A1 (fr)	1979-11-02
NL187686C (nl)	1991-12-16
NL7902723A (nl)	1979-10-10
US4224233A (en)	1980-09-23
FR2421908B1 (fr)	1984-08-17
CA1137504A (fr)	1982-12-14
BE875378A (fr)	1979-07-31
JPS54138520A (en)	1979-10-27
DE2815316B1 (de)	1979-07-26

Legal Events

Date	Code	Title	Description
1996-03-14	ENJ	Ceased due to non-payment of renewal fee

Publication	Publication Date	Title
EP0032376B1 (fr)	1983-07-20	Procédé pour la préparation en continu de silanes ou polysiloxanes contenant un groupement SiOC
DE2546957C3 (de)	1980-10-23	Verfahren zur Reinigung von Halogensilanen
DE69109187T2 (de)	1995-08-31	Trimethoxysilan-Herstellung über die Methanol-Silizium-Reaktion mit Recycling.
DE2851456C2 (de)	1982-09-23	Verfahren zur Herstellung von Organosiliciumverbindungen
DE2800017C2 (de)	1983-05-26	Verfahren zur Herstellung von Organoalkoxysilanen
DD142642A5 (de)	1980-07-09	Verfahren zur herstellung von alkylsilanen
EP0519181B1 (fr)	1996-01-31	Préparation de 3-chloropropylsilanes
DE2653290C2 (de)	1987-01-29	Beständige Lösung eines Gemisches von Aluminium-iso- und -n-butoxiden in den entsprechenden Alkoholen und Verfahren zu ihrer Herstellung
DE1289842B (de)	1969-02-27	Verfahren zur Spaltung von Disilanen
DD208973A5 (de)	1984-04-18	Verfahren zur herstellung von dimethylether
DE2131742A1 (de)	1972-12-28	Verfahren zur Herstellung von Alkenylsilanen
DE1198813B (de)	1965-08-19	Verfahren zur Herstellung von Vinylestern
DE3221702A1 (de)	1983-03-03	Verfahren zur herstellung von acyloxysilanen
DE2815978C2 (de)	1980-05-22	Verfahren zur Herstellung von Athylsilanen
DE2815316B2 (fr)
DE3507424C2 (de)	1987-02-26	Verfahren zur Herstellung von Dialkyldichlorsilanen hoher Reinheit
DE2533400C3 (de)	1978-06-15	Verfahren zur Herstellung von Dichlorsilan und Phenyltrichlorsilan
DE2414930C2 (de)	1983-07-07	Verfahren zur kontinuierlichen Herstellung von Hexamethylenimin
DE3017130C2 (de)	1982-10-28	Verfahren zur Herstellung von Organosiloxanen und Methylchlorid
DE2012099A1 (de)	1970-11-26	Verfahren zur Herstellung von Aryldimethylchlorsilanen
DE2733928A1 (de)	1978-02-02	Verfahren zur herstellung eines bizyklischen alkohols
DD283982A5 (de)	1990-10-31	Verfahren zur steigerung des anteils an siliciumtetrachlorid
DE1643926B2 (de)	1974-05-02	Verfahren zur Herstellung von Propyl- oder Butyltrihalogensilanen
DE2012229C3 (de)	1976-10-21	Verfahren zur Herstellung von Alkylsilanen
DE975968C (de)	1963-01-03	Verfahren zur kontinuierlichen Herstellung von Gemischen aus Essigsaeure und Methylacetat