DD148515A5 - Verfahren zur kontinuierlichen herstellung von bisphenol a - Google Patents
Verfahren zur kontinuierlichen herstellung von bisphenol a Download PDFInfo
- Publication number
- DD148515A5 DD148515A5 DD79218260A DD21826079A DD148515A5 DD 148515 A5 DD148515 A5 DD 148515A5 DD 79218260 A DD79218260 A DD 79218260A DD 21826079 A DD21826079 A DD 21826079A DD 148515 A5 DD148515 A5 DD 148515A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- reaction mixture
- layer
- catalyst
- reactor
- reactors
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 62
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 title claims abstract description 38
- 238000010924 continuous production Methods 0.000 title description 3
- 239000003054 catalyst Substances 0.000 claims abstract description 57
- 239000011541 reaction mixture Substances 0.000 claims abstract description 47
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims abstract description 40
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000009833 condensation Methods 0.000 claims abstract description 9
- 230000005494 condensation Effects 0.000 claims abstract description 9
- 238000005342 ion exchange Methods 0.000 claims abstract description 6
- 230000002378 acidificating effect Effects 0.000 claims abstract description 5
- 229920001577 copolymer Polymers 0.000 claims abstract description 4
- 239000002245 particle Substances 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 5
- 239000011949 solid catalyst Substances 0.000 claims 1
- 239000008187 granular material Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 21
- 239000000203 mixture Substances 0.000 description 7
- 239000006227 byproduct Substances 0.000 description 5
- 238000005341 cation exchange Methods 0.000 description 5
- 150000001768 cations Chemical class 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 230000003197 catalytic effect Effects 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000012451 post-reaction mixture Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000005727 Friedel-Crafts reaction Methods 0.000 description 1
- 229920002125 Sokalan® Chemical class 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- -1 bisphenol A cation Chemical class 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000009795 derivation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical class C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 239000004584 polyacrylic acid Chemical class 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/005—Separating solid material from the gas/liquid stream
- B01J8/006—Separating solid material from the gas/liquid stream by filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
- B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
- B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
- B01J8/0457—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being placed in separate reactors
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/11—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms
- C07C37/20—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms using aldehydes or ketones
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00265—Part of all of the reactants being heated or cooled outside the reactor while recycling
- B01J2208/00274—Part of all of the reactants being heated or cooled outside the reactor while recycling involving reactant vapours
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL1978212470A PL124542B1 (en) | 1978-12-30 | 1978-12-30 | Method of manufacture of bisphenol a |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD148515A5 true DD148515A5 (de) | 1981-05-27 |
Family
ID=19993792
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD79218260A DD148515A5 (de) | 1978-12-30 | 1979-12-29 | Verfahren zur kontinuierlichen herstellung von bisphenol a |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4301305A (cs) |
| BG (1) | BG49614A3 (cs) |
| CS (1) | CS212333B2 (cs) |
| DD (1) | DD148515A5 (cs) |
| IN (1) | IN151802B (cs) |
| PL (1) | PL124542B1 (cs) |
| RO (1) | RO78882A (cs) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0323831A1 (en) * | 1988-01-08 | 1989-07-12 | MITSUI TOATSU CHEMICALS, Inc. | Process for preparing bisphenol A |
| CN117599689A (zh) * | 2023-11-30 | 2024-02-27 | 上海交通大学 | 一种HCl高效转化为Cl2的方法及反应装置 |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4391997A (en) * | 1981-10-23 | 1983-07-05 | General Electric Company | Ion exchange catalyzed bisphenol process |
| PL153396B1 (en) * | 1987-10-07 | 1991-04-30 | Method of obtaining bisphenol a | |
| PL164289B1 (pl) * | 1990-11-24 | 1994-07-29 | Inst Ciezkiej Syntezy Orga | Sposób otrzymywani blsfenolu A PL PL |
| DE19526088A1 (de) * | 1995-07-18 | 1997-01-23 | Bayer Ag | Verfahren zur Herstellung von Bis(4-hydroxyaryl)alkanen |
| DE19701278A1 (de) * | 1997-01-16 | 1998-07-23 | Bayer Ag | Verfahren zur Herstellung von Bis-(4-hydroxyaryl)-alkanen |
| JP2002205966A (ja) * | 2001-01-11 | 2002-07-23 | Idemitsu Petrochem Co Ltd | ビスフェノールａの製造方法 |
| PL198633B1 (pl) * | 2001-08-07 | 2008-07-31 | Inst Ci & Eogon & Zdot Kiej Sy | Reaktor do prowadzenia reakcji otrzymywania bisfenolu A |
| DE102004005722A1 (de) * | 2004-02-05 | 2005-08-25 | Bayer Materialscience Ag | Verfahren zur Herstellung von Bisphenolen mit optimaler Befüllung des Reaktors mit Katalysator |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3172916A (en) * | 1965-03-09 | Bisphenol axpreparation u using ion ex- change resin containing mercapto and sulfonic acid groups | ||
| US3049569A (en) * | 1958-10-20 | 1962-08-14 | Union Carbide Corp | Production of 2, 2-bis(4-hydroxyphenyl) propane |
| US3049568A (en) * | 1958-10-20 | 1962-08-14 | Union Carbide Corp | Preparation of bisphenols |
| US3153001A (en) * | 1958-10-20 | 1964-10-13 | Union Carbide Corp | Cationic exchanging polymeric resin |
| PL96346B1 (pl) * | 1975-04-30 | 1977-12-31 | Sposob wytwarzania bisfenolu a | |
| GB1539184A (en) * | 1975-08-01 | 1979-01-31 | Shell Int Research | Cation-exchange resins |
| EP0001863B1 (en) * | 1977-11-09 | 1981-07-15 | Shell Internationale Researchmaatschappij B.V. | Preparation of bisphenols |
-
1978
- 1978-12-30 PL PL1978212470A patent/PL124542B1/pl unknown
-
1979
- 1979-12-28 RO RO7999752A patent/RO78882A/ro unknown
- 1979-12-28 US US06/108,403 patent/US4301305A/en not_active Expired - Lifetime
- 1979-12-28 BG BG046098A patent/BG49614A3/xx unknown
- 1979-12-29 CS CS799569A patent/CS212333B2/cs unknown
- 1979-12-29 DD DD79218260A patent/DD148515A5/de unknown
-
1980
- 1980-01-11 IN IN61/CAL/80A patent/IN151802B/en unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0323831A1 (en) * | 1988-01-08 | 1989-07-12 | MITSUI TOATSU CHEMICALS, Inc. | Process for preparing bisphenol A |
| CN117599689A (zh) * | 2023-11-30 | 2024-02-27 | 上海交通大学 | 一种HCl高效转化为Cl2的方法及反应装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| PL212470A3 (cs) | 1980-07-01 |
| PL124542B1 (en) | 1983-01-31 |
| US4301305A (en) | 1981-11-17 |
| BG49614A3 (en) | 1991-12-16 |
| IN151802B (cs) | 1983-08-06 |
| CS212333B2 (en) | 1982-03-26 |
| RO78882B (ro) | 1983-05-30 |
| RO78882A (ro) | 1983-06-01 |
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