DD157700A5 - Verfahren zur gewinnung von c tief 2-bis c tief 4-alkoholen - Google Patents

Verfahren zur gewinnung von c tief 2-bis c tief 4-alkoholen Download PDF

Info

Publication number: DD157700A5
Authority: DD; German Democratic Republic
Prior art keywords: ethanol; water; isobutene; parts; weight
Prior art date: 1980-03-31

Application number

DD81228774A

Other languages

German (de)

English (en)

Inventor

Ermanno Pescarollo

Francesco Ancillotti

Telemaco Floris

Original Assignee

Snam Progetti

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1980-03-31

Filing date

1981-03-31

Publication date

1982-12-01

1981-03-31 Application filed by Snam Progetti filed Critical Snam Progetti

1982-12-01 Publication of DD157700A5 publication Critical patent/DD157700A5/de

Links

238000000034 method Methods 0.000 title claims abstract description 15
239000000203 mixture Substances 0.000 claims abstract description 30
150000001336 alkenes Chemical group 0.000 claims abstract description 22
JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims abstract description 18
238000006243 chemical reaction Methods 0.000 claims abstract description 10
150000001298 alcohols Chemical class 0.000 claims abstract description 9
239000003456 ion exchange resin Substances 0.000 claims abstract description 8
229920003303 ion-exchange polymer Polymers 0.000 claims abstract description 8
239000002253 acid Substances 0.000 claims abstract description 6
239000003054 catalyst Substances 0.000 claims abstract description 6
125000000542 sulfonic acid group Chemical group 0.000 claims abstract 2
101000588924 Anthopleura elegantissima Delta-actitoxin-Ael1a Proteins 0.000 claims description 15
NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 6
238000011084 recovery Methods 0.000 claims description 4
239000002841 Lewis acid Substances 0.000 claims description 2
229910052500 inorganic mineral Inorganic materials 0.000 claims description 2
150000007517 lewis acids Chemical class 0.000 claims description 2
239000011707 mineral Substances 0.000 claims description 2
239000003377 acid catalyst Substances 0.000 claims 1
230000015572 biosynthetic process Effects 0.000 abstract description 3
150000002148 esters Chemical class 0.000 abstract description 2
230000002378 acidificating effect Effects 0.000 abstract 1
238000007086 side reaction Methods 0.000 abstract 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 105
VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical compound CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 description 53
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 39
DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 27
239000000047 product Substances 0.000 description 20
NUMQCACRALPSHD-UHFFFAOYSA-N tert-butyl ethyl ether Chemical compound CCOC(C)(C)C NUMQCACRALPSHD-UHFFFAOYSA-N 0.000 description 18
125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 15
239000007795 chemical reaction product Substances 0.000 description 12
239000011541 reaction mixture Substances 0.000 description 6
238000005194 fractionation Methods 0.000 description 5
239000000446 fuel Substances 0.000 description 5
239000004215 Carbon black (E152) Substances 0.000 description 4
238000000855 fermentation Methods 0.000 description 4
230000004151 fermentation Effects 0.000 description 4
229930195733 hydrocarbon Natural products 0.000 description 4
150000002430 hydrocarbons Chemical class 0.000 description 4
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
229930195734 saturated hydrocarbon Natural products 0.000 description 3
150000003509 tertiary alcohols Chemical class 0.000 description 3
MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 2
VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical compound CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 description 2
239000000654 additive Substances 0.000 description 2
IAQRGUVFOMOMEM-UHFFFAOYSA-N butene Natural products CC=CC IAQRGUVFOMOMEM-UHFFFAOYSA-N 0.000 description 2
238000004821 distillation Methods 0.000 description 2
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
239000007788 liquid Substances 0.000 description 2
239000007791 liquid phase Substances 0.000 description 2
238000010992 reflux Methods 0.000 description 2
238000001179 sorption measurement Methods 0.000 description 2
YZUPZGFPHUVJKC-UHFFFAOYSA-N 1-bromo-2-methoxyethane Chemical compound COCCBr YZUPZGFPHUVJKC-UHFFFAOYSA-N 0.000 description 1
-1 C 4 alcohols Chemical class 0.000 description 1
239000004793 Polystyrene Substances 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
230000000996 additive effect Effects 0.000 description 1
125000000217 alkyl group Chemical group 0.000 description 1
125000003118 aryl group Chemical group 0.000 description 1
238000010533 azeotropic distillation Methods 0.000 description 1
LRHPLDYGYMQRHN-UHFFFAOYSA-N butyl alcohol Substances CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 1
150000001720 carbohydrates Chemical class 0.000 description 1
235000014633 carbohydrates Nutrition 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
230000007423 decrease Effects 0.000 description 1
238000010586 diagram Methods 0.000 description 1
208000028659 discharge Diseases 0.000 description 1
230000000694 effects Effects 0.000 description 1
230000005611 electricity Effects 0.000 description 1
RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
150000002170 ethers Chemical class 0.000 description 1
238000000605 extraction Methods 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000000835 fiber Substances 0.000 description 1
235000011389 fruit/vegetable juice Nutrition 0.000 description 1
239000007789 gas Substances 0.000 description 1
239000007792 gaseous phase Substances 0.000 description 1
230000036571 hydration Effects 0.000 description 1
238000006703 hydration reaction Methods 0.000 description 1
239000012263 liquid product Substances 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000012528 membrane Substances 0.000 description 1
239000002808 molecular sieve Substances 0.000 description 1
238000005457 optimization Methods 0.000 description 1
238000005191 phase separation Methods 0.000 description 1
150000008442 polyphenolic compounds Chemical class 0.000 description 1
235000013824 polyphenols Nutrition 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
239000011148 porous material Substances 0.000 description 1
239000003380 propellant Substances 0.000 description 1
238000005204 segregation Methods 0.000 description 1
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
239000002689 soil Substances 0.000 description 1
230000003381 solubilizing effect Effects 0.000 description 1
239000002904 solvent Substances 0.000 description 1
239000000126 substance Substances 0.000 description 1
125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
239000004753 textile Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/03—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by addition of hydroxy groups to unsaturated carbon-to-carbon bonds, e.g. with the aid of H2O2
- C07C29/04—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by addition of hydroxy groups to unsaturated carbon-to-carbon bonds, e.g. with the aid of H2O2 by hydration of carbon-to-carbon double bonds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C11/00—Fermentation processes for beer
- C12C11/02—Pitching yeast

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
General Health & Medical Sciences (AREA)
Genetics & Genomics (AREA)
Food Science & Technology (AREA)
Biochemistry (AREA)
Bioinformatics & Cheminformatics (AREA)
General Engineering & Computer Science (AREA)
Mycology (AREA)
Health & Medical Sciences (AREA)
Microbiology (AREA)
Wood Science & Technology (AREA)
Zoology (AREA)
Chemical Kinetics & Catalysis (AREA)
General Chemical & Material Sciences (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Liquid Carbonaceous Fuels (AREA)

DD81228774A 1980-03-31 1981-03-31 Verfahren zur gewinnung von c tief 2-bis c tief 4-alkoholen DD157700A5 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
IT21068/80A IT1140794B (it)	1980-03-31	1980-03-31	Procedimento per la produzione di alcoli c2-c4 "grado benzine" da miscele acquose che li contengono

Publications (1)

Publication Number	Publication Date
DD157700A5 true DD157700A5 (de)	1982-12-01

Family

ID=11176255

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DD81228774A DD157700A5 (de)	1980-03-31	1981-03-31	Verfahren zur gewinnung von c tief 2-bis c tief 4-alkoholen

Country Status (25)

Country	Link
JP (1)	JPS56151790A (fr)
AU (1)	AU550088B2 (fr)
BE (1)	BE888150A (fr)
BR (1)	BR8101872A (fr)
CA (1)	CA1160252A (fr)
CH (1)	CH648340A5 (fr)
CS (1)	CS221292B2 (fr)
DD (1)	DD157700A5 (fr)
DE (1)	DE3112277C2 (fr)
DK (1)	DK137281A (fr)
ES (1)	ES501396A0 (fr)
FR (1)	FR2479186A1 (fr)
GB (1)	GB2072668B (fr)
HU (1)	HU192065B (fr)
IE (1)	IE51127B1 (fr)
IT (1)	IT1140794B (fr)
LU (1)	LU83265A1 (fr)
NL (1)	NL8101594A (fr)
NO (1)	NO811022L (fr)
NZ (1)	NZ196606A (fr)
PL (1)	PL230427A1 (fr)
RO (1)	RO84498B (fr)
SE (1)	SE8101977L (fr)
SU (1)	SU1034610A3 (fr)
YU (1)	YU41038B (fr)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH0723331B2 (ja) *	1985-03-12	1995-03-15	旭化成工業株式会社	第３級ブタノ−ルの製造方法
US7007764B2 (en)	2002-12-06	2006-03-07	Manitowoc Crane Companies, Inc.	Carbody to crawler connection
JP2007021643A (ja) *	2005-07-15	2007-02-01	Amada Co Ltd	永久磁石を用いたワーク吸着装置
US10570071B1 (en)	2018-12-12	2020-02-25	Saudi Arabian Oil Company	Membrane-based process for butanols production from mixed butenes

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
NL299568A (fr) *		1900-01-01
FR1314120A (fr) *	1962-01-08	1963-01-04	Bayer Ag	Procédé de préparation d'éthers de tert.-butyle et d'alcoyles
DE1249844B (de) *	1962-03-21	1967-09-14	GuIf Research &. Development Company, Pittsburgh, Pa (V St A)	Verfahren zur Herstellung von Alkoholen durch Anlagerung von Wasser an die entsprechenden Olefine m flussiger Phase
US3822119A (en) *	1970-11-19	1974-07-02	Goodyear Tire & Rubber	Anti-pollution anti-knock gasoline
DE2629769C3 (de) *	1976-07-02	1989-03-16	Hüls AG, 4370 Marl	Verfahren zur Herstellung von reinem Methyl-tertiär-butyläther
US4087471A (en) *	1977-05-20	1978-05-02	Petro-Tex Chemical Corporation	Fixed bed process for the production of t-butanol

1980
- 1980-03-31 IT IT21068/80A patent/IT1140794B/it active
1981
- 1981-03-18 IE IE602/81A patent/IE51127B1/en unknown
- 1981-03-19 GB GB8108640A patent/GB2072668B/en not_active Expired
- 1981-03-24 NZ NZ196606A patent/NZ196606A/en unknown
- 1981-03-26 BR BR8101872A patent/BR8101872A/pt unknown
- 1981-03-26 NO NO811022A patent/NO811022L/no unknown
- 1981-03-26 DK DK137281A patent/DK137281A/da not_active Application Discontinuation
- 1981-03-26 FR FR8106118A patent/FR2479186A1/fr active Granted
- 1981-03-27 DE DE3112277A patent/DE3112277C2/de not_active Expired
- 1981-03-27 SE SE8101977A patent/SE8101977L/xx not_active Application Discontinuation
- 1981-03-27 BE BE0/204278A patent/BE888150A/fr not_active IP Right Cessation
- 1981-03-30 JP JP4566881A patent/JPS56151790A/ja active Pending
- 1981-03-30 RO RO103858A patent/RO84498B/ro unknown
- 1981-03-30 AU AU68903/81A patent/AU550088B2/en not_active Ceased
- 1981-03-30 PL PL23042781A patent/PL230427A1/xx unknown
- 1981-03-30 HU HU81810A patent/HU192065B/hu unknown
- 1981-03-30 YU YU828/81A patent/YU41038B/xx unknown
- 1981-03-30 LU LU83265A patent/LU83265A1/fr unknown
- 1981-03-30 CH CH2146/81A patent/CH648340A5/it not_active IP Right Cessation
- 1981-03-30 SU SU813266251A patent/SU1034610A3/ru active
- 1981-03-30 CA CA000374128A patent/CA1160252A/fr not_active Expired
- 1981-03-31 CS CS812393A patent/CS221292B2/cs unknown
- 1981-03-31 NL NL8101594A patent/NL8101594A/nl not_active Application Discontinuation
- 1981-03-31 DD DD81228774A patent/DD157700A5/de unknown
- 1981-03-31 ES ES501396A patent/ES501396A0/es active Granted

Also Published As

Publication number	Publication date
NL8101594A (nl)	1981-10-16
RO84498A (fr)	1984-06-21
IE51127B1 (en)	1986-10-15
IT8021068A0 (it)	1980-03-31
NO811022L (no)	1981-10-01
YU82881A (en)	1983-02-28
PL230427A1 (fr)	1981-11-13
GB2072668A (en)	1981-10-07
DK137281A (da)	1981-10-01
DE3112277A1 (de)	1982-03-18
DE3112277C2 (de)	1985-05-02
RO84498B (ro)	1984-08-30
YU41038B (en)	1986-10-31
SE8101977L (sv)	1981-10-01
AU550088B2 (en)	1986-03-06
BR8101872A (pt)	1981-10-06
LU83265A1 (fr)	1981-10-29
FR2479186B1 (fr)	1982-11-26
CA1160252A (fr)	1984-01-10
SU1034610A3 (ru)	1983-08-07
IE810602L (en)	1981-09-30
JPS56151790A (en)	1981-11-24
GB2072668B (en)	1984-03-28
CS221292B2 (en)	1983-04-29
CH648340A5 (it)	1985-03-15
HU192065B (en)	1987-05-28
ES8202776A1 (es)	1982-02-16
AU6890381A (en)	1981-10-08
NZ196606A (en)	1984-03-16
FR2479186A1 (fr)	1981-10-02
IT1140794B (it)	1986-10-10
BE888150A (fr)	1981-09-28
ES501396A0 (es)	1982-02-16

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DE69918017T2 (de)	2005-07-07	Verfahren zur Herstellung eines Treibmittelbestandteils
EP1519906B1 (fr)	2009-02-25	Procede pour la production de methyl-tert-butylether de grande purete
DE19906518A1 (de)	2000-08-31	Verfahren zur Fraktionierung von Dibuten
EP1813588B1 (fr)	2012-01-04	Procédé de préparation de l'éthyl tert-butyl éther à partir de mélanges d'hydrocarbures C4
DE2521964A1 (de)	1975-11-27	Verfahren zur herstellung von teralkylaethern
DE10102082A1 (de)	2002-05-02	Verfahren zur Herstellung von hochreinem Raffinat II und Methyl-tert.-butylether
DD222301A5 (de)	1985-05-15	Verfahren zur gewinnung von hochreinem 1-buten
DD147664A5 (de)	1981-04-15	Verfahren zur gleichzeitigen herstellung von reinem methyl-tert.-butylether
EP0082316B1 (fr)	1985-07-03	Procédé de production de méthyl tertiobutyl éther (MTBE) et d'hydrocarbure-raffinates délivrés largement d'i-butène et méthanol et appareil pour la mise en oeuvre
EP1989239B1 (fr)	2011-05-04	Procede de fabrication de polyisobutylene ayant une teneur en doubles liaisons terminales superieure a 50 % a partir d'un courant technique d'hydrocarbures en c4 contenant du 1-butene, du 2-butene et de l'isobutene
DE3015346A1 (de)	1980-11-06	Verfahren zur herstellung von methyl-tert.-butylaether aus methanol und isobuten
DD207194A5 (de)	1984-02-22	Verfahren zur herstellung von tert-butylalkylaethern
WO2004018393A1 (fr)	2004-03-04	Procede de production d'isobutene a partir d'ether methyltertiobutylique technique
EP0068194B1 (fr)	1985-01-16	Procédé pour la séparation de tert.-oléfines pures à partir de mélanges de hydrocarbures
EP3798202A1 (fr)	2021-03-31	Procédé de purification du méthacrylate de méthyle des composants à bas point d'ébullition
DE2521963B2 (de)	1980-10-09	Verfahren zur Herstellung von Terbutyläthern
EP1431264A1 (fr)	2004-06-23	Procédé pour la préparation de tert.-butanol
DE3140573A1 (de)	1982-07-15	Verfahren zur veredelung von olefinischen c(pfeil abwaerts)4(pfeil abwaerts)-fraktionen
DD263978A5 (de)	1989-01-18	Verfahren zur herstellung von isopropylalkohol und tertiaeren c tief 4- bis c tief 5- alkoholen
DE3112277C2 (de)	1985-05-02	Verfahren zur Gewinnung eines Benzinzusatzes
DE69203017T2 (de)	1995-11-02	Verfahren zur Trennung von Ehtyl-tert-butylether aus Ethanol enthaltenden Mischungen.
EP0198236A2 (fr)	1986-10-22	Catalyseur et procédé de préparation d'oléfines tertiaires pures
DE3003126A1 (de)	1980-07-31	Verfahren zur herstellung von sek.-butanol
EP0257511B1 (fr)	1990-11-07	Procédé pour la préparation de l'alcool isopropylique et d'alcools tertiaires en C4 à C5
EP1462433B1 (fr)	2013-10-23	Procédé pour la séparation de 2-butanol d' un mélange tert.-butanol/eau