DD284812A5 - Verfahren zur granulierung von 1,5-diacetyl-2,4-dioxohexahydro-1,3,5-triazin - Google Patents

Verfahren zur granulierung von 1,5-diacetyl-2,4-dioxohexahydro-1,3,5-triazin Download PDF

Info

Publication number: DD284812A5
Authority: DD; German Democratic Republic
Prior art keywords: granulation; dadht; granules; fluidized bed; powder
Prior art date: 1989-06-09

Application number

DD32940589A

Other languages

German (de)

English (en)

Inventor

Dietrich Voigt

Guenther Gehrke

Wolfgang Beckhaus

Harald Schmidt

Eberhard Heynisch

Eberhard Schmidt

Bernd-Ruediger Meinhard

Hans-Peter Winkler

Original Assignee

Veb Leuna-Werke "Walter Ulbricht",Dd

Veb Waschmittelwerk Genthin,Dd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-06-09

Filing date

1989-06-09

Publication date

1990-11-28

1989-06-09 Application filed by Veb Leuna-Werke "Walter Ulbricht",Dd, Veb Waschmittelwerk Genthin,Dd filed Critical Veb Leuna-Werke "Walter Ulbricht",Dd

1989-06-09 Priority to DD32940589A priority Critical patent/DD284812A5/de

1990-06-08 Priority to EP19900110883 priority patent/EP0401851A3/fr

1990-11-28 Publication of DD284812A5 publication Critical patent/DD284812A5/de

Links

238000000034 method Methods 0.000 title claims abstract description 26
LYPVKWMHGFMDPD-UHFFFAOYSA-N 1,5-diacetyl-1,3,5-triazinane-2,4-dione Chemical compound CC(=O)N1CN(C(C)=O)C(=O)NC1=O LYPVKWMHGFMDPD-UHFFFAOYSA-N 0.000 title 1
238000005469 granulation Methods 0.000 claims abstract description 32
230000003179 granulation Effects 0.000 claims abstract description 32
239000008187 granular material Substances 0.000 claims abstract description 22
239000000126 substance Substances 0.000 claims abstract description 19
238000001704 evaporation Methods 0.000 claims abstract description 14
230000008020 evaporation Effects 0.000 claims abstract description 14
239000000203 mixture Substances 0.000 claims abstract description 12
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
239000004094 surface-active agent Substances 0.000 claims abstract description 9
239000013543 active substance Substances 0.000 claims abstract description 3
239000003979 granulating agent Substances 0.000 claims abstract description 3
239000012530 fluid Substances 0.000 claims abstract 3
239000000243 solution Substances 0.000 claims description 12
239000000843 powder Substances 0.000 claims description 11
239000007864 aqueous solution Substances 0.000 claims description 9
239000007787 solid Substances 0.000 claims description 9
239000003599 detergent Substances 0.000 claims description 8
238000003860 storage Methods 0.000 claims description 8
239000002245 particle Substances 0.000 claims description 6
239000012190 activator Substances 0.000 claims description 5
239000007788 liquid Substances 0.000 claims description 5
239000007844 bleaching agent Substances 0.000 claims description 4
238000002360 preparation method Methods 0.000 claims description 3
238000001228 spectrum Methods 0.000 claims description 3
239000004615 ingredient Substances 0.000 claims description 2
238000005406 washing Methods 0.000 claims description 2
239000004480 active ingredient Substances 0.000 claims 4
229910019142 PO4 Inorganic materials 0.000 claims 2
239000000428 dust Substances 0.000 claims 2
235000021317 phosphate Nutrition 0.000 claims 2
238000001694 spray drying Methods 0.000 claims 2
238000009736 wetting Methods 0.000 claims 2
239000000654 additive Substances 0.000 claims 1
230000000996 additive effect Effects 0.000 claims 1
230000009286 beneficial effect Effects 0.000 claims 1
239000003795 chemical substances by application Substances 0.000 claims 1
230000000295 complement effect Effects 0.000 claims 1
238000010924 continuous production Methods 0.000 claims 1
238000004090 dissolution Methods 0.000 claims 1
238000005265 energy consumption Methods 0.000 claims 1
239000003337 fertilizer Substances 0.000 claims 1
238000004519 manufacturing process Methods 0.000 claims 1
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 1
239000010452 phosphate Substances 0.000 claims 1
150000003013 phosphoric acid derivatives Chemical class 0.000 claims 1
230000006641 stabilisation Effects 0.000 claims 1
238000011105 stabilization Methods 0.000 claims 1
239000000725 suspension Substances 0.000 claims 1
239000006193 liquid solution Substances 0.000 abstract 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
229910052708 sodium Inorganic materials 0.000 description 4
239000011734 sodium Substances 0.000 description 4
XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 3
229920001807 Urea-formaldehyde Polymers 0.000 description 3
239000004202 carbamide Substances 0.000 description 3
239000007859 condensation product Substances 0.000 description 3
ODGAOXROABLFNM-UHFFFAOYSA-N polynoxylin Chemical compound O=C.NC(N)=O ODGAOXROABLFNM-UHFFFAOYSA-N 0.000 description 3
YTFXKURWTLWPKK-UHFFFAOYSA-N 1,3,5-triazinane-2,4-dione Chemical compound O=C1NCNC(=O)N1 YTFXKURWTLWPKK-UHFFFAOYSA-N 0.000 description 2
KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 description 2
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
238000000889 atomisation Methods 0.000 description 2
150000002191 fatty alcohols Chemical class 0.000 description 2
238000010348 incorporation Methods 0.000 description 2
239000002689 soil Substances 0.000 description 2
JIHQDMXYYFUGFV-UHFFFAOYSA-N 1,3,5-triazine Chemical compound C1=NC=NC=N1 JIHQDMXYYFUGFV-UHFFFAOYSA-N 0.000 description 1
229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
OHJMTUPIZMNBFR-UHFFFAOYSA-N biuret Chemical compound NC(=O)NC(N)=O OHJMTUPIZMNBFR-UHFFFAOYSA-N 0.000 description 1
239000001768 carboxy methyl cellulose Substances 0.000 description 1
235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
239000008112 carboxymethyl-cellulose Substances 0.000 description 1
239000000470 constituent Substances 0.000 description 1
239000012153 distilled water Substances 0.000 description 1
239000003995 emulsifying agent Substances 0.000 description 1
238000000605 extraction Methods 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
238000004128 high performance liquid chromatography Methods 0.000 description 1
238000000265 homogenisation Methods 0.000 description 1
230000007062 hydrolysis Effects 0.000 description 1
238000006460 hydrolysis reaction Methods 0.000 description 1
ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 1
239000000463 material Substances 0.000 description 1
KQVLODRFGIKJHZ-UHFFFAOYSA-N methylenediurea Chemical compound NC(=O)NCNC(N)=O KQVLODRFGIKJHZ-UHFFFAOYSA-N 0.000 description 1
238000002156 mixing Methods 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
239000000047 product Substances 0.000 description 1
239000002994 raw material Substances 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
229910052938 sodium sulfate Inorganic materials 0.000 description 1
235000011152 sodium sulphate Nutrition 0.000 description 1
238000004448 titration Methods 0.000 description 1
238000011144 upstream manufacturing Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3902—Organic or inorganic per-compounds combined with specific additives
- C11D3/3905—Bleach activators or bleach catalysts
- C11D3/3907—Organic compounds
- C11D3/3917—Nitrogen-containing compounds
- C11D3/392—Heterocyclic compounds, e.g. cyclic imides or lactames
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/28—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic using special binding agents

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Inorganic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Detergent Compositions (AREA)

DD32940589A 1989-06-09 1989-06-09 Verfahren zur granulierung von 1,5-diacetyl-2,4-dioxohexahydro-1,3,5-triazin DD284812A5 (de)

Priority Applications (2)

Application Number	Priority Date	Filing Date	Title
DD32940589A DD284812A5 (de)	1989-06-09	1989-06-09	Verfahren zur granulierung von 1,5-diacetyl-2,4-dioxohexahydro-1,3,5-triazin
EP19900110883 EP0401851A3 (fr)	1989-06-09	1990-06-08	Procédé et moyen de granulation pour granuler le 1,5-diacétyl-2,4-dioxohexahydro-1,3,5-triazine

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DD32940589A DD284812A5 (de)	1989-06-09	1989-06-09	Verfahren zur granulierung von 1,5-diacetyl-2,4-dioxohexahydro-1,3,5-triazin

Publications (1)

Publication Number	Publication Date
DD284812A5 true DD284812A5 (de)	1990-11-28

Family

ID=5609778

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DD32940589A DD284812A5 (de)	1989-06-09	1989-06-09	Verfahren zur granulierung von 1,5-diacetyl-2,4-dioxohexahydro-1,3,5-triazin

Country Status (2)

Country	Link
EP (1)	EP0401851A3 (fr)
DD (1)	DD284812A5 (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
AU2002344156A1 (en) *	2001-05-25	2002-12-09	Henkel Kommanditgesellschaft Auf Aktien	Granules containing one or more highly active substances and method for producing the same

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DD229692B3 (de) *	1984-12-17	1991-09-19	Leuna-Werke Ag,De	Verfahren zur herstellung von 2,4-dioxohexahydro-1.3.5-triazin
DD255881B3 (de) *	1986-11-07	1993-01-07	Waschmittelwerk Genthin Gmbh	Granulationsverfahren fuer 1.5-diacetyl-2.4-dioxo-hexahydro-1.3.5-triazin (dadht)
DD255884A1 (de) *	1986-11-07	1988-04-20	Leuna Werke Veb	Verfahren zur granulierung von 1,5-diacetyl-2,4-dioxo-hexahydro-1,3,5-triazin

1989
- 1989-06-09 DD DD32940589A patent/DD284812A5/de not_active IP Right Cessation
1990
- 1990-06-08 EP EP19900110883 patent/EP0401851A3/fr not_active Withdrawn

Also Published As

Publication number	Publication date
EP0401851A3 (fr)	1991-12-11
EP0401851A2 (fr)	1990-12-12

Legal Events

Date	Code	Title
1994-03-17	RPI	Change in the person, name or address of the patentee (searches according to art. 11 and 12 extension act)
1994-06-23	RPI	Change in the person, name or address of the patentee (searches according to art. 11 and 12 extension act)
1994-12-08	RPI	Change in the person, name or address of the patentee (searches according to art. 11 and 12 extension act)
1995-08-31	RPV	Change in the person, the name or the address of the representative (searches according to art. 11 and 12 extension act)
1998-04-23	ENJ	Ceased due to non-payment of renewal fee

Publication	Publication Date	Title
EP0550508B2 (fr)	1998-10-21	Procede de sechage de matieres de valeur et de melanges de matieres de valeur par pulverisation avec utilisation de vapeur d'eau surchauffee
DE69920899T2 (de)	2006-03-02	Umhüllte parfümteilchen und diese enthaltende waschmittelzusammensetzungen
DE68921858T2 (de)	1995-11-16	Verfahren zur Herstellung von Bleichmittelgranulaten.
EP0663946B1 (fr)	1997-04-09	Produits d'interet et melanges de produits d'interet pour agents mouillants, detergents et/ou nettoyants sous une nouvelle forme de preparation
DE2825039C3 (de)	1987-04-16	Verfahren zur Herstellung von Harnstoffkörnern
DE69207727T2 (de)	1996-09-19	Verfahren zur Herstellung von Salzgranulaten
DE4435743C2 (de)	1998-11-26	Verfahren zur Herstellung eines Mehrkomponenten-Granulates
DE69701731T2 (de)	2000-08-10	Verfahren zur herstellung einer waschmittelzusammensetzung
EP0084657A1 (fr)	1983-08-03	Agents de lavage granulaires très moussants séchés par pulvérisation avec une stabilité élevée des granulations et procédé pour sa fabrication
DE3804509A1 (de)	1989-08-24	Kontinuierliches verfahren zur herstellung von natriumperborat-granulaten
DE69716177T2 (de)	2003-05-28	Verfahren zur herstellung von granuliertem harnstoff
DE4208773A1 (de)	1993-09-23	Verfahren zur trocknung von wertstoffen oder deren gemischen, die als netz-, wasch- und/oder reinigungsmittel geeignet sind
WO2004073403A1 (fr)	2004-09-02	Procede de fabrication de granules dispersibles dans l'eau
DE60210339T2 (de)	2006-08-24	Freifliessendes melamincyanuratagglomerat
NL193406C (nl)	1999-09-06	Kunstmest met een hoge hardheid en opslagstabiliteit, alsmede de bereiding hiervan.
DE2431529A1 (de)	1976-01-22	Verfahren zur herstellung spruehgetrockneter, nichtionische tenside enthaltender waschmittel
DD140987A1 (de)	1980-04-09	Kontinuierliches herstellungsverfahren granulierter wasch-und reinigungsmittel in wirbelschichtapparaten
EP0431091A1 (fr)	1991-06-12	Procede antipoussiere pour granules d'engrais.
DE3539631C2 (de)	1997-07-31	Verfahren zur Herstellung von Oligomethylenharnstoffgemischen
EP0401851A2 (fr)	1990-12-12	Procédé et moyen de granulation pour granuler le 1,5-diacétyl-2,4-dioxohexahydro-1,3,5-triazine
DE3126884C2 (fr)	1989-11-16
EP0804535B1 (fr)	1998-11-18	Detergents et nettoyants de blanchiment sous forme de granulats
AT391121B (de)	1990-08-27	Verfahren zur herstellung von granuliertem stabilisiertem natriumperkarbonat
WO1993019151A1 (fr)	1993-09-30	Additif granulaire sans phosphate contenant des tensioactifs non ioniques pour produits de lavage et detergents
EP0061600B1 (fr)	1985-01-30	Procédé de fabrication de granulés mixtes de phosphates condensés et de charges