DD295606A5 - Verfahren zur reinigung von mit metallkationen verunreinigten waessrigen wasserstoffperoxidloesungen - Google Patents
Verfahren zur reinigung von mit metallkationen verunreinigten waessrigen wasserstoffperoxidloesungen Download PDFInfo
- Publication number
- DD295606A5 DD295606A5 DD90343002A DD34300290A DD295606A5 DD 295606 A5 DD295606 A5 DD 295606A5 DD 90343002 A DD90343002 A DD 90343002A DD 34300290 A DD34300290 A DD 34300290A DD 295606 A5 DD295606 A5 DD 295606A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- hydrogen peroxide
- solution
- exchange resin
- membrane
- cations
- Prior art date
Links
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title claims abstract description 82
- 238000000034 method Methods 0.000 title claims abstract description 55
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 13
- 239000002184 metal Substances 0.000 title claims abstract description 13
- 150000001768 cations Chemical class 0.000 title claims description 16
- 238000004140 cleaning Methods 0.000 title 1
- 239000000243 solution Substances 0.000 claims abstract description 47
- 239000012528 membrane Substances 0.000 claims abstract description 35
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000011347 resin Substances 0.000 claims abstract description 20
- 229920005989 resin Polymers 0.000 claims abstract description 20
- 229910052723 transition metal Inorganic materials 0.000 claims abstract description 17
- 150000003624 transition metals Chemical class 0.000 claims abstract description 16
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims abstract description 12
- 150000002739 metals Chemical class 0.000 claims abstract description 8
- 239000011148 porous material Substances 0.000 claims abstract description 6
- 239000006185 dispersion Substances 0.000 claims abstract description 5
- 230000008569 process Effects 0.000 claims description 17
- 239000003729 cation exchange resin Substances 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 11
- 239000002245 particle Substances 0.000 claims description 7
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 4
- -1 polytetrafluoroethylene Polymers 0.000 claims description 4
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 4
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 4
- 239000007858 starting material Substances 0.000 claims description 4
- 238000003860 storage Methods 0.000 claims description 4
- 230000002378 acidificating effect Effects 0.000 claims description 3
- 229920001903 high density polyethylene Polymers 0.000 claims description 2
- 239000004700 high-density polyethylene Substances 0.000 claims description 2
- 239000004033 plastic Substances 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 claims description 2
- 125000000542 sulfonic acid group Chemical group 0.000 claims description 2
- 239000000725 suspension Substances 0.000 claims 2
- 239000012736 aqueous medium Substances 0.000 claims 1
- 150000002978 peroxides Chemical class 0.000 abstract description 15
- 238000000746 purification Methods 0.000 abstract description 10
- 239000012535 impurity Substances 0.000 abstract description 9
- 239000003456 ion exchange resin Substances 0.000 abstract description 9
- 229920003303 ion-exchange polymer Polymers 0.000 abstract description 9
- 238000011282 treatment Methods 0.000 abstract description 7
- 238000000354 decomposition reaction Methods 0.000 abstract description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 4
- 229910001413 alkali metal ion Inorganic materials 0.000 abstract description 4
- 229910001420 alkaline earth metal ion Inorganic materials 0.000 abstract description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract description 2
- 239000003513 alkali Substances 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 abstract description 2
- 229910052802 copper Inorganic materials 0.000 abstract description 2
- 239000010949 copper Substances 0.000 abstract description 2
- 229910052742 iron Inorganic materials 0.000 abstract description 2
- 239000012527 feed solution Substances 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- 229910021645 metal ion Inorganic materials 0.000 description 10
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 8
- 229910052791 calcium Inorganic materials 0.000 description 8
- 239000011575 calcium Substances 0.000 description 8
- 150000002500 ions Chemical class 0.000 description 8
- 229910052708 sodium Inorganic materials 0.000 description 8
- 239000011734 sodium Substances 0.000 description 8
- 229910001428 transition metal ion Inorganic materials 0.000 description 6
- 239000002253 acid Substances 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 238000004821 distillation Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 125000001424 substituent group Chemical group 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 150000001340 alkali metals Chemical class 0.000 description 2
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 2
- 150000004056 anthraquinones Chemical class 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- CHRJZRDFSQHIFI-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;styrene Chemical compound C=CC1=CC=CC=C1.C=CC1=CC=CC=C1C=C CHRJZRDFSQHIFI-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000005341 cation exchange Methods 0.000 description 1
- 229940023913 cation exchange resins Drugs 0.000 description 1
- 229920002301 cellulose acetate Polymers 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229910052602 gypsum Inorganic materials 0.000 description 1
- 239000010440 gypsum Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 229910001410 inorganic ion Inorganic materials 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 150000001457 metallic cations Chemical class 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 150000004968 peroxymonosulfuric acids Chemical class 0.000 description 1
- 229920003053 polystyrene-divinylbenzene Polymers 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/14—Ultrafiltration; Microfiltration
- B01D61/147—Microfiltration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/013—Separation; Purification; Concentration
- C01B15/0135—Purification by solid ion-exchangers or solid chelating agents
Landscapes
- Chemical & Material Sciences (AREA)
- Water Supply & Treatment (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Detergent Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treatment Of Water By Ion Exchange (AREA)
- Treatment Of Water By Oxidation Or Reduction (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Compounds Of Unknown Constitution (AREA)
- Removal Of Specific Substances (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB898916934A GB8916934D0 (en) | 1989-07-25 | 1989-07-25 | Purification of hydrogen peroxide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD295606A5 true DD295606A5 (de) | 1991-11-07 |
Family
ID=10660564
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD90343002A DD295606A5 (de) | 1989-07-25 | 1990-07-23 | Verfahren zur reinigung von mit metallkationen verunreinigten waessrigen wasserstoffperoxidloesungen |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US5215665A (fr) |
| EP (1) | EP0484371B1 (fr) |
| JP (1) | JP3032903B2 (fr) |
| AT (1) | ATE119856T1 (fr) |
| AU (1) | AU641417B2 (fr) |
| BR (1) | BR9007560A (fr) |
| CA (1) | CA2064090C (fr) |
| DD (1) | DD295606A5 (fr) |
| DE (1) | DE69017907T2 (fr) |
| ES (1) | ES2072439T3 (fr) |
| GB (1) | GB8916934D0 (fr) |
| MY (1) | MY107128A (fr) |
| WO (1) | WO1991001267A1 (fr) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1336474C (fr) * | 1989-04-20 | 1995-08-01 | Martin Blake Hocking | Recuperation du peroxyde d'hydrogene a partir de solutions aqueuses colorees |
| CA2169158A1 (fr) * | 1993-08-11 | 1995-02-16 | Paul James Collins | Methode de traitement de peroxyde |
| JP2976776B2 (ja) * | 1993-10-12 | 1999-11-10 | 住友化学工業株式会社 | 過酸化水素水の精製方法 |
| FR2754529B1 (fr) * | 1996-10-15 | 1998-11-06 | Chemoxal Sa | Procede de purification de peroxyde d'hydrogene |
| JPH10236804A (ja) * | 1996-12-05 | 1998-09-08 | Startec Ventures Inc | 超高純度過酸化水素の現場製造システムおよび方法 |
| US6255009B1 (en) | 1998-03-28 | 2001-07-03 | The United States Of America As Represented By The Secretary Of The Navy | Combined cycle power generation using controlled hydrogen peroxide decomposition |
| US20040126313A1 (en) * | 2002-06-24 | 2004-07-01 | Haase Richard A. | Methods and processes of hydrogen peroxide production |
| US8268269B2 (en) * | 2006-01-24 | 2012-09-18 | Clearvalue Technologies, Inc. | Manufacture of water chemistries |
| JP5905207B2 (ja) * | 2011-04-21 | 2016-04-20 | 丸善石油化学株式会社 | 金属不純物量の少ない半導体リソグラフィー用共重合体の製造方法及び該共重合体を製造するための重合開始剤の精製方法 |
| US11028675B2 (en) | 2014-08-15 | 2021-06-08 | Global Oil EOR Systems, Ltd. | Hydrogen peroxide steam generator for oilfield applications |
| WO2016164380A1 (fr) * | 2015-04-06 | 2016-10-13 | Rasirc, Inc. | Procédés et systèmes de purification de solutions de peroxyde d'hydrogène |
| BR112021001869A2 (pt) | 2018-08-02 | 2021-04-27 | Evonik Corporation | soluções aquosas de peróxido de hidrogênio estabilizadas por polímero |
| US20210363008A1 (en) | 2018-08-02 | 2021-11-25 | Evonik Corporation | Process for preparing a stabilized aqueous hydrogen peroxide solution |
| US11059633B2 (en) | 2019-10-31 | 2021-07-13 | Cheer Pack North America | Flip-top closure for container |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1141299A (en) * | 1965-06-21 | 1969-01-29 | Laporte Chemical | Process for or relating to the production of hydrogen peroxide |
| US3944485A (en) * | 1973-05-23 | 1976-03-16 | California Institute Of Technology | Ion-exchange hollow fibers |
| US4132762A (en) * | 1977-10-31 | 1979-01-02 | Shell Oil Company | Hydrogen peroxide stabilization |
| JPH01153509A (ja) * | 1987-12-11 | 1989-06-15 | Tokai Denka Kogyo Kk | 高純度過酸化水素の製造方法 |
| US4879043A (en) * | 1988-07-20 | 1989-11-07 | E. I. Du Pont De Nemours And Company | Manufacture of high purity hydrogen peroxide by using reverse osmosis osmosis |
-
1989
- 1989-07-25 GB GB898916934A patent/GB8916934D0/en active Pending
-
1990
- 1990-07-12 MY MYPI90001165A patent/MY107128A/en unknown
- 1990-07-18 EP EP90910858A patent/EP0484371B1/fr not_active Expired - Lifetime
- 1990-07-18 AT AT90910858T patent/ATE119856T1/de not_active IP Right Cessation
- 1990-07-18 CA CA002064090A patent/CA2064090C/fr not_active Expired - Fee Related
- 1990-07-18 ES ES90910858T patent/ES2072439T3/es not_active Expired - Lifetime
- 1990-07-18 US US07/807,824 patent/US5215665A/en not_active Expired - Fee Related
- 1990-07-18 DE DE69017907T patent/DE69017907T2/de not_active Expired - Fee Related
- 1990-07-18 AU AU60312/90A patent/AU641417B2/en not_active Ceased
- 1990-07-18 JP JP2510034A patent/JP3032903B2/ja not_active Expired - Lifetime
- 1990-07-18 BR BR909007560A patent/BR9007560A/pt not_active IP Right Cessation
- 1990-07-18 WO PCT/GB1990/001102 patent/WO1991001267A1/fr not_active Ceased
- 1990-07-23 DD DD90343002A patent/DD295606A5/de not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| JPH04506952A (ja) | 1992-12-03 |
| CA2064090C (fr) | 2000-08-15 |
| DE69017907T2 (de) | 1995-09-28 |
| CA2064090A1 (fr) | 1991-01-26 |
| AU641417B2 (en) | 1993-09-23 |
| US5215665A (en) | 1993-06-01 |
| WO1991001267A1 (fr) | 1991-02-07 |
| EP0484371B1 (fr) | 1995-03-15 |
| JP3032903B2 (ja) | 2000-04-17 |
| AU6031290A (en) | 1991-02-22 |
| GB8916934D0 (en) | 1989-09-13 |
| MY107128A (en) | 1995-09-30 |
| ATE119856T1 (de) | 1995-04-15 |
| EP0484371A1 (fr) | 1992-05-13 |
| DE69017907D1 (de) | 1995-04-20 |
| BR9007560A (pt) | 1992-06-23 |
| ES2072439T3 (es) | 1995-07-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ENJ | Ceased due to non-payment of renewal fee |