DE60006277T2 - Verfahren zur reinigung von minderwertigen zuckersirupen mit nanofiltration - Google Patents

Verfahren zur reinigung von minderwertigen zuckersirupen mit nanofiltration Download PDF

Info

Publication number: DE60006277T2
Authority: DE; Germany
Prior art keywords: nanofiltration; sucrose; syrup; sugar; molasses
Prior art date: 1999-11-17
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

DE60006277T

Other languages

German (de)

English (en)

Other versions

DE60006277D1 (de

Inventor

Michael Great Dunmow DONOVAN

Marc Hlavacek

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Tate and Lyle Industries Ltd

Original Assignee

Tate and Lyle Industries Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1999-11-17

Filing date

2000-11-13

Publication date

2004-07-15

1999-11-17 Priority claimed from US09/441,988 external-priority patent/US6355110B1/en

2000-11-13 Application filed by Tate and Lyle Industries Ltd filed Critical Tate and Lyle Industries Ltd

2003-12-04 Application granted granted Critical

2003-12-04 Publication of DE60006277D1 publication Critical patent/DE60006277D1/de

2004-07-15 Publication of DE60006277T2 publication Critical patent/DE60006277T2/de

2020-11-14 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 82
238000001728 nano-filtration Methods 0.000 title claims abstract description 81
235000020374 simple syrup Nutrition 0.000 title description 4
238000004140 cleaning Methods 0.000 title 1
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 145
229930006000 Sucrose Natural products 0.000 claims abstract description 141
239000005720 sucrose Substances 0.000 claims abstract description 109
235000020357 syrup Nutrition 0.000 claims abstract description 95
239000006188 syrup Substances 0.000 claims abstract description 95
235000013379 molasses Nutrition 0.000 claims abstract description 83
239000012528 membrane Substances 0.000 claims abstract description 77
235000000346 sugar Nutrition 0.000 claims abstract description 50
238000002425 crystallisation Methods 0.000 claims abstract description 44
230000008025 crystallization Effects 0.000 claims abstract description 44
239000012466 permeate Substances 0.000 claims abstract description 44
239000012465 retentate Substances 0.000 claims abstract description 40
238000011084 recovery Methods 0.000 claims abstract description 11
235000011389 fruit/vegetable juice Nutrition 0.000 claims description 60
229960004903 invert sugar Drugs 0.000 claims description 49
238000001471 micro-filtration Methods 0.000 claims description 41
238000000108 ultra-filtration Methods 0.000 claims description 38
235000007201 Saccharum officinarum Nutrition 0.000 claims description 27
240000000111 Saccharum officinarum Species 0.000 claims description 27
239000000463 material Substances 0.000 claims description 26
238000011026 diafiltration Methods 0.000 claims description 17
239000000203 mixture Substances 0.000 claims description 10
150000004676 glycans Chemical class 0.000 claims description 9
239000005017 polysaccharide Substances 0.000 claims description 9
229920001282 polysaccharide Polymers 0.000 claims description 9
238000007670 refining Methods 0.000 claims description 9
241000219310 Beta vulgaris subsp. vulgaris Species 0.000 claims description 8
235000021536 Sugar beet Nutrition 0.000 claims description 8
239000000126 substance Substances 0.000 claims description 8
239000006227 byproduct Substances 0.000 claims description 7
235000015191 beet juice Nutrition 0.000 claims description 6
239000000084 colloidal system Substances 0.000 claims description 5
238000011109 contamination Methods 0.000 claims description 2
241000196324 Embryophyta Species 0.000 claims 1
239000007787 solid Substances 0.000 abstract description 11
150000008163 sugars Chemical class 0.000 abstract description 7
229960004793 sucrose Drugs 0.000 description 108
239000002956 ash Substances 0.000 description 23
238000002474 experimental method Methods 0.000 description 14
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
235000008733 Citrus aurantifolia Nutrition 0.000 description 12
101100399296 Mus musculus Lime1 gene Proteins 0.000 description 12
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
235000011941 Tilia x europaea Nutrition 0.000 description 12
239000004571 lime Substances 0.000 description 12
239000012452 mother liquor Substances 0.000 description 12
239000000356 contaminant Substances 0.000 description 10
239000013078 crystal Substances 0.000 description 10
235000016068 Berberis vulgaris Nutrition 0.000 description 9
241000335053 Beta vulgaris Species 0.000 description 9
238000010586 diagram Methods 0.000 description 8
238000004519 manufacturing process Methods 0.000 description 8
239000011148 porous material Substances 0.000 description 7
238000001914 filtration Methods 0.000 description 6
229930091371 Fructose Natural products 0.000 description 5
239000005715 Fructose Substances 0.000 description 5
RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 5
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 5
WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 5
210000001175 cerebrospinal fluid Anatomy 0.000 description 5
238000000855 fermentation Methods 0.000 description 5
230000004151 fermentation Effects 0.000 description 5
239000008103 glucose Substances 0.000 description 5
239000012535 impurity Substances 0.000 description 5
239000002244 precipitate Substances 0.000 description 5
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
241001465754 Metazoa Species 0.000 description 4
238000004458 analytical method Methods 0.000 description 4
238000005352 clarification Methods 0.000 description 4
JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 4
239000000047 product Substances 0.000 description 4
238000003763 carbonization Methods 0.000 description 3
235000013681 dietary sucrose Nutrition 0.000 description 3
238000000605 extraction Methods 0.000 description 3
238000011049 filling Methods 0.000 description 3
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
235000002918 Fraxinus excelsior Nutrition 0.000 description 2
TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
229910000019 calcium carbonate Inorganic materials 0.000 description 2
238000005119 centrifugation Methods 0.000 description 2
238000013375 chromatographic separation Methods 0.000 description 2
238000004042 decolorization Methods 0.000 description 2
238000002845 discoloration Methods 0.000 description 2
238000004128 high performance liquid chromatography Methods 0.000 description 2
239000004310 lactic acid Substances 0.000 description 2
235000014655 lactic acid Nutrition 0.000 description 2
150000007524 organic acids Chemical class 0.000 description 2
235000005985 organic acids Nutrition 0.000 description 2
239000011368 organic material Substances 0.000 description 2
238000011045 prefiltration Methods 0.000 description 2
238000004062 sedimentation Methods 0.000 description 2
238000000926 separation method Methods 0.000 description 2
239000001993 wax Substances 0.000 description 2
-1 35-55 % By weight Chemical compound 0.000 description 1
241000609240 Ambelania acida Species 0.000 description 1
241000283690 Bos taurus Species 0.000 description 1
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
235000006200 Glycyrrhiza glabra Nutrition 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
CZMRCDWAGMRECN-UHFFFAOYSA-N Rohrzucker Natural products OCC1OC(CO)(OC2OC(CO)C(O)C(O)C2O)C(O)C1O CZMRCDWAGMRECN-UHFFFAOYSA-N 0.000 description 1
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
SMNRFWMNPDABKZ-WVALLCKVSA-N [[(2R,3S,4R,5S)-5-(2,6-dioxo-3H-pyridin-3-yl)-3,4-dihydroxyoxolan-2-yl]methoxy-hydroxyphosphoryl] [[[(2R,3S,4S,5R,6R)-4-fluoro-3,5-dihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-hydroxyphosphoryl]oxy-hydroxyphosphoryl] hydrogen phosphate Chemical compound OC[C@H]1O[C@H](OP(O)(=O)OP(O)(=O)OP(O)(=O)OP(O)(=O)OC[C@H]2O[C@H]([C@H](O)[C@@H]2O)C2C=CC(=O)NC2=O)[C@H](O)[C@@H](F)[C@@H]1O SMNRFWMNPDABKZ-WVALLCKVSA-N 0.000 description 1
238000009825 accumulation Methods 0.000 description 1
229910000147 aluminium phosphate Inorganic materials 0.000 description 1
239000010905 bagasse Substances 0.000 description 1
230000009286 beneficial effect Effects 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
230000000903 blocking effect Effects 0.000 description 1
239000011575 calcium Substances 0.000 description 1
229910052791 calcium Inorganic materials 0.000 description 1
BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
239000001506 calcium phosphate Substances 0.000 description 1
229910000389 calcium phosphate Inorganic materials 0.000 description 1
235000011010 calcium phosphates Nutrition 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
239000011248 coating agent Substances 0.000 description 1
238000000576 coating method Methods 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
238000010411 cooking Methods 0.000 description 1
235000021551 crystal sugar Nutrition 0.000 description 1
230000006378 damage Effects 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
238000009792 diffusion process Methods 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
230000005611 electricity Effects 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
230000004907 flux Effects 0.000 description 1
239000000446 fuel Substances 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
239000007788 liquid Substances 0.000 description 1
235000011477 liquorice Nutrition 0.000 description 1
238000011068 loading method Methods 0.000 description 1
229910001629 magnesium chloride Inorganic materials 0.000 description 1
238000002844 melting Methods 0.000 description 1
230000008018 melting Effects 0.000 description 1
238000005374 membrane filtration Methods 0.000 description 1
238000005065 mining Methods 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000005416 organic matter Substances 0.000 description 1
238000010979 pH adjustment Methods 0.000 description 1
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
239000010452 phosphate Substances 0.000 description 1
239000011591 potassium Substances 0.000 description 1
229910052700 potassium Inorganic materials 0.000 description 1
238000001223 reverse osmosis Methods 0.000 description 1
239000011734 sodium Substances 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
239000011780 sodium chloride Substances 0.000 description 1
QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
238000005406 washing Methods 0.000 description 1
239000003643 water by type Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
- C13B30/04—Separating crystals from mother liquor
- C13B30/12—Recycling mother liquor or wash liquors
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/16—Purification of sugar juices by physical means, e.g. osmosis or filtration
- C13B20/165—Purification of sugar juices by physical means, e.g. osmosis or filtration using membranes, e.g. osmosis, ultrafiltration

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Biochemistry (AREA)
Organic Chemistry (AREA)
Sustainable Development (AREA)
Water Supply & Treatment (AREA)
Engineering & Computer Science (AREA)
Crystallography & Structural Chemistry (AREA)
Separation Using Semi-Permeable Membranes (AREA)
Jellies, Jams, And Syrups (AREA)
Saccharide Compounds (AREA)
External Artificial Organs (AREA)
Recrystallisation Techniques (AREA)

DE60006277T 1999-11-17 2000-11-13 Verfahren zur reinigung von minderwertigen zuckersirupen mit nanofiltration Expired - Fee Related DE60006277T2 (de)

Applications Claiming Priority (5)

Application Number	Priority Date	Filing Date	Title
US441988		1999-11-17
US09/441,988 US6355110B1 (en)	1999-11-17	1999-11-17	Process for purification of low grade sugar syrups using nanofiltration
US618234		2000-07-18
US09/618,234 US6406546B1 (en)	1999-11-17	2000-07-18	Process for purification of low grade sugar syrups using nanofiltration
PCT/GB2000/004321 WO2001036690A1 (fr)	1999-11-17	2000-11-13	Procede de purification de sirops de sucre du premier jet par nanofiltration

Publications (2)

Publication Number	Publication Date
DE60006277D1 DE60006277D1 (de)	2003-12-04
DE60006277T2 true DE60006277T2 (de)	2004-07-15

Family

ID=27033027

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DE60006277T Expired - Fee Related DE60006277T2 (de)	1999-11-17	2000-11-13	Verfahren zur reinigung von minderwertigen zuckersirupen mit nanofiltration

Country Status (10)

Country	Link
EP (1)	EP1230401B1 (fr)
AT (1)	ATE253129T1 (fr)
AU (1)	AU1290201A (fr)
BR (1)	BR0015571A (fr)
CA (1)	CA2390860C (fr)
DE (1)	DE60006277T2 (fr)
DK (1)	DK1230401T3 (fr)
MX (1)	MXPA02004621A (fr)
PT (1)	PT1230401E (fr)
WO (1)	WO2001036690A1 (fr)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN104323268A (zh) *	2006-09-19	2015-02-04	视界科技有限公司	从甘蔗中获得的提取物及其生产方法
CN101331924B (zh) *	2007-06-28	2011-01-12	定西市陇海乳品有限责任公司	用生产菊粉的废液制作菊粉糖浆的方法
EP2672832B1 (fr)	2011-02-08	2020-03-25	The Product Makers (Australia) Pty Ltd	Extraits de sucre
US20150201660A1 (en)	2012-08-28	2015-07-23	The Product Makers (Austrilia) Pty Ltd	Extraction Method
WO2015021512A1 (fr)	2013-08-16	2015-02-19	Horizon Science Pty Ltd	Extraits dérivés de canne à sucre et procédés de traitement
EP3318281B1 (fr) *	2016-11-04	2022-12-21	Coriolis Pharma Research GmbH	Sucres et compositions de sucre hautement purifiées
CN117248080A (zh) *	2023-10-08	2023-12-19	安徽金禾实业股份有限公司	一种低聚果糖生产中蔗糖的回收方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
AU635352B2 (en) *	1990-11-09	1993-03-18	Applied Membrane Systems Pty Ltd	A method and apparatus for fractionation of sugar containing solution
FR2701359B1 (fr) *	1993-02-15	1995-05-12	Bretagne Aromes	Procédé pour dénitrifier et déminéraliser, au moins partiellement, un jus de légumes et jus ainsi obtenu.
US6096136A (en) *	1996-10-18	2000-08-01	Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College	Method for producing white sugar
FR2754737B1 (fr) *	1996-10-21	1999-01-15	Tech Sep	Membrane inorganique de nanofiltration et son application dans l'industrie sucriere

2000
- 2000-11-13 AU AU12902/01A patent/AU1290201A/en not_active Abandoned
- 2000-11-13 DE DE60006277T patent/DE60006277T2/de not_active Expired - Fee Related
- 2000-11-13 AT AT00974685T patent/ATE253129T1/de not_active IP Right Cessation
- 2000-11-13 MX MXPA02004621A patent/MXPA02004621A/es active IP Right Grant
- 2000-11-13 BR BR0015571-3A patent/BR0015571A/pt not_active IP Right Cessation
- 2000-11-13 CA CA002390860A patent/CA2390860C/fr not_active Expired - Fee Related
- 2000-11-13 PT PT00974685T patent/PT1230401E/pt unknown
- 2000-11-13 DK DK00974685T patent/DK1230401T3/da active
- 2000-11-13 EP EP00974685A patent/EP1230401B1/fr not_active Expired - Lifetime
- 2000-11-13 WO PCT/GB2000/004321 patent/WO2001036690A1/fr not_active Ceased

Also Published As

Publication number	Publication date
PT1230401E (pt)	2004-03-31
EP1230401A1 (fr)	2002-08-14
ATE253129T1 (de)	2003-11-15
WO2001036690A1 (fr)	2001-05-25
CA2390860C (fr)	2008-10-07
DK1230401T3 (da)	2004-03-01
DE60006277D1 (de)	2003-12-04
BR0015571A (pt)	2002-07-30
MXPA02004621A (es)	2004-09-10
EP1230401B1 (fr)	2003-10-29
AU1290201A (en)	2001-05-30
CA2390860A1 (fr)	2001-05-25

Legal Events

Date	Code	Title	Description
2004-11-25	8364	No opposition during term of opposition
2010-09-16	8339	Ceased/non-payment of the annual fee

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CH630327A5 (de)	1982-06-15	Verfahren zur herstellung von xylit.
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WO2001014595A2 (fr)	2001-03-01	Procede pour filtrer sur membrane de la canne a sucre
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