DE69919599D1 - Verfahren zur herstellung von 4-trifluormethylsulfinylpyrazolderivat - Google Patents

Verfahren zur herstellung von 4-trifluormethylsulfinylpyrazolderivat

Info

Publication number
DE69919599D1
DE69919599D1 DE69919599T DE69919599T DE69919599D1 DE 69919599 D1 DE69919599 D1 DE 69919599D1 DE 69919599 T DE69919599 T DE 69919599T DE 69919599 T DE69919599 T DE 69919599T DE 69919599 D1 DE69919599 D1 DE 69919599D1
Authority
DE
Germany
Prior art keywords
sub
compound
formula
trifluormethylsulfinylpyrazole
derivative
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69919599T
Other languages
English (en)
Other versions
DE69919599T2 (de
Inventor
Jean-Louis Clavel
Isabelle Pelta
Bars Sylvie Le
Philippe Charreau
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF Agro BV Arnhem NL Zweigniederlassung Freienbach
Original Assignee
Bayer CropScience SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=8167491&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69919599(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Bayer CropScience SA filed Critical Bayer CropScience SA
Application granted granted Critical
Publication of DE69919599D1 publication Critical patent/DE69919599D1/de
Publication of DE69919599T2 publication Critical patent/DE69919599T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/04—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
DE69919599T 1999-10-22 1999-10-22 Verfahren zur herstellung von 4-trifluormethylsulfinylpyrazolderivat Expired - Lifetime DE69919599T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/EP1999/008687 WO2001030760A1 (en) 1999-10-22 1999-10-22 Process for preparing 4-trifluoromethylsulphinylpyrazole derivative

Publications (2)

Publication Number Publication Date
DE69919599D1 true DE69919599D1 (de) 2004-09-23
DE69919599T2 DE69919599T2 (de) 2005-08-11

Family

ID=8167491

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69919599T Expired - Lifetime DE69919599T2 (de) 1999-10-22 1999-10-22 Verfahren zur herstellung von 4-trifluormethylsulfinylpyrazolderivat

Country Status (30)

Country Link
US (2) US6620943B1 (de)
EP (1) EP1222173B1 (de)
JP (1) JP4666863B2 (de)
KR (2) KR100665599B1 (de)
CN (3) CN101445483B (de)
AT (1) ATE273961T1 (de)
AU (1) AU783139B2 (de)
BG (1) BG65483B1 (de)
BR (1) BR9917518B1 (de)
CA (1) CA2384283C (de)
CZ (1) CZ299822B6 (de)
DE (1) DE69919599T2 (de)
DK (1) DK1222173T3 (de)
EA (1) EA005077B1 (de)
ES (1) ES2222743T3 (de)
HR (1) HRP20020438B1 (de)
HU (1) HU229393B1 (de)
IL (2) IL149152A0 (de)
IN (2) IN2005MU00818A (de)
ME (1) MEP7808A (de)
MX (1) MX229662B (de)
NZ (2) NZ517770A (de)
PL (1) PL206482B1 (de)
PT (1) PT1222173E (de)
RO (1) RO121209B1 (de)
TR (2) TR200201072T2 (de)
TW (1) TW553936B (de)
UA (1) UA73752C2 (de)
WO (1) WO2001030760A1 (de)
ZA (1) ZA200201961B (de)

Families Citing this family (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1197492B1 (de) 1999-06-29 2007-09-05 Nihon Nohyaku Co., Ltd. Pyrazolderivate und verfahren zu ihrer herstellung und pestizide die diese als aktive inhaltsstoffe enthalten
WO2005023774A1 (en) * 2003-09-11 2005-03-17 Cheminova A/S Process for the preparation of a trifluoromethylthioether
CN100586934C (zh) * 2003-11-07 2010-02-03 凯米诺瓦有限公司 制备三氟甲基硫醚的方法
DE102004020069C5 (de) 2004-04-24 2013-12-05 Voith Patent Gmbh Verfahren zum Satinieren einer Papierbahn
AU2013203228B2 (en) * 2005-12-14 2015-08-27 Makhteshim Chemical Works Ltd Polymorphs and amorphous forms of 5-amino-1-[2,6- dichloro-4-(trifluoromethyl)phenyl]-4- [(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile
US8440709B2 (en) * 2005-12-14 2013-05-14 Makhteshim Chemical Works Ltd. Polymorphs and amorphous forms of 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile
AU2006342749B2 (en) 2006-04-25 2011-08-25 Gharda Chemicals Limited Process for the preparation of fipronil, an insecticide, and related pyrazoles
CN101168529B (zh) * 2006-10-24 2011-03-23 温州大学 氟虫腈、乙虫腈及其衍生物的合成方法
CA2667562A1 (en) 2006-11-10 2008-05-15 Basf Se Process for the sulfinylation of a pyrazole derivative
EP2083627A1 (de) * 2006-11-10 2009-08-05 Basf Se Kristalline fipronil-modifikation
EP2083628A1 (de) * 2006-11-10 2009-08-05 Basf Se Kristalline fipronil-modifikation
EP2083629B2 (de) * 2006-11-10 2014-11-26 Basf Se Kristallmodifikation von fipronil
BRPI0718774A2 (pt) 2006-11-10 2013-12-03 Basf Se "processo para a sulfinilação de um derivado de pirazol, 5-amino-1-[2,6-dicloro-4-(trifluorometil) fenil] -4-(trifluorometilsulfinil) -pirazol-3-carbonitrila, composição pesticida ou parasiticida, uso, métodos para o controle de insetos, acarídeos ou nematódeos, de proteger plantas em crescimento, para tratar, controlar, prevenir ou proteger animais, e, processo para a preparação de uma composição."
UA110598C2 (uk) * 2006-11-10 2016-01-25 Басф Се Спосіб одержання кристалічної модифікації фіпронілу
US8354007B2 (en) 2008-10-02 2013-01-15 Basf Se Method for producing and purifying trifluoromethanesulfinic acid
WO2010049746A1 (en) * 2008-10-27 2010-05-06 Dynamit Nobel Gmbh Explosivstoff-Und Systemtechnic Process for the synthesis of fipronil
US8476459B2 (en) 2009-10-30 2013-07-02 Basf Se Process for the preparation of 4-sulfinyl-pyrazole derivatives
AU2010100462A4 (en) 2010-03-03 2010-06-17 Keki Hormusji Gharda A process for the synthesis of Fipronil
IT1400666B1 (it) 2010-07-07 2013-06-28 Finchimica Srl Procedimento per la sintesi di 5-amino, 1-fenil, 3-ciano, 4-trifluorometil sulfinil pirazoli.
US20130197238A1 (en) 2010-07-12 2013-08-01 Irvita Plant Protection, A Branch Of Celsius Property B.V Fipronil production process
EP2663192A4 (de) * 2011-01-14 2015-06-03 Keki Hormusji Gharda Polymorphismen in 5-amino-1-(2,6-dichlor-4-trifluormethylphenyl-)3-cyan-4-trifluor-methyl-sulfinyl-pyrazol
WO2012164571A1 (en) 2011-05-30 2012-12-06 Keki Hormusji Gharda Process for synthesis of fipronil
CN102633722B (zh) * 2012-03-20 2015-05-06 金坛市凌云动物保健品有限公司 一种非泼罗尼的制备方法
TWI579274B (zh) 2012-04-20 2017-04-21 龍馬躍公司 製備１－芳基－５－烷基吡唑化合物的改良方法
CN102690232A (zh) * 2012-05-30 2012-09-26 河南中医学院 一种氟虫腈中间体的合成方法
US9049860B2 (en) 2013-04-17 2015-06-09 The Hartz Mountain Corporation Ectoparasiticidal methods
CN105254565A (zh) * 2015-09-30 2016-01-20 乐平市康鑫医药化工有限公司 由氰基吡唑一锅法合成硫醚的工艺方法
CN106977460A (zh) * 2017-04-19 2017-07-25 江苏托球农化股份有限公司 1‑(2,6‑二氯‑4‑三氟甲基)苯基‑3‑氰基‑4‑乙巯基‑5‑氨基吡唑的合成
EP3412658A1 (de) 2017-06-09 2018-12-12 Solvay Sa Prozesse für die herstellung von sulfur-substituierten pyrazole-derivaten
EP3412659A1 (de) 2017-06-09 2018-12-12 Solvay Sa Verfahren zur herstellung von schwefel-substituierte pyrazolederivate
CN112430213A (zh) * 2020-12-03 2021-03-02 江苏优普生物化学科技股份有限公司 一种三氟甲硫基吡唑合成工艺
CN113149909B (zh) * 2021-03-24 2022-04-19 台州达辰药业有限公司 5-氨基-3-氰基-1-(2,6-二氯-4-三氟甲基-苯基)吡唑二硫化物制备方法
CN113480482B (zh) * 2021-07-05 2022-11-18 海正药业南通有限公司 一种非泼罗尼中间体的合成方法
CN114213330A (zh) * 2021-12-29 2022-03-22 天和药业股份有限公司 一种氟虫腈精制母液的处理方法
CN121293157A (zh) * 2025-12-11 2026-01-09 长青(湖北)生物科技有限公司 一种制备氟虫腈及其中间体的工艺

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2716453B1 (fr) * 1994-02-22 1996-03-29 Rhone Poulenc Agrochimie Procédé de sulfinylation de composés hétérocycliques.
DE3602728A1 (de) * 1985-05-17 1986-11-20 Bayer Ag, 51373 Leverkusen Schaedlingsbekaempfungsmittel auf basis von pyrazolderivaten
GB8713768D0 (en) * 1987-06-12 1987-07-15 May & Baker Ltd Compositions of matter
US5232940A (en) 1985-12-20 1993-08-03 Hatton Leslie R Derivatives of N-phenylpyrazoles
US5547974A (en) * 1985-12-20 1996-08-20 Rhone-Poulenc Agriculture Ltd. Derivatives of N-phenylpyrazoles
CA2004776C (fr) 1988-12-13 2000-04-25 Claude Wakselman Procede de preparation de perfluoroalkylthioethers

Also Published As

Publication number Publication date
PL206482B1 (pl) 2010-08-31
KR100665598B1 (ko) 2007-01-10
HU229393B1 (en) 2013-11-28
CA2384283C (en) 2009-02-03
EA005077B1 (ru) 2004-10-28
KR100665599B1 (ko) 2007-01-10
DK1222173T3 (da) 2004-09-20
MX229662B (es) 2005-08-04
CA2384283A1 (en) 2001-05-03
KR20060097747A (ko) 2006-09-14
KR20020040899A (ko) 2002-05-30
CN1896066B (zh) 2011-06-15
CN1896066A (zh) 2007-01-17
ES2222743T3 (es) 2005-02-01
HRP20020438A2 (en) 2004-08-31
EA200200481A1 (ru) 2002-10-31
MXPA02003944A (es) 2003-10-15
US6620943B1 (en) 2003-09-16
WO2001030760A1 (en) 2001-05-03
CN101445483B (zh) 2011-03-30
EP1222173A1 (de) 2002-07-17
BR9917518A (pt) 2002-06-18
RO121209B1 (ro) 2007-01-30
IL149152A (en) 2008-08-07
HUP0203206A2 (hu) 2003-03-28
CN1332730A (zh) 2002-01-23
AU783139B2 (en) 2005-09-29
AU1270700A (en) 2001-05-08
IL149152A0 (en) 2002-11-10
CN101445483A (zh) 2009-06-03
IN2005MU00818A (de) 2005-11-11
DE69919599T2 (de) 2005-08-11
CN1163488C (zh) 2004-08-25
PT1222173E (pt) 2004-11-30
BG65483B1 (bg) 2008-09-30
JP4666863B2 (ja) 2011-04-06
NZ517770A (en) 2003-11-28
PL354611A1 (en) 2004-02-09
TW553936B (en) 2003-09-21
ZA200201961B (en) 2003-05-28
NZ527896A (en) 2004-07-30
HRP20020438B1 (en) 2011-01-31
IN192712B (de) 2004-05-15
JP2003512456A (ja) 2003-04-02
BR9917518B1 (pt) 2009-08-11
MEP7808A (en) 2010-06-10
EP1222173B1 (de) 2004-08-18
US6881848B2 (en) 2005-04-19
TR200202806T2 (tr) 2003-03-21
CZ20021384A3 (cs) 2002-08-14
HUP0203206A3 (en) 2005-11-28
BG106622A (en) 2002-12-29
TR200201072T2 (tr) 2002-07-22
CZ299822B6 (cs) 2008-12-03
US20040034234A1 (en) 2004-02-19
IN2002MU00312A (de) 2007-06-29
ATE273961T1 (de) 2004-09-15
UA73752C2 (en) 2005-09-15

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Legal Events

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8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: BASF ARGO B.V., ARNHEM (NL)-WAEDENSWIL-BRANCH,, CH