DK0442621T3 - Fremgangsmåde til fremstilling af tetrahydroisoalfa- og hexahydroisoalfasyrer - Google Patents

Fremgangsmåde til fremstilling af tetrahydroisoalfa- og hexahydroisoalfasyrer

Info

Publication number
DK0442621T3
DK0442621T3 DK91300480.0T DK91300480T DK0442621T3 DK 0442621 T3 DK0442621 T3 DK 0442621T3 DK 91300480 T DK91300480 T DK 91300480T DK 0442621 T3 DK0442621 T3 DK 0442621T3
Authority
DK
Denmark
Prior art keywords
acids
mixture
hhiaa
thiaa
exposing
Prior art date
Application number
DK91300480.0T
Other languages
English (en)
Inventor
Bruce Allan Hay
Original Assignee
Pfizer
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pfizer filed Critical Pfizer
Application granted granted Critical
Publication of DK0442621T3 publication Critical patent/DK0442621T3/da

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C5/00—Other raw materials for the preparation of beer
    • C12C5/02—Additives for beer
    • C12C5/026—Beer flavouring preparations
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C3/00—Treatment of hops
    • C12C3/04—Conserving; Storing; Packing
    • C12C3/08—Solvent extracts from hops
    • C12C3/10—Solvent extracts from hops using carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C3/00—Treatment of hops
    • C12C3/12—Isomerised products from hops
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C9/00—Methods specially adapted for the making of beerwort
    • C12C9/02—Beerwort treatment; Boiling with hops; Hop extraction
    • C12C9/025—Preparation of hop extracts; Isomerisation of these extracts; Treatment of beerwort with these extracts; Surrogates of the hop

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Food Science & Technology (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Fats And Perfumes (AREA)
  • Seasonings (AREA)
  • Heterocyclic Compounds Containing Sulfur Atoms (AREA)
DK91300480.0T 1990-01-31 1991-01-22 Fremgangsmåde til fremstilling af tetrahydroisoalfa- og hexahydroisoalfasyrer DK0442621T3 (da)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/473,268 US5013571A (en) 1990-01-31 1990-01-31 Methods for making tetrahydroisoalpha and hexahydroisoalpha acids

Publications (1)

Publication Number Publication Date
DK0442621T3 true DK0442621T3 (da) 1996-06-03

Family

ID=23878861

Family Applications (1)

Application Number Title Priority Date Filing Date
DK91300480.0T DK0442621T3 (da) 1990-01-31 1991-01-22 Fremgangsmåde til fremstilling af tetrahydroisoalfa- og hexahydroisoalfasyrer

Country Status (11)

Country Link
US (1) US5013571A (da)
EP (1) EP0442621B1 (da)
JP (2) JPH0737414B2 (da)
AT (1) ATE138097T1 (da)
DE (1) DE69119442T2 (da)
DK (1) DK0442621T3 (da)
ES (1) ES2087239T3 (da)
GR (1) GR3020279T3 (da)
IE (1) IE73636B1 (da)
MX (1) MX169175B (da)
PT (1) PT96589B (da)

Families Citing this family (61)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2113274C (en) * 1991-07-15 2001-01-02 Robert J. Smith Hops-derived foam stability and bittering agents isomerized-.alpha.-acids
US5200227A (en) * 1992-05-11 1993-04-06 Kalamazoo Holdings, Inc. Stable aqueous solutions of tetrahydro and hexahydro iso-alpha acids
EP0672107B1 (en) * 1992-06-04 1998-09-09 S.S. Steiner, Inc. Production of isomerized hop extract
US5370863A (en) * 1992-12-16 1994-12-06 Miller Brewing Company Oral care compositions containing hop acids and method
US5296637A (en) * 1992-12-31 1994-03-22 Kalamazoo Holdings, Inc. Production of odor-free tetrahydroisohumulates from alpha acids via their tetrahydrohumulates and subsequent isomerization
CN1035993C (zh) * 1994-01-15 1997-10-01 沈阳佳源国际医疗科技有限公司 由酒花浸膏制备四氢异葎草酮的方法
US5583262A (en) * 1994-11-10 1996-12-10 Maye; John P. Solid salts of hop acids
US5523489A (en) * 1995-02-07 1996-06-04 Miller Brewing Company Preparation of tetrahydroisohumulones
US5600012A (en) * 1995-04-06 1997-02-04 John I. Haas, Inc. Process for producing tetrahydroisoalpha acids
US6020019A (en) * 1996-03-26 2000-02-01 Miller Brewing Company Hydrogenation of hop soft resins using CO2
DE19620171A1 (de) * 1996-05-20 1997-11-27 Nigu Chemie Gmbh Verfahren zur katalytischen Hydrierung von Terpenoiden
US5965777A (en) * 1996-10-29 1999-10-12 Cultor Food Service, Inc. Process to remove catalyst poisons from hop extracts
US5767319A (en) * 1996-10-30 1998-06-16 Miller Brewing Company Preparation of tetrahydroiso-α-acids by the hydrogenation of the metal salts of iso-α-acids
US5874633A (en) * 1996-10-30 1999-02-23 Miller Brewing Company Concentrated single phase aqueous solutions of tetrahydroiso-α-acids and methods of preparing the same
CN1058699C (zh) * 1998-10-06 2000-11-22 新疆大学 以酒花浸膏为原料制备四氢异α酸的方法
US6198004B1 (en) 1999-06-10 2001-03-06 Haas Hop Products, Inc. Process for hydrogenation of isoalpha acids
US6303824B1 (en) * 1999-11-11 2001-10-16 Miller Brewing Company Method of hydrogenating iso-α acids in a buffered solution
DE69940361D1 (de) * 1999-11-18 2009-03-12 Steiner Inc S S Verfahren zur Hydrierung von Hopfenharzsäuren
US6583322B1 (en) 2000-02-25 2003-06-24 Kalamazoo Holdings, Inc. Dihydro and hexahydro isoalpha acids having a high ratio of trans to cis isomers, production thereof, and products containing the same
US20060193960A1 (en) * 2000-06-30 2006-08-31 Wilson Richard J Improvements to the bittering of beer
BR0110965A (pt) 2000-06-30 2003-06-03 Steiner Inc S S Aperfeiçoamentos no amargor da cerveja
US8142819B2 (en) * 2002-10-21 2012-03-27 Metaproteomics, Llc Synergistic compositions that treat or inhibit pathological conditions associated with inflammatory response
US7901713B2 (en) * 2001-06-20 2011-03-08 Metaproteomics, Llc Inhibition of COX-2 and/or 5-LOX activity by fractions isolated or derived from hops
US7270835B2 (en) * 2001-06-20 2007-09-18 Metaproteomics, Llc Compositions that treat or inhibit pathological conditions associated with inflammatory response
US7901714B2 (en) * 2001-06-20 2011-03-08 Metaproteomics, Llp Treatment modalities for autoimmune diseases
US8206753B2 (en) * 2001-06-20 2012-06-26 Metaproteomics, Llc Anti-inflammatory botanical products for the treatment of metabolic syndrome and diabetes
US7718198B2 (en) * 2001-06-20 2010-05-18 Metaproteomics, Llc Treatment modalities for autoimmune diseases
US20040219240A1 (en) * 2001-06-20 2004-11-04 Babish John G. Anti-inflammatory pharmaceutical compositions for reducing inflammation and the treatment or prevention of gastric toxicity
US7205151B2 (en) * 2001-06-20 2007-04-17 Metaproteomics, Llc Complex mixtures exhibiting selective inhibition of cyclooxygenase-2
US8168234B2 (en) * 2001-06-20 2012-05-01 Metaproteomics, Llc Compositions that treat or inhibit pathological conditions associated with inflammatory response
US20040115290A1 (en) * 2001-06-20 2004-06-17 Tripp Matthew L. Modulation of inflammation by hops fractions and derivatives
US7815944B2 (en) * 2001-06-20 2010-10-19 Metaproteomics, Llc Anti-inflammatory pharmaceutical compositions for reducing inflammation and the treatment of prevention of gastric toxicity
US20090263522A1 (en) * 2001-10-26 2009-10-22 Babish John G Curcuminoid Compositions Exhibiting Synergistic Inhibition Of The Expression And/Or Activity Of Cyclooxygenase-2
US7279185B2 (en) 2001-10-26 2007-10-09 Metaproteonics, Llc Curcuminoid compositions exhibiting synergistic inhibition of the expression and/or activity of cyclooxygenase-2
US8158160B2 (en) 2001-11-13 2012-04-17 Eric Hauser Kuhrts Anti-inflammatory cyclooxygenase inhibitors
US20060233902A1 (en) * 2002-02-14 2006-10-19 Kirin Beer Kabushiki Kaisha Compositions and foods for improving lipid metabolism
US7258887B2 (en) * 2002-03-26 2007-08-21 Miller Brewing Company Preparation of light stable hops
US7413758B2 (en) * 2002-03-26 2008-08-19 Millercoors Llc Preparation of light stable hop products
KR20050071605A (ko) * 2002-10-21 2005-07-07 메타프로테오믹스, 엘엘씨 염증반응과 관련된 병리학적 상태를 치료하거나 저해하는조성물
GB0306568D0 (en) * 2003-03-21 2003-04-30 Unilever Plc Compositions of natural products and use thereof
WO2005039483A2 (en) * 2003-05-22 2005-05-06 Metaproteomics, Llc Anti-inflammatory pharmaceutical compositions for reducing inflammation and the treatment or prevention of gastric toxicity
US7914831B2 (en) 2004-02-27 2011-03-29 Metaproteomics, Llc Synergistic anti-inflammatory pharmaceutical compositions and related methods using curcuminoids or methylxanthines
US20050192356A1 (en) * 2004-02-27 2005-09-01 Babish John G. Synergistic anti-inflammatory pharmaceutical compositions and methods of use
WO2006053249A2 (en) * 2004-11-13 2006-05-18 Metaproteomics, Llc Compositions exhibiting inhibition of cyclooxygenase-2
EP2248532A1 (en) * 2005-08-09 2010-11-10 Metaproteomics, LLP Protein kinase modulation by hops and acacia products cross-reference to related applications
NZ568860A (en) * 2005-12-09 2012-09-28 Metaproteomics Llc Protein kinase modulation by hops and acacia products
US20080051466A1 (en) * 2006-06-20 2008-02-28 Metaproteomics, Llc Isoalpha acid based protein kinase modulation cancer treatment
US20080033057A1 (en) * 2006-06-20 2008-02-07 Metaproteomics, Llc Hexahydro-isoalpha acid based protein kinase modulation cancer treatment
CN1966638B (zh) * 2006-11-11 2011-04-20 玉门拓璞科技开发有限责任公司 异构化二氧化碳酒花浸膏的生产方法
JP2010522190A (ja) * 2007-03-19 2010-07-01 メタプロテオミクス， エルエルシー 骨及び関節の健康を助成するための方法と組成物
US8241674B2 (en) * 2007-05-11 2012-08-14 Metaproteomics, Llc Methods and compositions for heavy metal detoxification
AU2008335156A1 (en) * 2007-12-10 2009-06-18 Metaproteomics, Llc Substituted 1,3-cyclopentadione multi-target protein kinase modulators of cancer, angiogenesis and the inflammatory pathways associated therewith
JP2011516492A (ja) * 2008-04-02 2011-05-26 メタプロテオミクス， エルエルシー 内皮炎症及び内皮−単球相互作用の置換１，３−シクロペンタジオンによる減弱
US20110117252A1 (en) 2009-11-13 2011-05-19 Kalamazoo Holdings, Inc. Process for the preparation of tetrahydroisohumulone compositions
HUE055712T2 (hu) * 2010-05-21 2021-12-28 Coors Brewing Co Hop savak és származékaik elõállítása
GB201009873D0 (en) * 2010-06-14 2010-07-21 Univ Leuven Kath Method for hydrogenation of isoalpha-acids (isohumulones) to hexahydro-iso-alpha-acids (hexahydro-isohumulones) by using heterogeneous ruthenium
GB201016430D0 (en) 2010-09-30 2010-11-17 Univ Leuven Kath Improved method for isomerisation of hop alpha-acids to iso-alpha-acids
US9222064B1 (en) 2014-08-18 2015-12-29 Hop Ting Resources, LLC Solvent-free processes for making light stable ISO-alpha-acids derivatives from both hop alpha-acids and beta-acids resins
CN110951559A (zh) * 2019-12-31 2020-04-03 齐鲁工业大学 一种通过添加四氢或六氢异构酒花浸膏提高啤酒泡沫性能的方法
GB202400585D0 (en) 2024-01-16 2024-02-28 Greenhouse Gmbh & Co Kg Natural foam enhancer
WO2026009596A1 (ja) * 2024-07-05 2026-01-08 三菱瓦斯化学株式会社 アルデヒドの製造方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3044879A (en) * 1959-02-11 1962-07-17 Miller Brewing Anactinic malt product and hop extract therefor
GB1145240A (en) * 1965-03-01 1969-03-12 Kalamazoo Spice Extract Co Hop flavours for malt beverages and the like
US4002683A (en) * 1971-05-03 1977-01-11 Kalsec, Inc. Process for isomerizing alpha acids to iso-alpha acids
US4123561A (en) * 1977-02-01 1978-10-31 S.S. Steiner, Inc. Method for processing hops for brewing
US4590296A (en) * 1984-01-25 1986-05-20 Miller Brewing Company Process for separation of beta-acids from extract containing alpha-acids and beta-acids
US4644084A (en) * 1984-01-25 1987-02-17 Miller Brewing Company Preparation of tetrahydroisohumulones
US4767640A (en) * 1985-10-29 1988-08-30 Miller Brewing Company Light stable hop extracts and method of preparation

Also Published As

Publication number Publication date
MX169175B (es) 1993-06-23
GR3020279T3 (en) 1996-09-30
ATE138097T1 (de) 1996-06-15
ES2087239T3 (es) 1996-07-16
IE73636B1 (en) 1997-06-18
JPH05148178A (ja) 1993-06-15
EP0442621B1 (en) 1996-05-15
PT96589B (pt) 1998-08-31
US5013571A (en) 1991-05-07
DE69119442T2 (de) 1996-09-26
JPH0737414B2 (ja) 1995-04-26
DE69119442D1 (de) 1996-06-20
PT96589A (pt) 1991-10-15
JPH0769965A (ja) 1995-03-14
IE910312A1 (en) 1991-07-31
EP0442621A1 (en) 1991-08-21
JP2525133B2 (ja) 1996-08-14

Similar Documents

Publication Publication Date Title
ES2087239T3 (es) Procedimientos para preparar acidos tetrahidroisoalfa y hexahidroisoalfa.
DE69217564D1 (de) Verfahren zur Herstellung von Additionspolymersiationskatalysatoren via Metalzentraoxidation
DK0576231T3 (da) Proces til fremstilling af alfa-anomerberigede 1-halogen-2-deoxy-2, 2-difluor-D-ribofuranosylderivater
ATE326477T1 (de) Synthese von 9-deoxo-9a-aza 11,12-deoxy-9a-methyl-9a-homoerythromycin a 11,12-hydrogenorthoborat- dihydrat
DK32684A (da) Fremgangsmaade til fremstilling af 26,26,26,27,27,27-hexafluor-1alfa,25-dihydroxycholesterol og mellemprodukter til brug herfor
DE3668621D1 (de) Verfahren zur herstellung von pteridinderivaten.
ATE116636T1 (de) Verfahren zur herstellung von 2,6- dichlordiphenylaminessigsäurederivaten.
ATE69795T1 (de) Verfahren zur herstellung von ethylenischen carbonylverbindungen.
DE3855002D1 (de) Verfahren zur Herstellung von Dodecahydro-3a,6,6,9a-tetramethylnaphto(2,1-b)furan
NO921439L (no) Fremgangsmaate for fremstilling av glyoksylsyre ved enzymatisk oksidasjon av glykolsyre
BG104302A (en) Method for preparing substituted 4-phenyl-4-cyanocyclohexanoic acids
IT1058547B (it) Procedimento di ciclizzazione del deidrolinalolo e prodotti ottenuti con tale procedimento
JPS529757A (en) Clamping method of bolt and its washer
ES2022348B3 (es) Preparacion de diamino-y dialquilaminobencenodioles.
JPS51136615A (en) Process for preparation of methacrylic acid
DE69503106D1 (de) Verfahren zur Herstellung von L-Ascorbinsäure
Ono et al. A NEW METHOD FOR REGIOSELECTIVE α-MONO-OR α, α-DI-DEUTERATION OF CARBONYL COMPOUNDS
DK0535448T3 (da) Fremgangsmåde og mellemprodukter til fremstilling af et antiviralt middel indeholdende en cyclobutylgruppe
JPS5210250A (en) Preparations of cholesta-5,23,24-triene- 3beta -ols
SU590261A1 (ru) Способ очистки природных вод от органических соединений
DE58901557D1 (de) Verfahren zur herstellung von 1,2-disulfon-verbindungen.
ATE126214T1 (de) Verfahren zur selektiven mono-ortho- hydroxyalkylierung von 4-substituierten pyridin- derivaten.
DK10082A (da) Fremgangsmaade til fremstilling af 4-aminobutyramid
ES2018712B3 (es) Acido acrilaminoglicolico cristalizado puro anhidro y su procedimiento de preparacion.
JPS53101302A (en) Purification of organocyamic compounds