DK0448413T3 - Selektiv 6-acylering af saccharose medieret af cycliske addukter af dialkyltinoxider og dioler - Google Patents

Selektiv 6-acylering af saccharose medieret af cycliske addukter af dialkyltinoxider og dioler

Info

Publication number: DK0448413T3
Authority: DK; Denmark
Prior art keywords: acylation; diols; selective; dialkyltin oxides; cyclic adducts
Prior art date: 1990-03-23

Application number

DK91302546.6T

Other languages

Danish (da)

English (en)

Inventor

Robert E Walkup

Nicholas M Vernon

Robert E Wingard Jr

Original Assignee

Noramco Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1990-03-23

Filing date

1991-03-22

Publication date

1995-07-10

1991-03-22 Application filed by Noramco Inc filed Critical Noramco Inc

1995-07-10 Application granted granted Critical

1995-07-10 Publication of DK0448413T3 publication Critical patent/DK0448413T3/da

Links

CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 title 1
229930006000 Sucrose Natural products 0.000 title 1
238000005917 acylation reaction Methods 0.000 title 1
125000004122 cyclic group Chemical group 0.000 title 1
150000002009 diols Chemical class 0.000 title 1
230000001404 mediated effect Effects 0.000 title 1
239000005720 sucrose Substances 0.000 title 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/22—Tin compounds
- C07F7/2224—Compounds having one or more tin-oxygen linkages
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C07H13/06—Fatty acids
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H23/00—Compounds containing boron, silicon or a metal, e.g. chelates or vitamin B12

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Health & Medical Sciences (AREA)
Biochemistry (AREA)
Biotechnology (AREA)
General Health & Medical Sciences (AREA)
Genetics & Genomics (AREA)
Molecular Biology (AREA)
Life Sciences & Earth Sciences (AREA)
Saccharide Compounds (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Fats And Perfumes (AREA)
Catalysts (AREA)

DK91302546.6T 1990-03-23 1991-03-22 Selektiv 6-acylering af saccharose medieret af cycliske addukter af dialkyltinoxider og dioler DK0448413T3 (da)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US07/499,731 US5089608A (en)	1990-03-23	1990-03-23	Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols

Publications (1)

Publication Number	Publication Date
DK0448413T3 true DK0448413T3 (da)	1995-07-10

Family

ID=23986463

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DK91302546.6T DK0448413T3 (da)	1990-03-23	1991-03-22	Selektiv 6-acylering af saccharose medieret af cycliske addukter af dialkyltinoxider og dioler

Country Status (10)

Country	Link
US (1)	US5089608A (de)
EP (1)	EP0448413B1 (de)
JP (1)	JP3064462B2 (de)
CA (1)	CA2038740C (de)
DE (1)	DE69109719T2 (de)
DK (1)	DK0448413T3 (de)
ES (1)	ES2072541T3 (de)
GR (1)	GR910100124A (de)
IE (1)	IE66892B1 (de)
PT (1)	PT97115B (de)

Families Citing this family (38)

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US5034551A (en) *	1990-04-23	1991-07-23	Noramco, Inc.	Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds
US5298611A (en) *	1993-03-12	1994-03-29	Mcneil-Ppc, Inc.	Sucralose pentaester production
US6608039B1 (en)	1994-07-11	2003-08-19	The United States Of America As Represented By The Secretary Of Agriculture	Chemically synthesized sugar esters for the control of soft-bodied arthropods
IL114551A0 (en)	1994-07-11	1995-11-27	Us Agriculture	Chemically synthesized sugar esters for the control of soft bodied arthropods
US5498709A (en)	1994-10-17	1996-03-12	Mcneil-Ppc, Inc.	Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
DK0776903T3 (da) *	1995-11-28	2003-05-12	Mcneil Ppc Inc	Fremgangsmåde til fremstilling af en saccharose-6-ester
US6121430A (en) *	1998-12-28	2000-09-19	University Of Iowa Research Foundation	Regiospecific synthesis of glucose-based surfactants
US20090105470A1 (en) *	2005-02-22	2009-04-23	Pharmed Medicare Private Limited , A Corporation	Tin Mediated Regioselective Synthesis of Sucrose-6-Esters
US20060276639A1 (en) *	2005-06-01	2006-12-07	Healthy Brands, Llc	Conversion of sucralose-6-ester to sucralose
CN100418976C (zh) *	2006-04-03	2008-09-17	广州科宏食品添加物有限公司	一种三氯蔗糖的制备方法
US8143432B2 (en)	2006-11-17	2012-03-27	Janssen Pharmaceutica N.V.	Process for regioselective mono-tosylation of diols
GB0702854D0 (en) *	2007-01-09	2007-03-28	Tate & Lyle Plc	Method for the synthesis of sucrose-6-esters
GB0702857D0 (en) *	2007-01-19	2007-03-28	Tate & Lyle Plc	Improved sucralose production method
US20080227971A1 (en) *	2007-01-19	2008-09-18	Leinhos Duane A	Deacylation of sucralose-6-acylates
CN100420695C (zh) *	2007-02-02	2008-09-24	上海迪赛诺医药发展有限公司	制备三氯蔗糖的方法
US20090076261A1 (en) *	2007-09-13	2009-03-19	Polymed Therapeutics, Inc.	Novel process for preparing sucrose-6-esters
AR070082A1 (es) *	2008-01-04	2010-03-10	Tate & Lyle Technology Ltd	Metodo para la produccion de sucralosa
US8557976B2 (en) *	2008-03-13	2013-10-15	Tate & Lyle Technology Limited	Microbial consortia and methods for their use
CN101977664B (zh) *	2008-03-20	2014-02-26	塔特和莱利技术有限公司	从叔酰胺溶剂中去除酸
US8436157B2 (en) *	2008-03-26	2013-05-07	Tate & Lyle Technology Limited	Method for the production of sucralose
US8497367B2 (en) *	2008-04-03	2013-07-30	Tate & Lyle Technology Limited	Sucralose purification process
WO2009137193A2 (en) *	2008-04-03	2009-11-12	Tate & Lyte Technology Ltd	Effect of carbohydrate concentration on sucralose extraction efficiency
AR071134A1 (es) *	2008-04-03	2010-05-26	Tate & Lyle Technology Ltd	Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
US20090299055A1 (en) *	2008-04-03	2009-12-03	Tate & Lyle Technology Limited	Purification of Sucralose Containing Feed Streams for Sucralose Crystallization
US20090259036A1 (en) *	2008-04-03	2009-10-15	Tate & Lyle Technology Limited	Extraction of less polar impurities from sucralose containing aqueous feed streams
GB2469157B (en)	2009-03-30	2011-07-06	John Kerr	Process for removing dimethylamine during sucralose production
GB2469158B (en)	2009-03-31	2011-09-28	Peter J Seaberg	Base-assisted formation of tin-sucrose adducts
GB2471348B (en)	2009-06-22	2011-12-14	Tate & Lyle Technology Ltd	A method for producing sucralose-6-acylate
GB2474310B (en)	2009-10-12	2012-02-29	Tate & Lyle Technology Ltd	Process for the production of sucrose-6-ester
GB2474311B (en)	2009-10-12	2012-10-17	Tate & Lyle Technology Ltd	Low temperature, single solvent process for the production of sucrose-6-ester
GB201110520D0 (en)	2011-05-10	2011-08-03	Tate & Lyle Technology Ltd	Extraction of carboxylic acids with tin compounds
CN102796145B (zh) *	2012-06-19	2015-04-15	天津北方食品有限公司	一种蔗糖-6-苯甲酸酯的制备方法
CN105829332B (zh)	2013-12-16	2018-10-02	塔特和莱利技术有限公司	蔗糖-6-酯的氯化
GB2544217B (en)	2014-08-08	2020-03-25	Tate & Lyle Tech Ltd	Chlorination of sucrose-6-esters
GB2536480B (en)	2015-03-17	2019-09-04	Tate & Lyle Tech Ltd	DMF Distillation
GB2551591B (en)	2016-06-23	2019-08-07	Tate & Lyle Tech Ltd	Liquid-liquid extraction of DMF
CN107459540A (zh) *	2017-08-28	2017-12-12	山东三和维信生物科技有限公司	用于三氯蔗糖生产的节省dmf及提高蔗糖‑6‑酯产率的方法
WO2022051988A1 (zh)	2020-09-10	2022-03-17	安徽金禾实业股份有限公司	一种蔗糖-6-酯的制备方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2583084A (en) *	1948-12-15	1952-01-22	Union Carbide & Carbon Corp	Hydrocarbon tin alcoholates
US2789994A (en) *	1952-07-11	1957-04-23	Metal & Thermit Corp	Polyhydric alcohol-organotin derivatives
DE3065399D1 (en) *	1979-12-18	1983-11-24	Tate & Lyle Plc	Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3062467D1 (en) *	1979-12-20	1983-04-28	Tate & Lyle Plc	Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
ATE9355T1 (de) *	1980-07-08	1984-09-15	Tate & Lyle Public Limited Company	Verfahren zur herstellung von 4,1',6'-trichlor4,1',6'-trideoxygalactosucrose (tgs).
US4430456A (en) *	1981-02-02	1984-02-07	Air Products And Chemicals, Inc.	Polyurethane-forming process using amino and amido dialkyl tin carboxylates
US4360670A (en) *	1981-02-02	1982-11-23	Air Products And Chemicals, Inc.	Amino and amido dialkyl tin carboxylates
US4464490A (en) *	1981-02-02	1984-08-07	Air Products And Chemicals, Inc.	Amino and amido dialkyl tin carboxylates and their use in preparing polyurethane products
US4465828A (en) *	1982-12-23	1984-08-14	The Procter & Gamble Company	Process of preparing alkylsaccharides
GB8622345D0 (en) *	1986-09-17	1986-10-22	Tate & Lyle Plc	Sucrose derivatives
US4950746A (en) *	1988-07-18	1990-08-21	Noramco, Inc.	Process for synthesizing sucrose derivatives by regioselective reaction

1990
- 1990-03-23 US US07/499,731 patent/US5089608A/en not_active Expired - Lifetime
1991
- 1991-03-14 GR GR910100124A patent/GR910100124A/el not_active IP Right Cessation
- 1991-03-20 JP JP3080358A patent/JP3064462B2/ja not_active Expired - Fee Related
- 1991-03-21 CA CA002038740A patent/CA2038740C/en not_active Expired - Lifetime
- 1991-03-22 PT PT97115A patent/PT97115B/pt not_active IP Right Cessation
- 1991-03-22 ES ES91302546T patent/ES2072541T3/es not_active Expired - Lifetime
- 1991-03-22 DE DE69109719T patent/DE69109719T2/de not_active Expired - Fee Related
- 1991-03-22 IE IE96291A patent/IE66892B1/en not_active IP Right Cessation
- 1991-03-22 DK DK91302546.6T patent/DK0448413T3/da active
- 1991-03-22 EP EP91302546A patent/EP0448413B1/de not_active Expired - Lifetime

Also Published As

Publication number	Publication date
DE69109719D1 (de)	1995-06-22
PT97115B (pt)	1998-08-31
DE69109719T2 (de)	1996-01-04
JPH04217993A (ja)	1992-08-07
PT97115A (pt)	1991-11-29
CA2038740A1 (en)	1991-09-24
JP3064462B2 (ja)	2000-07-12
GR910100124A (el)	1992-06-30
IE66892B1 (en)	1996-02-07
EP0448413B1 (de)	1995-05-17
CA2038740C (en)	2001-10-23
ES2072541T3 (es)	1995-07-16
US5089608A (en)	1992-02-18
EP0448413A1 (de)	1991-09-25
IE910962A1 (en)	1991-09-25

Publication	Publication Date	Title
DK0448413T3 (da)	1995-07-10	Selektiv 6-acylering af saccharose medieret af cycliske addukter af dialkyltinoxider og dioler
DK106191D0 (da)	1991-06-04	Mellemprodukter til fremstilling af penemer og carbapenemer
DK150585C (da)	1987-10-05	Kasseformet byggeelement og tagkonstruktion opbygget af saadanne elementer
DK482889D0 (da)	1989-10-02	Fremgangsmaade og apparat til fremstilling af boerstevarer
DK400088D0 (da)	1988-07-15	Fremstilling og anvendelse af t-cellesuppressorfaktor
FR2602031B3 (fr)	1988-08-26	Structure de construction de fours menagers
DK657889D0 (da)	1989-12-22	Kredsloeb til behandling af impulssignaler
DK695187A (da)	1988-07-23	Projektil med udfoldelig faldskaerm
DK540886A (da)	1987-10-04	Apparat til rensning af aeg
DK163377C (da)	1992-07-20	Skaerm til sloering af infraroed straaling
DK175587A (da)	1987-10-24	Fremstilling af substituerede (dichlormethyl)-pyridiner
LV5137A3 (lv)	1993-06-10	Saharozes 6-esteru iegusanas panemiens
DK0550757T3 (da)	2001-11-12	Impulsgenerator og støvkollektor med anvendelse af denne impulsgenerator
DK626784A (da)	1984-12-21	Fremgangsmaade og rensning af alkylerede antraquinoner
ES1007873Y (es)	1991-04-16	Mecanismo extensor y recogedor de cortinas.
DK123186A (da)	1987-09-19	Polypropylenfiberformmoertel og hjoernebyggekomponent
BR9002149A (pt)	1991-11-12	Terminal de poste e fachada
KR900005966U (ko)	1990-03-09	유선 tv 수신기의 입력회로
PL201104A1 (pl)	1979-04-23	Sposob laczenia elementow szklanych i/lub ceramicznych
SE8601797D0 (sv)	1986-04-18	Elektromekaniskt styrt och lasbart cykelstell
DK307190D0 (da)	1990-12-28	Skylning af gas gennem en smelte i en stoebeske
KR890011800U (ko)	1989-07-15	타이머에 의한 충전차단회로
KR920005447U (ko)	1992-03-26	다이얼 펄스 발생기 및 그 비율 가변회로
KR860004415U (ko)	1986-05-01	등화펄스 검출회로
DK143087D0 (da)	1987-03-20	Apparat til behandling af honningtavler