DK1005475T3 - Fremgangsmåde til fremstilling af Glufosinat samt mellemprodukter dertil - Google Patents

Fremgangsmåde til fremstilling af Glufosinat samt mellemprodukter dertil

Info

Publication number
DK1005475T3
DK1005475T3 DK98945195T DK98945195T DK1005475T3 DK 1005475 T3 DK1005475 T3 DK 1005475T3 DK 98945195 T DK98945195 T DK 98945195T DK 98945195 T DK98945195 T DK 98945195T DK 1005475 T3 DK1005475 T3 DK 1005475T3
Authority
DK
Denmark
Prior art keywords
glufosinate
intermediates
preparation
Prior art date
Application number
DK98945195T
Other languages
English (en)
Inventor
Lothar Willms
Original Assignee
Bayer Cropscience Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Cropscience Gmbh filed Critical Bayer Cropscience Gmbh
Application granted granted Critical
Publication of DK1005475T3 publication Critical patent/DK1005475T3/da

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/12Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6571Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
    • C07F9/657163Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms the ring phosphorus atom being bound to at least one carbon atom
    • C07F9/657172Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms the ring phosphorus atom being bound to at least one carbon atom the ring phosphorus atom and one oxygen atom being part of a (thio)phosphinic acid ester: (X = O, S)
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/30Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/301Acyclic saturated acids which can have further substituents on alkyl
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/30Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/32Esters thereof
    • C07F9/3205Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
    • C07F9/3211Esters of acyclic saturated acids which can have further substituents on alkyl

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
DK98945195T 1997-08-20 1998-08-08 Fremgangsmåde til fremstilling af Glufosinat samt mellemprodukter dertil DK1005475T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19736125A DE19736125A1 (de) 1997-08-20 1997-08-20 Verfahren zur Herstellung von Glufosinate und phosphorhaltige alpha-Aminonitrile als Zwischenprodukte
PCT/EP1998/005053 WO1999009039A1 (de) 1997-08-20 1998-08-08 Verfahren zur herstellung von glufosinate und zwischenprodukte dafür

Publications (1)

Publication Number Publication Date
DK1005475T3 true DK1005475T3 (da) 2004-05-17

Family

ID=7839559

Family Applications (1)

Application Number Title Priority Date Filing Date
DK98945195T DK1005475T3 (da) 1997-08-20 1998-08-08 Fremgangsmåde til fremstilling af Glufosinat samt mellemprodukter dertil

Country Status (27)

Country Link
US (1) US6359162B1 (da)
EP (1) EP1005475B1 (da)
JP (1) JP4519316B2 (da)
KR (1) KR100674326B1 (da)
CN (1) CN1261442C (da)
AR (1) AR015932A1 (da)
AT (1) ATE258180T1 (da)
AU (1) AU756471B2 (da)
BR (1) BR9811971B1 (da)
CA (1) CA2301181C (da)
CO (1) CO5031316A1 (da)
CZ (1) CZ2000593A3 (da)
DE (2) DE19736125A1 (da)
DK (1) DK1005475T3 (da)
ES (1) ES2214727T3 (da)
HU (1) HUP0003501A3 (da)
IL (1) IL134633A0 (da)
MY (1) MY132853A (da)
PH (1) PH11998002119A1 (da)
PL (1) PL191587B1 (da)
PT (1) PT1005475E (da)
RU (1) RU2275376C2 (da)
TR (1) TR200000456T2 (da)
TW (1) TW530063B (da)
UA (1) UA66806C2 (da)
WO (1) WO1999009039A1 (da)
ZA (1) ZA987465B (da)

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CN102399239A (zh) * 2011-12-27 2012-04-04 江苏优士化学有限公司 一种草铵膦及类似物的合成方法
CN102399240A (zh) * 2011-12-27 2012-04-04 江苏优士化学有限公司 一种改进的草铵膦及类似物的合成方法
CN103183707B (zh) * 2011-12-30 2016-06-15 中化蓝天集团有限公司 一种草胺膦的制备方法
CN102584893B (zh) * 2012-02-07 2015-03-04 浙江工业大学 一种草铵膦的制备方法
CN103374030B (zh) * 2012-04-13 2016-03-23 浙江新安化工集团股份有限公司 一种制备草铵膦的方法及其中间体的制备方法
CN103483379A (zh) * 2013-09-26 2014-01-01 江苏辉丰农化股份有限公司 一种草铵膦酸的制备方法
MX2016014792A (es) 2014-05-13 2017-03-23 Bayer Cropscience Ag Proceso para preparar cianhidrinas que contienen fosforo.
CN104558033B (zh) * 2014-12-19 2016-05-18 浙江工业大学 一种l-草铵膦-n-羧酸酐及其制备和应用
BR112017023253B1 (pt) 2015-04-27 2022-09-13 Basf Se Combinações de herbicida que compreendem glufosinato e indaziflam
JP2018529662A (ja) 2015-09-02 2018-10-11 バイエル・クロップサイエンス・アクチェンゲゼルシャフト リン含有シアノヒドリンエステルの製造方法
MX2018002729A (es) 2015-09-02 2018-04-13 Bayer Cropscience Ag Proceso para la elaboracion de esteres de cianohidrina que contienen fosforo.
KR20180048894A (ko) 2015-09-02 2018-05-10 바이엘 크롭사이언스 악티엔게젤샤프트 인 함유 시아노하이드린 에스테르의 제조 방법
KR20180045012A (ko) 2015-09-02 2018-05-03 바이엘 크롭사이언스 악티엔게젤샤프트 인 함유 시아노하이드린 에스테르의 제조 방법
MX377470B (es) 2015-09-29 2025-03-10 Bayer Cropscience Ag Proceso para producir fosfinatos.
CN107236001A (zh) * 2016-04-06 2017-10-10 四川省乐山市福华通达农药科技有限公司 一种膦醛的合成方法
CN107417721B (zh) * 2016-05-24 2019-05-28 四川福思达生物技术开发有限责任公司 一种氢氰酸加成工艺
WO2018108794A1 (de) 2016-12-15 2018-06-21 Bayer Cropscience Aktiengesellschaft Verfahren zur herstellung von d-glufosinat oder dessen salzen unter verwendung von ephedrin
WO2018108797A1 (de) 2016-12-15 2018-06-21 Bayer Cropscience Aktiengesellschaft Verfahren zur herstellung von l-glufosinat oder dessen salzen unter verwendung von ephedrin
EP3392237B1 (de) 2017-04-21 2019-10-02 Evonik Degussa GmbH Verfahren zur herstellung von acroleincyanhydrinen
CN111065270A (zh) * 2017-07-18 2020-04-24 阿格里麦蒂斯有限责任公司 L-草胺膦的生产方法
EP3655413B1 (de) 2017-07-21 2021-08-11 Basf Se Herstellung von glufosinat durch umsetzung von 3-[n-butoxy(methyl)phosphoryl]-1-cyanopropylacetat zu einer mischung aus n-butyl(3-amino-3-cyanopropyl)-methylphosphinat und (3-amino-3-cyanopropyl)-methylphosphinsäure ammoniumsalz
CN111479816B (zh) 2017-12-19 2023-10-27 巴斯夫欧洲公司 制备含磷α-氨基腈的方法
CN109134534B (zh) * 2018-08-08 2020-09-08 江苏好收成韦恩农化股份有限公司 一种3,3-二烷氧基丙基甲基膦酸酯简易制备方法
KR102131687B1 (ko) 2018-09-10 2020-07-08 주식회사 휴런 파킨슨 병 진단 장치 및 방법
AU2019420442B2 (en) 2019-01-11 2022-06-02 Cj Cheiljedang Corporation L-glufosinate intermediate and L-glufosinate preparation method
CN111662326B (zh) * 2019-03-05 2023-03-24 利尔化学股份有限公司 一种制备l-草铵膦的方法
CN111662324B (zh) * 2019-03-05 2023-02-24 利尔化学股份有限公司 一种制备l-草铵膦的方法
CN111662325B (zh) * 2019-03-05 2023-03-24 利尔化学股份有限公司 一种制备l-草铵膦的方法
CN110003269B (zh) * 2019-04-29 2022-04-05 利尔化学股份有限公司 低能耗生产草铵膦的方法
CN110590836B (zh) * 2019-09-30 2022-07-26 江苏七洲绿色化工股份有限公司 一种草铵膦中间体的合成方法
CN112898338A (zh) * 2019-12-04 2021-06-04 利尔化学股份有限公司 草铵膦中间体及草铵膦的制备方法
CN111659330B (zh) * 2020-04-23 2021-05-07 河北威远生物化工有限公司 一种连续化生产草铵膦的工艺与设备
CN112358499A (zh) * 2020-11-12 2021-02-12 江苏春江润田农化有限公司 一种草铵膦的合成方法
AU2022250692B2 (en) 2021-04-01 2024-01-04 Evonik Operations Gmbh Enzymatic method for producing l-glufosinate and its phosphoesters
EP4105335A1 (en) 2021-06-16 2022-12-21 Evonik Operations GmbH Enzymatic method for the production of l-glufosinate p-alkyl esters
CA3198877A1 (en) * 2021-07-20 2023-01-26 Min Xu Method for preparing glufosinate or analogues thereof
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CN114163472B (zh) * 2021-11-27 2024-08-09 永农生物科学有限公司 醇溶剂下合成α-氨基腈的方法及草铵膦的合成方法
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Also Published As

Publication number Publication date
MY132853A (en) 2007-10-31
TR200000456T2 (tr) 2000-07-21
BR9811971A (pt) 2000-08-15
JP2001515084A (ja) 2001-09-18
CN1267305A (zh) 2000-09-20
KR100674326B1 (ko) 2007-01-24
CA2301181C (en) 2008-08-05
HUP0003501A2 (en) 2001-03-28
KR20010023069A (ko) 2001-03-26
BR9811971B1 (pt) 2010-12-28
ES2214727T3 (es) 2004-09-16
TW530063B (en) 2003-05-01
AU756471B2 (en) 2003-01-16
ATE258180T1 (de) 2004-02-15
CO5031316A1 (es) 2001-04-27
JP4519316B2 (ja) 2010-08-04
UA66806C2 (uk) 2004-06-15
EP1005475A1 (de) 2000-06-07
ZA987465B (en) 1999-02-22
HUP0003501A3 (en) 2002-01-28
PH11998002119A1 (en) 2003-10-10
CA2301181A1 (en) 1999-02-25
CN1261442C (zh) 2006-06-28
AU9259898A (en) 1999-03-08
WO1999009039A1 (de) 1999-02-25
US6359162B1 (en) 2002-03-19
PT1005475E (pt) 2004-06-30
RU2275376C2 (ru) 2006-04-27
DE59810636D1 (de) 2004-02-26
CZ2000593A3 (cs) 2000-06-14
AR015932A1 (es) 2001-05-30
EP1005475B1 (de) 2004-01-21
DE19736125A1 (de) 1999-02-25
PL338855A1 (en) 2000-11-20
IL134633A0 (en) 2001-04-30
PL191587B1 (pl) 2006-06-30

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