DK2334591T3 - Fremgangsmåde til fremstilling af ammoniaksyntesegas - Google Patents

Fremgangsmåde til fremstilling af ammoniaksyntesegas Download PDF

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DK2334591T3
DK2334591T3 DK09817274.5T DK09817274T DK2334591T3 DK 2334591 T3 DK2334591 T3 DK 2334591T3 DK 09817274 T DK09817274 T DK 09817274T DK 2334591 T3 DK2334591 T3 DK 2334591T3
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syngas
reformer
reforming
primary
gas
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DK09817274.5T
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DK2334591T4 (da
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Ermanno Filippi
Geoffrey Frederick Skinner
Marco Badano
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Casale Sa
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/025—Preparation or purification of gas mixtures for ammonia synthesis
    • C—CHEMISTRY; METALLURGY
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    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/32—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air
    • C01B3/34—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/382—Processes with two or more reaction steps, of which at least one is catalytic, e.g. steam reforming and partial oxidation
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    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/32—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air
    • C01B3/34—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents
    • C01B3/48—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents followed by reaction of water vapour with carbon monoxide
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    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0233—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being a steam reforming step
    • C—CHEMISTRY; METALLURGY
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    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0244—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being an autothermal reforming step, e.g. secondary reforming processes
    • C—CHEMISTRY; METALLURGY
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    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0283—Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • C01B2203/0288—Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step containing two CO-shift steps
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    • C01B2203/0415—Purification by absorption in liquids
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    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0435—Catalytic purification
    • C01B2203/0445—Selective methanation
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    • C01B2203/0465—Composition of the impurity
    • C01B2203/047—Composition of the impurity the impurity being carbon monoxide
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    • C01B2203/0475—Composition of the impurity the impurity being carbon dioxide
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    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06—Integration with other chemical processes
    • C01B2203/068—Ammonia synthesis
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    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0805—Methods of heating the process for making hydrogen or synthesis gas
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    • C01B2203/0872—Methods of cooling
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    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1041—Composition of the catalyst
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    • C01B2203/1052—Nickel or cobalt catalysts
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    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205—Composition of the feed
    • C01B2203/1211—Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1235—Hydrocarbons
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    • C01B2203/14—Details of the flowsheet
    • C01B2203/142—At least two reforming, decomposition or partial oxidation steps in series
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    • C01B2203/14—Details of the flowsheet
    • C01B2203/146—At least two purification steps in series
    • C01B2203/147—Three or more purification steps in series
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00—Metal working
    • Y10T29/49—Method of mechanical manufacture
    • Y10T29/49716—Converting

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Claims (4)

1. Fremgangsmåde til fremstilling af ammoniaksyntesegas ud fra et carbonhydrid-indeholdende råmateriale (10), hvilken fremgangsmåde omfatter trinnene til dampreformering af det carbonhydrid-indeholdende råmateriale i en primær reformer (12), hvor alt råmaterialet (10) tilføres den primære reformer (12), opnåelse af en delvist reformeret gasstrøm (13), og sekundær reformering af den delvist reformerede gasstrøm i en sekundær reformer (14), som virker med overskydende luft, hvilken fremgangsmåde er kendetegnet ved, at: - den primære reformering og den sekundære reformering udvirkes ved et tryk på mindst 35 bar, - produktsyngassen (16) ved den sekundære reformerings udgang afkøles og underkastes katalytisk mellemtemperaturskift, idet CO konverteres til CO2 og H2, hvilket mellemtemperaturskift udføres på en kobberbaseret katalysator ved en i det væsentlige konstant temperatur i området 220-320 °C, - CO2 fjernes fra syngassen nedstrøms for mellemtemperaturskiftet ved hjælp af fysisk absorbering, - hvor damp/carbon-forholdet (SC) i den primære reformer (12) er mindre end 2,7.
2. Fremgangsmåde ifølge et hvilket som helst af de foregående krav, hvor den delvist reformerede syngas (13) ved den primære reformers (12) udgang har en temperatur i området 650-750 °C.
3. Fremgangsmåde ifølge et hvilket som helst af de foregående krav, hvor der udføres et yderligere lavtemperaturskift på syngasstrømmen (20) nedstrøms for mellemtemperaturskiftet.
4. Fremgangsmåde ifølge et hvilket som helst af de foregående krav, hvor CO2 fjernes under anvendelse af methanol som opløsningsmiddel eller et organisk opløsningsmiddel.
DK09817274.5T 2008-10-02 2009-08-26 Fremgangsmåde til fremstilling af ammoniaksyntesegas DK2334591T4 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP08017372A EP2172417A1 (en) 2008-10-02 2008-10-02 Process for the production of ammonia synthesis gas
PCT/EP2009/060970 WO2010037598A1 (en) 2008-10-02 2009-08-26 Process for producing ammonia synthesis gas

Publications (2)

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DK2334591T3 true DK2334591T3 (da) 2015-01-19
DK2334591T4 DK2334591T4 (da) 2019-06-03

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DK09817274.5T DK2334591T4 (da) 2008-10-02 2009-08-26 Fremgangsmåde til fremstilling af ammoniaksyntesegas

Country Status (13)

Country Link
US (1) US8545727B2 (da)
EP (2) EP2172417A1 (da)
CN (1) CN102171135B (da)
AR (1) AR075281A1 (da)
AU (1) AU2009299990B2 (da)
BR (1) BRPI0920435B1 (da)
CA (1) CA2737649C (da)
CL (1) CL2011000725A1 (da)
DK (1) DK2334591T4 (da)
MX (1) MX2011002860A (da)
MY (1) MY154901A (da)
RU (1) RU2510883C2 (da)
WO (1) WO2010037598A1 (da)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2404869A1 (en) * 2010-07-06 2012-01-11 Ammonia Casale S.A. Process for producing ammonia synthesis gas
CA2875696C (en) 2012-06-27 2020-09-01 Grannus, Llc Polygeneration production of power and fertilizer through emissions capture
US20150129806A1 (en) * 2013-11-08 2015-05-14 Ammonia Casale Sa Process for Producing Ammonia Synthesis Gas and a Method for Revamping a Front-End of an Ammonia Plant
EP3050849A1 (en) * 2015-01-27 2016-08-03 Casale SA A process for the synthesis of ammonia
DE102015210801A1 (de) 2015-06-12 2016-12-15 Thyssenkrupp Ag Mehrdruckverfahren zur Herstellung von Ammoniak ohne Anreicherung von Inertgas
EP3383794A4 (en) 2015-12-04 2019-04-17 Grannus, LLC HYDROGEN-PRODUCTION OF HYDROGEN FOR USE IN DIFFERENT INDUSTRIAL PROCESSES
EA202090244A1 (ru) 2017-07-13 2020-04-28 Хальдор Топсёэ А/С Способ и катализаторы для получения синтез-газа для производства аммиака
US12565423B2 (en) 2023-01-26 2026-03-03 Valero Services, Inc. Process for producing hydrogen from natural gas
EP4588888A1 (en) * 2024-01-19 2025-07-23 Yara International ASA Method for shutting down a plant comprising a hydrogen production system

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU327764A1 (ru) * 1969-06-11 1977-04-25 Способ производства аммиака
EP0031209B1 (en) * 1979-12-19 1986-01-29 Imperial Chemical Industries Plc Purification of hydrogen
FR2473032A1 (fr) * 1980-01-07 1981-07-10 Banquy David Procede de production d'ammoniac et du gaz de synthese correspondant
DE3571797D1 (en) * 1984-03-02 1989-08-31 Ici Plc Process for producing ammonia synthesis gas
US5736116A (en) * 1995-10-25 1998-04-07 The M. W. Kellogg Company Ammonia production with enriched air reforming and nitrogen injection into the synthesis loop
US6232352B1 (en) * 1999-11-01 2001-05-15 Acetex Limited Methanol plant retrofit for acetic acid manufacture
EP1603995B1 (en) * 2003-03-18 2018-05-30 Kellogg Brown & Root, Inc. Autothermal reformer-reforming exchanger arrangement for hydrogen production
DE10334590B4 (de) * 2003-07-28 2006-10-26 Uhde Gmbh Verfahren zur Gewinnung von Wasserstoff aus einem methanhaltigen Gas, insbesondere Erdgas und Anlage zur Durchführung des Verfahrens
EP1750836A4 (en) * 2004-05-28 2008-04-02 Hyradix Inc METHOD FOR PRODUCING HYDROGEN BY PARTIAL OXIDATION / STEAM REFORMING
EP1698588A1 (en) 2005-03-04 2006-09-06 Ammonia Casale S.A. Ammonia synthesis process

Also Published As

Publication number Publication date
EP2172417A1 (en) 2010-04-07
RU2510883C2 (ru) 2014-04-10
DK2334591T4 (da) 2019-06-03
CA2737649A1 (en) 2010-04-08
EP2334591B1 (en) 2014-10-15
BRPI0920435A2 (pt) 2015-12-22
MX2011002860A (es) 2011-06-16
WO2010037598A1 (en) 2010-04-08
RU2011117064A (ru) 2012-11-10
MY154901A (en) 2015-08-28
CN102171135A (zh) 2011-08-31
US20110168948A1 (en) 2011-07-14
CA2737649C (en) 2017-03-28
CN102171135B (zh) 2014-05-28
AU2009299990B2 (en) 2015-04-09
AR075281A1 (es) 2011-03-23
CL2011000725A1 (es) 2011-08-26
US8545727B2 (en) 2013-10-01
AU2009299990A1 (en) 2010-04-08
EP2334591A1 (en) 2011-06-22
EP2334591B2 (en) 2019-03-06
BRPI0920435B1 (pt) 2019-05-28

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