DK2509416T3 - Fremgangsmåde til at reducere og/eller opretholde den samlede levedygtige mængde af bakterier i vandigt formalet naturligt calciumkarbonat og/eller præcipiteret calciumkarbonat og/eller dolomit og/eller overfladereageret ... - Google Patents
Fremgangsmåde til at reducere og/eller opretholde den samlede levedygtige mængde af bakterier i vandigt formalet naturligt calciumkarbonat og/eller præcipiteret calciumkarbonat og/eller dolomit og/eller overfladereageret ... Download PDFInfo
- Publication number
- DK2509416T3 DK2509416T3 DK10787753.2T DK10787753T DK2509416T3 DK 2509416 T3 DK2509416 T3 DK 2509416T3 DK 10787753 T DK10787753 T DK 10787753T DK 2509416 T3 DK2509416 T3 DK 2509416T3
- Authority
- DK
- Denmark
- Prior art keywords
- biocide
- calcium carbonate
- weight
- aqueous
- aldehyde
- Prior art date
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/08—Amines; Quaternary ammonium compounds containing oxygen or sulfur
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aliphatically bound aldehyde or keto groups, or thio analogues thereof; Derivatives thereof, e.g. acetals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/04—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aldehyde or keto groups, or thio analogues thereof, directly attached to an aromatic ring system, e.g. acetophenone; Derivatives thereof, e.g. acetals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Agronomy & Crop Science (AREA)
- Health & Medical Sciences (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Claims (15)
1. Fremgangsmåde til at reducere og/eller opretholde den samlede levedygtige mængde af bakterier i et vandigt mineralpræparat omfattende et trin af: (a) at tilføje mindst et aldehyd-indeholdende og/eller aldehyd-frigivende og/eller phenol og/eller isothiazolin-biocid til det vandige mineralpræparat; kendetegnet ved at: - mineralet omfatter mindst et af: et formalet naturligt calciumkarbonat, et præcipiteret calciumkarbonat, et dolomit, et overfladereageret calciumkarbonat, eller en blanding deraf; - fremgangsmåden omfatter et trin (b), som kan være samtidigt med og/eller særskilt fra trin (a), af at tilføje mindst et monoalkohol primært alkanolamin til det vandige mineralpræparat; - biocidet/biociderne tilføjes til det vandige præparat i en mængde svarende til fra 90 til 1 350 ppm baseret på vægten af den vandige fase af det vandige præparat; og - det/de monoalkohol primære alkanolamin/alkanolaminer tilføjes til det vandige præparat i en mængde svarende til fra 600 til 1 200 ppm baseret på vægten af den vandige fase af det vandige præparat, hvor det mindst ene monoalkohol primært alkanolamin er valgt fra 2-amino-2-methyl-l-propanol, 2-aminoethanol og blandinger deraf.
2. Fremgangsmåde ifølge krav 1, kendetegnet ved at de aldehyd-indeholdende og/eller aldehyd-frigivende og/eller phenol og/eller isothiazolin-biocid/biocider tilføjes til det vandige præparat i en samlet mængde på fra 100 ppm til 1 000 ppm, og fortrinsvis i mængde af fra 150 ppm til 800 ppm, udregnet i forhold til vandet i præparatet.
3. Fremgangsmåde ifølge krav 1 eller 2, kendetegnet ved at det aldehydbaserede biocid er valgt fra gruppen bestående af formaldehyd, acetaldehyd, glyoxal, succinaldehyd, glutaraldehyd, 2-propenal, ftal dialdehyd og blandinger deraf, og fortrinsvis er formaldehyd, glutaraldehyd og blandinger deraf, og/eller kendetegnet ved at de aldehyd-frigivende biocider vælges fra gruppen bestående af formaldehyd-frigivende biocider, acetaldehyd-frigivende biocider, succinaldehyd-frigivende biocider, 2-propenal-frigivende biocider og blandinger deraf, hvor de aldehyd-frigivende biocider fortrinsvis vælges fra gruppen bestående af benzyl alkoholmono(poly)-hemiformal, ethylenglycolhemiformal (EGHF), [l,2-Ethanediylbis(oxy)]-bis-methanol,tetrahydro-l,3,4,6-tetrakis(hydroxylmethyl)imidazo[4,5-d]imidazole-2,5(lH,3H)-dione (også alment kendt som TetraMethylolAcetyleneDiurea TMAD) og blandinger deraf.
4. Fremgangsmåde ifølge et hvilket som helst af krav 1 til 3, kendetegnet ved at phenol-biocidet er orthophenylphenol (OPP), og/eller kendetegnet ved at isothiazolin-biocidet er valgt fra gruppen bestående af 2-methyl-4-isothiazolin-3-one (MIT), 5-chloro-2-methyl-2H-isothiazolin-3-one (CIT), l,2-benzisothiazolin-3-one (BIT), og blandinger deraf.
5. Fremgangsmåde ifølge et hvilket som helst af krav 1 til 4, kendetegnet ved at det aldehyd-frigivende og/eller aldehyd-baserede biocid anvendes sammen med biocider valgt fra gruppen bestående af 5-chloro-2-methyl-2H-isothiazolin-3-one (CIT), 2-methyl-2H-isothiazolin-3-one (MIT) og blandinger deraf.
6. Fremgangsmåde ifølge krav 1 eller 2, kendetegnet ved at biociderne er en kombination af glutaraldehyd, 5-chloro-2-methyl-2H-isothiazolin-3-one (CIT) og 2-methyl-2H-isothiazolin-3-one (MIT), eller en kombination af ethylenglycolhemiformal, 5-chloro-2-methyl-2H-isothiazolin-3-one (CIT) og 2-methyl-2H-isothiazolin-3-one (MIT).
7. Fremgangsmåde ifølge et hvilket som helst af krav 1 til 6, kendetegnet ved at mineralet omfatter et eller flere af: formalet naturligt calciumkarbonat, præcipiteret calciumkarbonat, dolomit og overfladereageret calciumkarbonat, og et eller flere af: kaolin, kaolin ler, calcineret kaolin ler, talkum, calciumsulfat, kvarts, attapulgit, montmorillonit, diatoméjord, fint inddelt silica, aluminiumoxid, aluminiumhydroxid, silikater såsom aluminiumsilikat, pimpsten og sepiolit, hvor det formalede naturlige calciumkarbonat og/eller præcipiterede calciumkarbonat og/eller dolomit og/eller overfladereagerede calciumkarbonat fortrinsvis er til stede i en mængde større end eller lig med 50 procent efter vægt, mere fortrinsvis større end eller lig med 60 procent efter vægt, endnu mere fortrinsvis større end eller lig med 70 procent efter vægt, endnu mere fortrinsvis større end eller lig med 80 procent efter vægt, og mest fortrinsvis større end eller lig med 90 procent efter vægt, i forhold til den samlede vægt af mineral faststofferne.
8. Fremgangsmåde ifølge et hvilket som helst af krav 1 til 7, kendetegnet ved at mineralet består i alt væsentligt af kun formalet naturligt calciumkarbonat, præcipiteret calciumkarbonat, dolomit, overfladereageret calciumkarbonat eller blandinger deraf, og fortrinsvis består i alt væsentligt kun af formalet naturligt calciumkarbonat.
9. Fremgangsmåde ifølge et hvilket som helst af krav 1 til 8, kendetegnet ved at det vandige mineralpræparat har et faststofindhold på fra 40 til 82 procent efter vægt, fortrinsvis på fra 50 til 80 procent efter vægt, og endnu mere fortrinsvis på fra 60 til 80 procent efter vægt; og/eller kendetegnet ved at det vandige mineralpræparat har en pH på mellem 8 og 10, forud for tilføjelsen af et hvilket som helst biocid og/eller monoalkohol primært alkanolamin.
10. Fremgangsmåde ifølge et hvilket som helst af krav 1 til 9, kendetegnet ved at det vandige mineralpræparat dispergeres, fortrinsvis med et dispergeringsmiddel lavet af monomerer og/eller co-monomerer valgt fra gruppen bestående af akrylsyre, methakrylsyre, itakonsyre, crotonsyre, fumarsyre, maleinanhydridsyre, isocrotonsyre, aconitsyre (cis eller trans), mesaconsyre, sinapinsyre, undecylensyre, angelicasyre, canellinsyre, hydroxyakrylsyre, acrolein, akrylamid, acrylonitril, dimethylaminoethyl methakrylat, vinylpyrrolidon, vinylcaprolactam, ethylen, propylen, isobutylen, diisobutylen, vinylacetat, styren, a-methyl styren, methyl vinyl keton, estere af akryl- og methakrylsyrer og blandinger deraf, hvor poly(akrylsyre) og/eller poly (methakrylsyre) er foretrukne som dispergeringsmiddel.
11. Fremgangsmåde ifølge krav 1 eller 2, kendetegnet ved at i tilfældet hvor biocidet er aldehyd-baseret biocid, de monoalkohol primære alkanolaminer tilføjes i en mængde således at vægtforholdet biocid : monoalkohol primært alkanolamin er fra 1 : 4 til 1 : 1, eller kendetegnet ved at i tilfældet hvor biocidet er et phenol biocid, det monoalkohol primære alkanolamin tilføjes i en mængde således at vægtforholdet biocid : monoalkohol primært alkanolamin er fra 1 : 4 til 1 : 2.
12. Fremgangsmåde ifølge et hvilket som helst af krav 1 til 11, kendetegnet ved at biocidet/biociderne og det monoalkohol primære alkanolamin tilføjes separat fra det vandige præparat, hvor alt af det monoalkohol primære alkanolamin fortrinsvis tilføjes før et hvilket som helst af biocidet/biociderne.
13. Fremgangsmåde ifølge et hvilket som helst af krav 1 til 12, kendetegnet ved at forud for tilføjelsen af et hvilket som helst af det monoalkohol primære alkanolamin eller biocidet, det vandige præparat indeholder bakterier valgt fra gruppen bestående af Thermus sp., Propionibacterium sp., Rhodococcus sp., Panninobacter sp., Caulobacter sp., Brevundimonas sp., Asticcacaulis sp., Sphingomonas sp., Rhizobium sp., Ensifer sp., Bradyrhizobium sp., Tepidimonas sp., Tepidicella sp., Aquabacterium sp.,Pelomonas sp., Alcaligenis sp., Achromobacter sp., Ralstonia sp., Limnobacter sp.,Massilia sp., Hydrogenophaga sp., Acidovorax sp., Curvibacter sp., Delftia sp., Rhodoferax sp., Alishewanella sp., Stenotrophomonas sp., Dokdonella sp.,Methylosinus sp., Hyphomicrobium sp., Methylosulfomonas sp., Methylobacteria sp.,Pseudomonas sp. og blandinger deraf, og mere fortrinsvis indeholder bakterier valgt fra gruppen bestående af Pseudomonas putida, Pseudomonas mendocina, Pseudomonas fluorescens, Pseudomonas alcaligenes, Pseudomonas pseudoalcaligenes, Pseudomonas entomophila, Pseudomonas syringae, Methylobacterium extorquens, Methylobacterium radiotolerants, Methylobacterium dichloromethanicum, Methylobacterium organophilu, Hyphomicrobium zavarzini og blandinger deraf.
14. Fremgangsmåde ifølge krav 13, kendetegnet ved at alle eller andele af bakterierne er resistente overfor, tolerante overfor og/eller nedbryder biociderne i mangel på det monoalkohol primære alkanolamin.
15. Anvendelse af mindst et monoalkohol primært alkanolamin som en biocidaktivitetsfremmende forbindelse i et vandigt formalet naturligt calciumkarbonat og/eller præcipiteret calciumkarbonat og/eller dolomit og/eller overfladereageret calciumkarbonat-omfattende mineral præparat omfattende mindst et aldehyd-indeholdende og/eller aldehyd-frigivende og/eller phenol og/eller isothiazolin-biocid, hvor den samlede mængde af biocidet/biociderne i det vandige præparat er fra 90 ppm til 1 350 ppm, udregnet i forhold til vægten af den vandige fase af præparatet, og den samlede mængde af det/de monoalkohol primære alkanolamin/alkanolaminer i det vandige præparat er fra 600 til 1 200 ppm, udregnet i forhold til vægten af den vandige fase af præparatet, hvor det mindst ene monoalkohol primært alkanolamin er valgt fra 2-amino-2-methyl-l-propanol, 2-aminoethanol og blandinger deraf.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09178228A EP2329712A1 (en) | 2009-12-07 | 2009-12-07 | Process for bacterial stabilizing of aqueous ground natural calcium carbonate and/or precipitated calcium carbonate and/or dolomite and/or surface-reacted calcium carbonate-comprising mineral preparations |
| US28419909P | 2009-12-14 | 2009-12-14 | |
| EP10165674 | 2010-06-11 | ||
| PCT/EP2010/068966 WO2011069961A1 (en) | 2009-12-07 | 2010-12-06 | Process for bacterial stabilizing of aqueous ground natural calcium carbonate and/or precipitated calcium carbonate and/or dolomite and/or surface-reacted calcium carbonate-comprising mineral preparations |
Publications (1)
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| DK2509416T3 true DK2509416T3 (da) | 2015-12-07 |
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| JP (1) | JP5643331B2 (da) |
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| CN (1) | CN102647902B (da) |
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| CO (1) | CO6551735A2 (da) |
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| MX (1) | MX2012006212A (da) |
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| PT (1) | PT2509416E (da) |
| RU (2) | RU2515380C2 (da) |
| SI (1) | SI2509416T1 (da) |
| TW (1) | TWI577283B (da) |
| WO (1) | WO2011069961A1 (da) |
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| PL2596702T3 (pl) * | 2011-11-25 | 2015-10-30 | Omya Int Ag | Sposób stabilizowania zawartości bakterii w wodnych preparatach mineralnych zawierających mielony, naturalny węglan wapnia i/lub strącony węglan wapnia, i/lub dolomit, i/lub poddany powierzchniowej reakcji węglan wapnia |
| GB2515473A (en) * | 2013-06-18 | 2014-12-31 | Robert Timothy Gros | Anti microbial inks and sealants |
| EP2824147B1 (en) * | 2013-07-12 | 2016-01-20 | Omya International AG | Use of 2-amino-2-ethyl-1,3-propanediol as additive in aqueous suspensions of calcium carbonate-comprising materials while maintaining stable suspension conductivity |
| CN103555000A (zh) * | 2013-09-28 | 2014-02-05 | 昆山市周市溴化锂溶液厂 | 超细重质碳酸钙的研磨方法 |
| GB201322840D0 (en) * | 2013-12-23 | 2014-02-12 | Imerys Minerals Ltd | Aqueous suspension of inorganic particulate material |
| TWI490333B (zh) | 2013-12-26 | 2015-07-01 | Ind Tech Res Inst | 用於培養嗜熱性鹼性蛋白酶生產菌屬（Ｔｅｐｉｄｉｍｏｎａｓ）之菌的培養基以及方法 |
| EP3045042A1 (en) * | 2015-01-15 | 2016-07-20 | Omya International AG | Use of surface-reacted calcium carbonate as carrier for agrochemical compounds |
| EP3183969A1 (en) * | 2015-12-22 | 2017-06-28 | Omya International AG | Metal oxides and/or hydrates thereof for stabilising an aqueous preparation against microbial growth |
| EP3611248B1 (en) * | 2016-09-08 | 2022-10-26 | Morehouse School of Medicine | Method of making a cleaning composition |
| PH12022552369A1 (en) * | 2020-04-28 | 2023-12-18 | Unilever Ip Holdings B V | An aqueous laundry treatment composition |
| CN113104877A (zh) * | 2021-04-22 | 2021-07-13 | 铜陵博锋实业有限公司 | 一种超细白云石的制备方法及超细白云石的应用 |
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