DK3426601T3 - Fremgangsmåde og anlæg til at fremstille en produktgas under varierende belastningsforhold - Google Patents

Fremgangsmåde og anlæg til at fremstille en produktgas under varierende belastningsforhold Download PDF

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Publication number
DK3426601T3
DK3426601T3 DK17709411.7T DK17709411T DK3426601T3 DK 3426601 T3 DK3426601 T3 DK 3426601T3 DK 17709411 T DK17709411 T DK 17709411T DK 3426601 T3 DK3426601 T3 DK 3426601T3
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DK
Denmark
Prior art keywords
procedure
producing
product gas
under various
gas under
Prior art date
Application number
DK17709411.7T
Other languages
English (en)
Inventor
Bärbel Kolbe
Christoph Roosen
Joachim Johanning
Beerbühl Simon Schulte
Frank Schultmann
Original Assignee
Thyssenkrupp Ind Solutions Ag
Thyssenkrupp Ag Thyssenkrupp Ag
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Application filed by Thyssenkrupp Ind Solutions Ag, Thyssenkrupp Ag Thyssenkrupp Ag filed Critical Thyssenkrupp Ind Solutions Ag
Application granted granted Critical
Publication of DK3426601T3 publication Critical patent/DK3426601T3/da

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/04—Preparation of ammonia by synthesis
    • C01C1/0405—Preparation of ammonia by synthesis from N2 and H2 in presence of a catalyst
    • C01C1/0417—Preparation of ammonia by synthesis from N2 and H2 in presence of a catalyst characterised by the synthesis reactor, e.g. arrangement of catalyst beds and heat exchangers in the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0453—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0457—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being placed in separate reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0492—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/04—Preparation of ammonia by synthesis
    • C01C1/0405—Preparation of ammonia by synthesis from N2 and H2 in presence of a catalyst
    • C01C1/0458—Separation of NH3
    • C01C1/047—Separation of NH3 by condensation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/04—Preparation of ammonia by synthesis
    • C01C1/0405—Preparation of ammonia by synthesis from N2 and H2 in presence of a catalyst
    • C01C1/0482—Process control; Start-up or cooling-down procedures
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
    • C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00176—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles outside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00265—Part of all of the reactants being heated or cooled outside the reactor while recycling
    • B01J2208/00274—Part of all of the reactants being heated or cooled outside the reactor while recycling involving reactant vapours
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00327—Controlling the temperature by direct heat exchange
    • B01J2208/00336—Controlling the temperature by direct heat exchange adding a temperature modifying medium to the reactants
    • B01J2208/00353—Non-cryogenic fluids
    • B01J2208/00371—Non-cryogenic fluids gaseous
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00389—Controlling the temperature using electric heating or cooling elements
    • B01J2208/00415—Controlling the temperature using electric heating or cooling elements electric resistance heaters
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00548—Flow
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Automation & Control Theory (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
DK17709411.7T 2016-03-08 2017-03-06 Fremgangsmåde og anlæg til at fremstille en produktgas under varierende belastningsforhold DK3426601T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102016203753.6A DE102016203753A1 (de) 2016-03-08 2016-03-08 Verfahren zur Herstellung von Produkten unter wechselnden Lastbedingungen
PCT/EP2017/055120 WO2017153304A1 (de) 2016-03-08 2017-03-06 Verfahren sowie anlage zur herstellung eines produktgases unter wechselnden lastbedingungen

Publications (1)

Publication Number Publication Date
DK3426601T3 true DK3426601T3 (da) 2020-07-20

Family

ID=58261653

Family Applications (1)

Application Number Title Priority Date Filing Date
DK17709411.7T DK3426601T3 (da) 2016-03-08 2017-03-06 Fremgangsmåde og anlæg til at fremstille en produktgas under varierende belastningsforhold

Country Status (4)

Country Link
EP (1) EP3426601B1 (da)
DE (1) DE102016203753A1 (da)
DK (1) DK3426601T3 (da)
WO (1) WO2017153304A1 (da)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102017222948A1 (de) 2017-12-15 2019-01-24 Thyssenkrupp Ag Produktion von Ammoniak und Wasserstoff mit direkter Stromeinspeisung aus Offshore Energiegewinnungsanlagen
NL2023912B1 (en) 2019-09-26 2021-05-27 Univ Delft Tech Periodic ammonia production
EP3819261A1 (en) * 2019-11-08 2021-05-12 Casale Sa Control of an ammonia synthesis loop at partial load
WO2021149013A1 (en) * 2020-01-24 2021-07-29 Cri Hf Load-following reactor system, associated facilities, and method of operating the same
PE20230900A1 (es) * 2020-10-30 2023-06-01 Casale Sa Control de un circuito de sintesis de amoniaco a carga parcial
US12491484B2 (en) 2021-01-15 2025-12-09 CRI, hf Reactor for synthesis of methanol or other products
EP4277736A1 (en) 2021-01-15 2023-11-22 Cri Hf Methanol synthesis reactor
DE102021122602B4 (de) 2021-09-01 2024-03-28 Uniper Technologies GmbH Anlage und Verfahren zur kontinuierlichen Herstellung von Ammoniak unter Verwendung von erneuerbaren Energien
EP4148020A1 (en) * 2021-09-13 2023-03-15 Casale Sa Method for controlling an ammonia plant
BE1029986B1 (de) * 2021-12-03 2023-07-03 Thyssenkrupp Ag Verfahren zum Betreiben einer Ammoniakanlage und Anlage zur Herstellung von Ammoniak
BE1029985B1 (de) * 2021-12-03 2023-07-04 Thyssenkrupp Ag Verfahren zur Ammoniaksynthese und Anlage zur Herstellung von Ammoniak
WO2023099743A1 (de) * 2021-12-03 2023-06-08 Thyssenkrupp Industrial Solutions Ag Verfahren zum betreiben einer ammoniakanlage und anlage zur herstellung von ammoniak
PE20251304A1 (es) * 2022-05-12 2025-05-15 Casale Sa Metodo para controlar un convertidor de amoniaco o metanol
EP4349779A1 (de) 2022-10-19 2024-04-10 Linde GmbH Verfahren zur betrieb einer ammoniaksynthese in teillast sowie teillastfähige ammoniaksynthese
EP4474032A1 (de) 2023-06-07 2024-12-11 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Wechsellastbetrieb einer methanolanlage
EP4516740A1 (en) 2023-09-04 2025-03-05 Topsoe A/S Method for controlling an ammonia plant using renewable energy
WO2025073609A1 (de) 2023-10-04 2025-04-10 Thyssenkrupp Uhde Gmbh Synthese von grünem ammoniak bei variablem durchsatz
LU103199B1 (de) 2023-10-04 2025-04-04 Thyssenkrupp Ag Synthese von grünem Ammoniak bei variablem Durchsatz
WO2025196205A1 (en) 2024-03-21 2025-09-25 Casale Sa Method of managing an ammonia synthesis reactor during fluctuating feed rates
EP4685112A1 (de) 2024-07-26 2026-01-28 Linde GmbH Verfahren und anlage zur herstellung eines ammoniakprodukts

Family Cites Families (10)

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GB1565824A (en) * 1976-11-15 1980-04-23 Ici Ltd Exothermic process and apparatus therefor
US4341737A (en) * 1979-05-22 1982-07-27 The Lummus Company Apparatus for carrying out catalytic exothermic and endothermic high-pressure gas reactions
EP0026057B1 (en) * 1979-09-14 1984-03-14 Imperial Chemical Industries Plc Synthesis reactor and processes
DE8717724U1 (de) * 1987-03-18 1989-10-05 Uhde Gmbh, 4600 Dortmund Zweistufiger Ammoniakkonverter mit wenigstens einem Katalysatorbett mit in dessen Inneren angeordneten Wärmetauscher
DE3905034A1 (de) * 1989-02-18 1990-08-23 Fuderer Michael Ammoniaksyntheseverfahren mit hochdruckstripper
DD295741A7 (de) * 1989-04-05 1991-11-14 Stickstoffwerke Ag Wittenberg,De Verfahren zur steuerung des methan- und edelgasgehaltes eines ammoniak-wasserstoffrueckgewinnung-edelgas-komplexes
US20070107432A1 (en) * 2005-11-11 2007-05-17 Sheldon Smith Packaged system for the production of chemical compounds from renewable energy resources
WO2012037571A2 (en) 2010-09-17 2012-03-22 Robertson John S Energy storage and conversion systems
EP2589574B1 (en) 2011-11-02 2015-10-21 Casale Sa Method for load regulation of an ammonia plant
EP2610001A1 (en) * 2011-12-27 2013-07-03 Ammonia Casale S.A. Adiabatic multi-bed catalytic converter with inter-bed cooling and a related process

Also Published As

Publication number Publication date
EP3426601A1 (de) 2019-01-16
DE102016203753A1 (de) 2017-09-14
WO2017153304A1 (de) 2017-09-14
EP3426601B1 (de) 2020-05-06

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