EP0356858A3 - Verfahren zur Abtrennung von Cyclohexanol - Google Patents

Verfahren zur Abtrennung von Cyclohexanol Download PDF

Info

Publication number
EP0356858A3
EP0356858A3 EP19890115357 EP89115357A EP0356858A3 EP 0356858 A3 EP0356858 A3 EP 0356858A3 EP 19890115357 EP19890115357 EP 19890115357 EP 89115357 A EP89115357 A EP 89115357A EP 0356858 A3 EP0356858 A3 EP 0356858A3
Authority
EP
European Patent Office
Prior art keywords
cyclohexanol
separation
mindestens einem
ether
phenol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP19890115357
Other languages
English (en)
French (fr)
Other versions
EP0356858A2 (de
EP0356858B1 (de
Inventor
Hans-Juergen Dr. Gosch
Rolf Dr. Fischer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of EP0356858A2 publication Critical patent/EP0356858A2/de
Publication of EP0356858A3 publication Critical patent/EP0356858A3/de
Application granted granted Critical
Publication of EP0356858B1 publication Critical patent/EP0356858B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

Verfahren zur Abtrennung von Cyclohexanol aus solche und aromatische Sulfonsäuren enthaltenden wäßrigen Lösungen durch Extraktion, dadurch gekennzeichnet, daß man als Extraktionsmittel Gemische aus
  • a) mindestens einem bei Extraktionsbedingungen inerten flüssigen aliphatischen, cycloaliphatischen oder aromatischen Kohlenwasserstoff, Halogenchlorkohlenwasserstoff oder Ether und
  • b) mindestens einem Phenol
  • verwendet
    EP89115357A 1988-08-27 1989-08-19 Verfahren zur Abtrennung von Cyclohexanol Expired - Lifetime EP0356858B1 (de)

    Applications Claiming Priority (2)

    Application Number Priority Date Filing Date Title
    DE3829142A DE3829142A1 (de) 1988-08-27 1988-08-27 Verfahren zur abtrennung von cyclohexanol
    DE3829142 1988-08-27

    Publications (3)

    Publication Number Publication Date
    EP0356858A2 EP0356858A2 (de) 1990-03-07
    EP0356858A3 true EP0356858A3 (de) 1992-01-08
    EP0356858B1 EP0356858B1 (de) 1994-10-19

    Family

    ID=6361739

    Family Applications (1)

    Application Number Title Priority Date Filing Date
    EP89115357A Expired - Lifetime EP0356858B1 (de) 1988-08-27 1989-08-19 Verfahren zur Abtrennung von Cyclohexanol

    Country Status (5)

    Country Link
    US (1) US4990688A (de)
    EP (1) EP0356858B1 (de)
    JP (1) JPH02108643A (de)
    DE (2) DE3829142A1 (de)
    ES (1) ES2063090T3 (de)

    Families Citing this family (2)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    US6197817B1 (en) * 1999-01-22 2001-03-06 Selectus Pharmaceuticals, Inc. Phenylpropionic acids and esters: compounds and methods for inducing beta-blockade for the treatment of cardiac disorders
    KR20040012990A (ko) * 2001-06-28 2004-02-11 제온 코포레이션 시클로알킬 알킬 에테르 화합물을 함유하여 이루어지는용제 및 시클로알킬 알킬 에테르 화합물의 제조방법

    Citations (2)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    EP0227931A2 (de) * 1985-11-22 1987-07-08 Sumitomo Chemical Company, Limited Herstellungsverfahren von Cycloalkanolen
    EP0285911A2 (de) * 1987-04-07 1988-10-12 Sumitomo Chemical Company, Limited Trennungsverfahren von Cyclohexanol

    Family Cites Families (5)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    US2927944A (en) * 1960-03-08 Process for separation of cyclohexanol and cyclohexanone
    US2974174A (en) * 1958-11-03 1961-03-07 Phillips Petroleum Co Solvent extraction process
    US4306101A (en) * 1980-11-05 1981-12-15 Shell Oil Company Olefin hydration process
    JPS59193836A (ja) * 1983-04-15 1984-11-02 Asahi Chem Ind Co Ltd アルコ−ル類の製造法
    JPS62103033A (ja) * 1985-07-02 1987-05-13 Sumitomo Chem Co Ltd シクロヘキサノ−ルの分離法

    Patent Citations (2)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    EP0227931A2 (de) * 1985-11-22 1987-07-08 Sumitomo Chemical Company, Limited Herstellungsverfahren von Cycloalkanolen
    EP0285911A2 (de) * 1987-04-07 1988-10-12 Sumitomo Chemical Company, Limited Trennungsverfahren von Cyclohexanol

    Also Published As

    Publication number Publication date
    EP0356858A2 (de) 1990-03-07
    US4990688A (en) 1991-02-05
    ES2063090T3 (es) 1995-01-01
    DE58908524D1 (de) 1994-11-24
    DE3829142A1 (de) 1990-03-01
    JPH02108643A (ja) 1990-04-20
    EP0356858B1 (de) 1994-10-19

    Similar Documents

    Publication Publication Date Title
    AU535196B2 (en) Separating rare earth ozides from galliom oxide
    DE59608686D1 (de) Verfahren zur Entfernung von unerwünschten lipophilen Verunreinigungen und/oder Rückständen, welche in Getränken oder pflanzlichen Zubereitungen enthalten sind
    CA2011151A1 (en) Mercury removal from liquid hydrocarbon compound
    BR9006775A (pt) Sistema e processo para ministrar uma mistura de concentrado e diluente,sistema para ministrar um liquido e conjunto de controle de vazao
    DE3587996D1 (de) Verfahren zur Bereitstellung einer "On-line"-Hilfestellung für interaktive Datenverarbeitungsanlagen.
    DE69125275D1 (de) Verfahren zur flüssigchromatografischen extraction von strontium aus säurelösungen
    DE3774754D1 (de) Verfahren und vorrichtung zur herstellung von glasgarnen durch mechanisches ziehen und erhaltene gegenstaende.
    TW324715B (en) Process for a rectificative separation of (meth)acrylic acid from a hydrophobic mixture containing crude (meth)acrylic acid
    DE58907088D1 (de) Verfahren zur Trennung von Folinsäure.
    DE3765158D1 (de) Verfahren zur abtrennung von phenolen und basen aus steinkohlenteeroelen durch extraktion.
    AU7460687A (en) Method for amino acid extraction
    DE59407429D1 (de) Verfahren zur Wiederaufbereitung von gebrauchten glykolischen Flugzeugenteisungsmitteln
    DE69402633D1 (de) Verfahren zur Trennung und Rückgewinnung von Plutonium und Neptunium aus einer Salpetersäurelösung
    DE69023764D1 (de) Verfahren zur Trennung durch Adsorption von 2,6- oder 3,5-Diethyltoluol aus einer Mischung davon mit einem anderen Diethyltoluolisomer.
    DE68900939D1 (de) Entfernung von sauren verunreinigungen in einem loesungsmittelextraktionsverfahren zur trennung von aromaten von nichtaromaten.
    AU1338788A (en) Process for separation of rare earths
    DE59001782D1 (de) Verfahren zur trennung eines gemisches aus 1-methoxypropanol-2 und wasser in seine bestandteile.
    DE3865510D1 (de) Verfahren zur beseitigung von radioaktivitaet aus abwaessern durch fluessig-fluessig-extraktion.
    ES524070A0 (es) Un procedimiento de dosificacion de las lipoproteinas de baja densidad (ldl) contenidas en los liquidos biologicos o en los extractos tisulares
    DE69315477D1 (de) Verfahren zur Rückgewinnung von Phenol aus dessen Cumol- oder Alpha-methylstyrol enthaltenden Gemischen
    CA2184311A1 (en) Method for Removing Sulfolane Present in Hydrocarbon
    AT388570B (de) Extraktionsmittel sowie verfahren zur aufarbeitung von ge-haeltigen waesserigen loesungen durch fluessig/fluessigextraktion
    DE58907389D1 (de) Verfahren zur Abtrennung von Cyclohexanol aus solches und aromatische Sulfonsäuren enthaltenden wässrigen Lösungen.
    ATE53835T1 (de) Verfahren zur abtrennung von schwefelsaeure aus waesserigen loesungen, die sie zusammen mit alkansulfonsaeuren enthalten.
    ATE35533T1 (de) Verfahren zur rueckgewinnung von reiner benzoesaeure.

    Legal Events

    Date Code Title Description
    PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

    Free format text: ORIGINAL CODE: 0009012

    AK Designated contracting states

    Kind code of ref document: A2

    Designated state(s): BE CH DE ES FR GB IT LI NL

    17P Request for examination filed

    Effective date: 19901227

    PUAL Search report despatched

    Free format text: ORIGINAL CODE: 0009013

    AK Designated contracting states

    Kind code of ref document: A3

    Designated state(s): BE CH DE ES FR GB IT LI NL

    17Q First examination report despatched

    Effective date: 19930902

    GRAA (expected) grant

    Free format text: ORIGINAL CODE: 0009210

    AK Designated contracting states

    Kind code of ref document: B1

    Designated state(s): BE CH DE ES FR GB IT LI NL

    REF Corresponds to:

    Ref document number: 58908524

    Country of ref document: DE

    Date of ref document: 19941124

    ITF It: translation for a ep patent filed
    GBT Gb: translation of ep patent filed (gb section 77(6)(a)/1977)

    Effective date: 19941103

    REG Reference to a national code

    Ref country code: ES

    Ref legal event code: FG2A

    Ref document number: 2063090

    Country of ref document: ES

    Kind code of ref document: T3

    ET Fr: translation filed
    PLBE No opposition filed within time limit

    Free format text: ORIGINAL CODE: 0009261

    STAA Information on the status of an ep patent application or granted ep patent

    Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

    26N No opposition filed
    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: DE

    Payment date: 20010811

    Year of fee payment: 13

    REG Reference to a national code

    Ref country code: GB

    Ref legal event code: IF02

    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: FR

    Payment date: 20020716

    Year of fee payment: 14

    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: NL

    Payment date: 20020724

    Year of fee payment: 14

    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: CH

    Payment date: 20020725

    Year of fee payment: 14

    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: ES

    Payment date: 20020807

    Year of fee payment: 14

    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: GB

    Payment date: 20020815

    Year of fee payment: 14

    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: BE

    Payment date: 20020830

    Year of fee payment: 14

    PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

    Ref country code: DE

    Free format text: LAPSE BECAUSE OF THE APPLICANT RENOUNCES

    Effective date: 20020924

    PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

    Ref country code: GB

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20030819

    PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

    Ref country code: ES

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20030820

    PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

    Ref country code: LI

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20030831

    Ref country code: CH

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20030831

    Ref country code: BE

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20030831

    BERE Be: lapsed

    Owner name: *BASF A.G.

    Effective date: 20030831

    PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

    Ref country code: NL

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20040301

    GBPC Gb: european patent ceased through non-payment of renewal fee

    Effective date: 20030819

    REG Reference to a national code

    Ref country code: CH

    Ref legal event code: PL

    PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

    Ref country code: FR

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20040430

    NLV4 Nl: lapsed or anulled due to non-payment of the annual fee

    Effective date: 20040301

    REG Reference to a national code

    Ref country code: FR

    Ref legal event code: ST

    REG Reference to a national code

    Ref country code: ES

    Ref legal event code: FD2A

    Effective date: 20030820

    PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

    Ref country code: IT

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES;WARNING: LAPSES OF ITALIAN PATENTS WITH EFFECTIVE DATE BEFORE 2007 MAY HAVE OCCURRED AT ANY TIME BEFORE 2007. THE CORRECT EFFECTIVE DATE MAY BE DIFFERENT FROM THE ONE RECORDED.

    Effective date: 20050819