EP0458845A1 - Granule a additifs detergents et procede de production d'un tel granule. - Google Patents

Granule a additifs detergents et procede de production d'un tel granule.

Info

Publication number
EP0458845A1
EP0458845A1 EP90903319A EP90903319A EP0458845A1 EP 0458845 A1 EP0458845 A1 EP 0458845A1 EP 90903319 A EP90903319 A EP 90903319A EP 90903319 A EP90903319 A EP 90903319A EP 0458845 A1 EP0458845 A1 EP 0458845A1
Authority
EP
European Patent Office
Prior art keywords
granulate
core
shell
detergent additive
granulate according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP90903319A
Other languages
German (de)
English (en)
Other versions
EP0458845B1 (fr
Inventor
Erik Kjaer Markussen
Per Falholt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Novozymes AS
Original Assignee
Novo Nordisk AS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=8097473&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=EP0458845(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Novo Nordisk AS filed Critical Novo Nordisk AS
Publication of EP0458845A1 publication Critical patent/EP0458845A1/fr
Application granted granted Critical
Publication of EP0458845B1 publication Critical patent/EP0458845B1/fr
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38672—Granulated or coated enzymes

Definitions

  • the enzyme containing granulate described in Danish patent application No. 4368/88 comprises a core surrounded by a coating comprising cellulose fibres or artificial fibres in an amount of 1.5 to 40% by weight, based on the dry weight of the granulate except for the core, a binder in an amount of 0 to 15% by weight, based on the dry weight of the granulate, except for the core, a filler, and one or more granulating agents, whereby the core and/or the coating contains an enzyme.
  • the invention is a further development of the special embodiment of the invention described in Danish patent application No. 4368/88, which comprises an enzyme in either the core or the shell.
  • the shell or the core in the detergent additive granulate according to the invention does not necessarily contain an enzyme; but the core contains one detergent additive (which may be an enzyme, here identified as the primary detergent additive) , and the shell contains another detergent additive (which may be another enzyme, here identified as the secondary detergent additive) .
  • the primary detergent additive should be protected against the secondary detergent additive and/or environmental factors ,- ⁇ e.g. in cases where an enzyme is degraded by a bleaching agent and humidity in the atmosphere, or vice versa
  • there is a need for an effective separation between the primary and secondary detergent additives during storage there is a need for a granulate with high physical strength, and for a. corresponding method of production, which is easily controllable and adapted for an industrial scale.
  • the filler consists of or comprises inorganic salts.
  • the shell is surrounded by a final dust suppressing coating. This is advantageous in those cases where the shell tends to produce an unacceptable amount of dust.
  • This final dust suppressing coating can also in certain cases serve as a further protective coating.
  • Example 1 is granulated in a Lodige mixer FM 50 with pure water as granulating agent as described in US patent No. 4.106.991, Example 1.
  • the granulate is dried on a fluid bed to a water content below 1% and finally siftet to get a product with particle range 300 ⁇ m to 900 ⁇ m.
  • Example 7 kg of a granulate produced as described in Example 1 with particle size between 300-900 ⁇ m is coated with a layer of glyceryl stearate/palmitate Grindtek MSP 90 (melting point 68°C) and bentonite ASB 350 ECC in the following manner.
  • the granulate is heated to 75-80°C in a 20 1 heat jacketed Lodige mixer which temperature is kept during the whole coating process.
  • the heated granulate is mixed and sprayed with 700 g melted MSP90 followed by a powdering with 1000 g bentonite followed by spraying with 210 g* * MSP90 followed by powdering with 1000 g MSP90 followed by spraying with 210 g MSP90.
  • the granulate is finally cooled to room temperature on a fluid bed and siftet between 300 and 1000 ⁇ m.
  • a granulate with an inner core containing an optical brightener and an outer shell containing a proteolytic enzyme with the core and the shell separated by a protective layer is produced in the following manner.
  • the granulate is finally dried to a water content below 1% and siftet between 300 and 1000 ⁇ m.
  • Example 3 7 kg of granulate as produced as described in Example 3 is coated with a layer of sodium thiosulphate and kaolin by a conventionel fluid bed coating process.
  • 280 g sodium thiosulphate and 280 g kaolin SPESWHITE ECC are dissolved/dispersed in 1000 g of water and sprayed onto the 7 kg of granulate in a Glatt WSG 5 fluid bed with continuous layering and drying.
  • the granulate has a proteolytic activity of 5.2 KNPU/g.
  • the stability test is made at a temperature of 37°C and a humidity of 70%.
  • a granulate with an inner core containing TAED and 5 an outer shell containing a proteolytic enzyme with the core and the shell separated by a protective layer was produced in the following manner.
  • the shell was supplied with a continuous self- regulating loss-in-weight powder dosing system with a powder dosing rate of 20 kg/h and with a total of 2.6 kg of an

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

Le granulé à additifs détergents décrit comprend un noyau avec un additif détergent primaire entouré par une enveloppe comprenant un additif détergent secondaire, un liant et des agents de granulation, ainsi qu'éventuellement une charge, une couche de revêtement protectrice étant en outre placée entre le noyau et l'enveloppe. L'enveloppe comprend des fibres de cellulose ou des fibres artificielles et le noyau comprend facultativement des fibres de cellulose ou des fibres artificielles. Le granulé à additifs détergents présente une résistance physique élevée et les additifs détergents primaire et secondaire sont séparés l'un de l'autre et/ou des facteurs environnants nocifs. Le granulé à additifs détergents est produit par introduction de ses composants dans un tambour de granulation. Ce procédé de production est facilement commandable et est adapté pour être appliqué à une échelle industrielle.
EP90903319A 1989-02-20 1990-02-16 Granule a additifs detergents et procede de production d'un tel granule Expired EP0458845B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DK078089A DK78089D0 (da) 1989-02-20 1989-02-20 Detergentholdigt granulat og fremgangsmaade til fremstilling deraf
DK780/89 1989-02-20

Publications (2)

Publication Number Publication Date
EP0458845A1 true EP0458845A1 (fr) 1991-12-04
EP0458845B1 EP0458845B1 (fr) 1992-12-23

Family

ID=8097473

Family Applications (1)

Application Number Title Priority Date Filing Date
EP90903319A Expired EP0458845B1 (fr) 1989-02-20 1990-02-16 Granule a additifs detergents et procede de production d'un tel granule

Country Status (7)

Country Link
EP (1) EP0458845B1 (fr)
JP (1) JP2801395B2 (fr)
AT (1) ATE83797T1 (fr)
DE (1) DE69000662T2 (fr)
DK (2) DK78089D0 (fr)
ES (1) ES2036904T3 (fr)
WO (1) WO1990009428A1 (fr)

Cited By (20)

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WO2002061427A1 (fr) 2001-01-31 2002-08-08 Novozymes A/S Procede d'analyse d'une composition granulaire par fluorimetrie
WO2003080827A2 (fr) 2002-03-27 2003-10-02 Novozymes A/S Granules a enrobages filamenteux
WO2004033083A2 (fr) 2002-10-09 2004-04-22 Novozymes A/S Procede destine a ameliorer des compositions particulaires
WO2004067739A2 (fr) 2003-01-27 2004-08-12 Novozymes A/S Stabilisation de granules
WO2007098756A1 (fr) 2006-03-02 2007-09-07 Novozymes A/S Procédé d'encapsulation haute capacité
WO2008017661A1 (fr) 2006-08-07 2008-02-14 Novozymes A/S Granules d'enzyme pour alimentation animale
WO2009118329A1 (fr) 2008-03-28 2009-10-01 Novozymes A/S Système à libération déclenchée
EP2143338A1 (fr) 2004-09-27 2010-01-13 Novozymes A/S Granules d'enzyme
WO2011000924A1 (fr) 2009-07-03 2011-01-06 Abbott Products Gmbh Amylase séchée par pulvérisation, préparations pharmaceutiques la comprenant et son utilisation
WO2011098579A1 (fr) 2010-02-12 2011-08-18 University Of Newcastle Upon Tyne Composés à base de désoxyribonucléase batérienne et méthodes pour la désintégration et la prévention d'un biofilm
EP2537918A1 (fr) 2011-06-20 2012-12-26 The Procter & Gamble Company Produits de consommation avec particules enrobées comprenant une lipase
US8802087B2 (en) 2004-03-22 2014-08-12 Abbott Products Gmbh Pharmaceutical compositions of lipase-containing products, in particular of pancreation
US9198871B2 (en) 2005-08-15 2015-12-01 Abbott Products Gmbh Delayed release pancreatin compositions
EP3072399A1 (fr) 2006-08-07 2016-09-28 Novozymes A/S Granules d'enzyme pour alimentation animale
WO2017102477A1 (fr) * 2015-12-18 2017-06-22 Henkel Ag & Co. Kgaa Procédé de lavage à étapes multiples
US10072256B2 (en) 2006-05-22 2018-09-11 Abbott Products Gmbh Process for separating and determining the viral load in a pancreatin sample
WO2020053238A1 (fr) 2018-09-11 2020-03-19 Novozymes A/S Granulés stables pour compositions d'alimentation
US10704037B2 (en) 2005-07-29 2020-07-07 Abbott Products Gmbh Processes for the manufacture and use of pancreatin
US11266607B2 (en) 2005-08-15 2022-03-08 AbbVie Pharmaceuticals GmbH Process for the manufacture and use of pancreatin micropellet cores
WO2022074166A1 (fr) 2020-10-07 2022-04-14 Novozymes A/S Nouveaux granulés pour l'alimentation d'animaux

Families Citing this family (110)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4322229A1 (de) * 1993-07-05 1995-01-12 Cognis Bio Umwelt Umhüllte Enzymzubereitung für Wasch- und Reinigungsmittel
KR100413241B1 (ko) * 1995-05-29 2004-03-30 가오가부시끼가이샤 효소함유조립물및그제조방법
DE19524287A1 (de) * 1995-07-06 1997-01-09 Henkel Kgaa Von Staub- und Feinanteilen freie granulare Wasch- und Reinigungsmittel hoher Schüttdichte
DE19545729A1 (de) 1995-12-08 1997-06-12 Henkel Kgaa Bleich- und Waschmittel mit enzymatischem Bleichsystem
GB2339575A (en) * 1998-07-15 2000-02-02 Procter & Gamble Cellulose disintegrant for detergent compositions
CN1312280C (zh) * 1999-07-09 2007-04-25 诺沃奇梅兹有限公司 一种制备含酶颗粒的方法
US6933141B1 (en) 1999-10-01 2005-08-23 Novozymes A/S Enzyme granulate
IT1319655B1 (it) 2000-11-15 2003-10-23 Eurand Int Microsfere di enzimi pancreatici con elevata stabilita' e relativometodo di preparazione.
US20050085406A1 (en) 2001-12-21 2005-04-21 Novozymes A/S Salt coatings
PL1807498T3 (pl) † 2004-11-02 2013-04-30 Henkel Ag & Co Kgaa Sposób wytwarzania granulatów bądź aglomeratów środków piorących lub czyszczących
US8246950B2 (en) 2007-02-20 2012-08-21 Aptalis Pharma Limited Stable digestive enzyme compositions
WO2009109856A2 (fr) 2008-03-07 2009-09-11 Axcan Pharma Inc. Procédé pour détecter un parvovirus infectieux dans des préparations pharmaceutiques
EP2216393B1 (fr) 2009-02-09 2024-04-24 The Procter & Gamble Company Composition de détergent
UA111726C2 (uk) 2010-10-01 2016-06-10 Апталіс Фарма Лімітед Препарат панкреліпази низької сили з кишковорозчинним покриттям
EP2732018B1 (fr) 2011-07-12 2017-01-04 Novozymes A/S Granules d'enzyme stables au stockage
CA2843556A1 (fr) 2011-08-08 2013-02-14 Aptalis Pharma Ltd. Procede de test de dissolution de compositions solides contenant des enzymes digestives
EP2674475A1 (fr) 2012-06-11 2013-12-18 The Procter & Gamble Company Composition détergente
WO2014200658A1 (fr) 2013-06-13 2014-12-18 Danisco Us Inc. Alpha-amylase issue de promicromonospora vindobonensis
WO2014200657A1 (fr) 2013-06-13 2014-12-18 Danisco Us Inc. Alpha-amylase provenant destreptomyces xiamenensis
WO2014200656A1 (fr) 2013-06-13 2014-12-18 Danisco Us Inc. Alpha-amylase provenant de streptomyces umbrinus
EP3011020A1 (fr) 2013-06-17 2016-04-27 Danisco US Inc. Alpha-amylase issue d'un membre de la famille des bacillaceae
MX2016001593A (es) 2013-08-09 2016-09-29 Allergan Pharmaceuticals Int Ltd Composicion de enzima digestiva adecuada para administracion enterica.
US20160177240A1 (en) * 2013-08-28 2016-06-23 Novozymes A/S Enzyme Granule with Fluorescent Whitening Agent
WO2015050724A1 (fr) 2013-10-03 2015-04-09 Danisco Us Inc. Alpha-amylases faisant partie d'un sous-ensemble d'exiguobacterium, et procédés d'utilisation correspondants
US20160160199A1 (en) 2013-10-03 2016-06-09 Danisco Us Inc. Alpha-amylases from exiguobacterium, and methods of use, thereof
MX2016006489A (es) 2013-11-20 2016-08-03 Danisco Us Inc Alfa-amilasas variantes que tienen susceptibilidad reducida a la escision por proteasas y metodos de uso.
JP2017519490A (ja) 2014-06-19 2017-07-20 アプタリス ファルマ リミテッド 膵臓抽出物からのウイルス汚染の除去方法
EP3181670B1 (fr) 2015-12-17 2019-01-30 The Procter and Gamble Company Composition de detergent de lave-vaisselle automatique
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EP4638724A1 (fr) 2022-12-19 2025-10-29 Novozymes A/S Polypeptides de la famille 1 d'estérase de glucide (ce1) présentant une activité d'estérase d'acide férulique et/ou d'estérase d'acétyl xylane et polynucléotides codant pour ceux-ci
EP4638684A1 (fr) 2022-12-21 2025-10-29 Novozymes A/S Protéase recombinante pour détachement cellulaire
CN120476196A (zh) 2022-12-21 2025-08-12 诺维信公司 用于细胞分离的微生物蛋白酶
EP4389865A1 (fr) 2022-12-21 2024-06-26 Novozymes A/S Protéase recombinante pour le détachement cellulaire
WO2024175631A1 (fr) 2023-02-22 2024-08-29 Novozymes A/S Composition de soins buccodentaires comprenant une invertase
AU2024325961A1 (en) 2023-08-15 2026-01-29 Novozymes A/S Polypeptides having alkaline phosphatase activity for animal feed
WO2025103765A1 (fr) 2023-11-17 2025-05-22 Novozymes A/S Monooxygénases polysaccharidiques lytiques et leur utilisation dans un détergent
WO2025111274A2 (fr) 2023-11-20 2025-05-30 Novozymes A/S Variants d'épimérase et polynucléotides les codant
AU2024391409A1 (en) 2023-11-30 2026-04-23 Novozymes A/S Oral care composition comprising peptidase or lactonase
WO2025114053A1 (fr) 2023-11-30 2025-06-05 Novozymes A/S Biopolymères destinés à être utilisés dans un détergent
WO2025128568A1 (fr) 2023-12-11 2025-06-19 Novozymes A/S Composition et son utilisation pour augmenter la solubilisation de fibres hémicellulosiques
WO2025191164A2 (fr) 2024-03-12 2025-09-18 Novozymes A/S Utilisation de chymopapaïne dans le détachement de cellules
WO2025196175A1 (fr) 2024-03-22 2025-09-25 Novozymes A/S Compositions de soins bucco-dentaires comprenant des dnases
WO2025217017A1 (fr) 2024-04-08 2025-10-16 Novozymes A/S Compositions et procédés pour augmenter la disponibilité du phosphore
WO2025257254A1 (fr) 2024-06-12 2025-12-18 Novozymes A/S Lipases et variants de lipase et leur utilisation
WO2026068782A1 (fr) 2024-09-30 2026-04-02 Novozymes A/S Variants de protéase et polynucléotides codant pour ceux-ci

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WO2002061427A1 (fr) 2001-01-31 2002-08-08 Novozymes A/S Procede d'analyse d'une composition granulaire par fluorimetrie
WO2003080827A2 (fr) 2002-03-27 2003-10-02 Novozymes A/S Granules a enrobages filamenteux
WO2004033083A2 (fr) 2002-10-09 2004-04-22 Novozymes A/S Procede destine a ameliorer des compositions particulaires
WO2004067739A2 (fr) 2003-01-27 2004-08-12 Novozymes A/S Stabilisation de granules
US8802087B2 (en) 2004-03-22 2014-08-12 Abbott Products Gmbh Pharmaceutical compositions of lipase-containing products, in particular of pancreation
EP2258209A1 (fr) 2004-09-27 2010-12-08 Novozymes A/S Granules d'enzyme
EP2143338A1 (fr) 2004-09-27 2010-01-13 Novozymes A/S Granules d'enzyme
EP2143339A1 (fr) 2004-09-27 2010-01-13 Novozymes A/S Granules d'enzyme
EP2160950A1 (fr) 2004-09-27 2010-03-10 Novozymes A/S Granules d'enzyme
DE202005021811U1 (de) 2004-09-27 2010-04-15 Novozymes A/S Körnchen mit einem Kern und einer Beschichtung
DE202005021810U1 (de) 2004-09-27 2010-04-22 Novozymes A/S Körnchen mit einem Kern und einer Beschichtung
US10704037B2 (en) 2005-07-29 2020-07-07 Abbott Products Gmbh Processes for the manufacture and use of pancreatin
US9198871B2 (en) 2005-08-15 2015-12-01 Abbott Products Gmbh Delayed release pancreatin compositions
US11266607B2 (en) 2005-08-15 2022-03-08 AbbVie Pharmaceuticals GmbH Process for the manufacture and use of pancreatin micropellet cores
WO2007098756A1 (fr) 2006-03-02 2007-09-07 Novozymes A/S Procédé d'encapsulation haute capacité
US10072256B2 (en) 2006-05-22 2018-09-11 Abbott Products Gmbh Process for separating and determining the viral load in a pancreatin sample
WO2008017661A1 (fr) 2006-08-07 2008-02-14 Novozymes A/S Granules d'enzyme pour alimentation animale
EP3072399A1 (fr) 2006-08-07 2016-09-28 Novozymes A/S Granules d'enzyme pour alimentation animale
US10557108B2 (en) 2008-03-28 2020-02-11 Novozymes A/S Triggered release system
WO2009118329A1 (fr) 2008-03-28 2009-10-01 Novozymes A/S Système à libération déclenchée
WO2011000924A1 (fr) 2009-07-03 2011-01-06 Abbott Products Gmbh Amylase séchée par pulvérisation, préparations pharmaceutiques la comprenant et son utilisation
WO2011098579A1 (fr) 2010-02-12 2011-08-18 University Of Newcastle Upon Tyne Composés à base de désoxyribonucléase batérienne et méthodes pour la désintégration et la prévention d'un biofilm
WO2013003025A1 (fr) 2011-06-20 2013-01-03 The Procter & Gamble Company Produits de consommation à base de lipase comprenant des particules enrobées
EP2537918A1 (fr) 2011-06-20 2012-12-26 The Procter & Gamble Company Produits de consommation avec particules enrobées comprenant une lipase
WO2017102477A1 (fr) * 2015-12-18 2017-06-22 Henkel Ag & Co. Kgaa Procédé de lavage à étapes multiples
WO2020053238A1 (fr) 2018-09-11 2020-03-19 Novozymes A/S Granulés stables pour compositions d'alimentation
WO2022074166A1 (fr) 2020-10-07 2022-04-14 Novozymes A/S Nouveaux granulés pour l'alimentation d'animaux

Also Published As

Publication number Publication date
DK0458845T3 (da) 1993-03-29
ATE83797T1 (de) 1993-01-15
DE69000662D1 (de) 1993-02-04
JP2801395B2 (ja) 1998-09-21
ES2036904T3 (es) 1993-06-01
EP0458845B1 (fr) 1992-12-23
JPH04503369A (ja) 1992-06-18
DK78089D0 (da) 1989-02-20
DE69000662T2 (de) 1993-04-22
WO1990009428A1 (fr) 1990-08-23

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