EP1725706A2 - Procede pour mettre en suspension et introduire des substances solides dans des processus haute pression - Google Patents
Procede pour mettre en suspension et introduire des substances solides dans des processus haute pressionInfo
- Publication number
- EP1725706A2 EP1725706A2 EP05735864A EP05735864A EP1725706A2 EP 1725706 A2 EP1725706 A2 EP 1725706A2 EP 05735864 A EP05735864 A EP 05735864A EP 05735864 A EP05735864 A EP 05735864A EP 1725706 A2 EP1725706 A2 EP 1725706A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- suspension
- pressure
- pressure process
- fluid
- solid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract 35
- 239000007787 solid Substances 0.000 title claims abstract 9
- 239000000725 suspension Substances 0.000 claims abstract 24
- 239000012530 fluid Substances 0.000 claims abstract 7
- 239000007788 liquid Substances 0.000 claims abstract 7
- 239000007789 gas Substances 0.000 claims 3
- 239000000126 substance Substances 0.000 claims 3
- 239000000203 mixture Substances 0.000 claims 2
- 125000002015 acyclic group Chemical group 0.000 claims 1
- 239000002318 adhesion promoter Substances 0.000 claims 1
- 150000001298 alcohols Chemical class 0.000 claims 1
- 150000001299 aldehydes Chemical class 0.000 claims 1
- 239000007844 bleaching agent Substances 0.000 claims 1
- 125000004122 cyclic group Chemical group 0.000 claims 1
- 239000007792 gaseous phase Substances 0.000 claims 1
- 229930195733 hydrocarbon Natural products 0.000 claims 1
- 150000002430 hydrocarbons Chemical class 0.000 claims 1
- 150000002576 ketones Chemical class 0.000 claims 1
- 239000007791 liquid phase Substances 0.000 claims 1
- 235000019645 odor Nutrition 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 239000003086 colorant Substances 0.000 abstract 1
- 239000000049 pigment Substances 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/94—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dyes dissolved in solvents which are in the supercritical state
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
- D06B23/20—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
- D06B23/205—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation for adding or mixing constituents of the treating material
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
- D06B23/20—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
Definitions
- the suspension of the solid is carried out in a completely separated suspension process at low pressure.
- the solid is suspended in a non-critical and liquefied gas or partially dissolved.
- the pressure in this suspension process is less than 90% of the critical pressure of the liquefied gas.
- the entry of the suspension in the high pressure process by means of a pump.
- DE 199 28 405 is directed to a process for dyeing a textile substrate in at least one supercritical fluid, wherein a dosing is disclosed which divides the required amount of dye for the dyeing dye on a plurality of subsets and each dye subset for so long with the supercritical fluid in contact until it is dissolved or dispersed.
- the disclosed device provides an oscillating and two-sided piston, which is guided transversely to and through the process line of the critical fluid. This piston absorbs solid in one end position in a first bore, and in the other end position, this first bore is located in the main flow of the critical fluid, so that there the solid is washed out of the bore.
- a second bore is filled or emptied in reverse order at the other end of the piston.
- a disadvantage of the method presented in DE 19928405 and the device disclosed for this purpose is that the device must be designed and dimensioned for the same pressures as the main process. Furthermore, supercritical gas is trapped in the emptied and mainstream bore and guided into the filling position, so that either the same or a higher pressure must be present here or a relaxation takes place each time, which hinders the rapid filling process. that would. Another critical factor is certainly driving over a high-pressure seal with the bores guided through the piston. Damage to the sealing material and thus sealing problems are to be expected here after short periods of use. From WO 97/13915 a very common entry method for solids in ü berkritica process is described.
- the dye is provided in a dye formulation vessel which is located in a bypass to the main process.
- the corresponding valves are opened and the solids are entrained by means of a partial volume flow of the main process fluid.
- a constant dosage or targeted control of the dye supply is thus not possible because the fluid-solid mixture is diluted by the inflowing process fluid.
- all components of this by-pass method must meet the pressure and temperature requirements of the main process.
- a method optimized in comparison with the suspension method known from WO 97/13915 is described in US Pat. No. 6,261,326. In this method, an agitator is arranged in the dye-selling vessel for dissolving or suspending the solid or pumped by means of a pump, a subset in a circle.
- this preparation process there is a critical or an almost critical fluid state, since this preparation process from the main process, the treatment process, is supplied with supercritical fluid. As in the above-mentioned methods, this preparation method also suffers from the defect that it has to satisfy the high-pressure conditions of the main process, here called the treatment method. Furthermore, the entry of the solid, which is not shown in US Pat. No. 6,261,326, must take place via an expensive lock, or the solids feed containers must likewise be designed for the high pressure of the treatment process.
- the object of the invention was therefore to provide a suspension and solids introduction process which operates independently and more economically from the cycle of the high-pressure process than the processes from the prior art.
- the invention solves the problem by means of a method for suspension and
- This process represents a suspension stage of the high pressure Process is and is formed of a suspension tank and a device for fluid circulation and supply and discharge lines.
- the suspension container in a first step is filled with a solid and a fluid, wherein the fluid used is a liquefied gas which is in a non-critical state.
- the solid is suspended in the fluid by means of a fluid circulation device and kept in suspension.
- the liquid circulation device is ideally configured as a stirrer or as a pump arranged outside of the suspension container, which is connected via a suction and a pressure line to the suspension container and promotes a subset of the suspension continuously in a circle.
- the pressure in the suspension stage is advantageously less than 90% of the critical pressure of the gas used and is ideally less than 60 bar.
- the temperature is adjusted such that a gaseous phase is present above the liquid phase.
- the suspension is conveyed by means of a pump in the high-pressure process.
- a pump in the high-pressure process.
- the fluid used for the suspension is substantially chemically identical to the process medium of the high pressure process.
- the fluid is mixed with other substances.
- substances are, for example, cyclic and short-chain acyclic hydrocarbons or short-chain alcohols, aldehydes or ketones, and H 2 O and mixtures of these aforementioned substances.
- the pressure in the suspension vessel during the introduction of the suspension in the high-pressure process is kept constant in the inventive method by gas is nachge devist in gaseous state.
- the volume flow and thus the concentration of the solid in the fluid in a constant size or variable over the conveyor - power of the pump can be adjusted.
- the concentration in the suspension tank is substantially constant during the emptying, since the nachge deviste gas is not liquid, but is gaseous.
- the solid is a substance to be dissolved in the high-pressure process, such as, for example, dye particles, adhesion promoters, bleaching agents, flavors, odorous substances or mixtures thereof.
- an advantage of the invention is the fact that the solid is not dissolved as in the prior art, but only suspended and the specific solubility of the respective starting materials need not be met in the suspension stage. Rather, these substances dissolve in the introduction into the large volume flow of the main process due to the high concentration gradient directly.
- an advantageous embodiment of the invention is that the suspension stream is set at the initiation into the high-pressure process such that the ratio of the volume flows of suspension to Hochlichreamedi- to smaller than 1:50 and ideally equal to or less than 1: 100.
- the very low suspension flow in relation to the main process volume flow has a negligible physical influence on the main process as a rule.
- Fig. 1 shows the suspension process with a pump as wellsstechniksum stiilzaggregat and Figure 2 shows the method with a stirrer without external Ummélznikank.
- the suspension process 1 which is connected via the conduction path 6 with the high-pressure process 4, consisting essentially of the suspension vessel 2 and the pump 3 is formed.
- the suspension vessel 2 is filled via the conduit 7 with liquefied gas and via the conduit 8 with the solid.
- a liquid volume 2 a and a gas volume 2 b form in the suspension container 2.
- a further embodiment of the method can be seen, wherein in the suspension vessel 2, a stirrer 13 is arranged, by means of which the suspension is generated and kept stable.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Pipeline Systems (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Processing Of Solid Wastes (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL05735864T PL1725706T3 (pl) | 2004-03-17 | 2005-03-16 | Sposób przeprowadzania w zawiesinę i wprowadzania substancji stałych do procesu wysokociśnieniowego |
| SI200531554T SI1725706T1 (sl) | 2004-03-17 | 2005-03-16 | Postopek za odmerjanje in vpeljevanje trdne snovi v visokotlaäśni postopek |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102004013338A DE102004013338A1 (de) | 2004-03-17 | 2004-03-17 | Verfahren zur Suspendierung und Einspeisung von Feststoffen in einen Hochdruckprozeß |
| PCT/DE2005/000491 WO2005090667A2 (fr) | 2004-03-17 | 2005-03-16 | Procede pour mettre en suspension et introduire des substances solides dans des processus haute pression |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EP1725706A2 true EP1725706A2 (fr) | 2006-11-29 |
| EP1725706B1 EP1725706B1 (fr) | 2012-05-02 |
Family
ID=34972410
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP05735864A Expired - Lifetime EP1725706B1 (fr) | 2004-03-17 | 2005-03-16 | Procede pour mettre en suspension et introduire des substances solides dans des processus haute pression |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US20080034509A1 (fr) |
| EP (1) | EP1725706B1 (fr) |
| JP (1) | JP4917532B2 (fr) |
| KR (1) | KR101337155B1 (fr) |
| CN (1) | CN101001988B (fr) |
| AT (1) | ATE556168T1 (fr) |
| AU (1) | AU2005224953A1 (fr) |
| CA (1) | CA2559316A1 (fr) |
| DE (2) | DE102004013338A1 (fr) |
| ES (1) | ES2386358T3 (fr) |
| MA (1) | MA28511B1 (fr) |
| PL (1) | PL1725706T3 (fr) |
| PT (1) | PT1725706E (fr) |
| RU (1) | RU2353722C2 (fr) |
| SI (1) | SI1725706T1 (fr) |
| UA (1) | UA83735C2 (fr) |
| WO (1) | WO2005090667A2 (fr) |
| ZA (1) | ZA200607729B (fr) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102018222883A1 (de) | 2017-12-22 | 2019-06-27 | Thyssenkrupp Ag | Vorrichtung und Verfahren zum kontinuierlichen Hochdruckbehandeln von Schüttgut sowie Verwendung |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102004013338A1 (de) | 2004-03-17 | 2005-10-06 | Uhde High Pressure Technologies Gmbh | Verfahren zur Suspendierung und Einspeisung von Feststoffen in einen Hochdruckprozeß |
| CN104032603A (zh) * | 2014-05-16 | 2014-09-10 | 江苏美罗家用纺织品有限公司 | 无水低能耗新型染色工艺 |
| US11291931B2 (en) | 2014-12-15 | 2022-04-05 | Akadeum Life Sciences, Inc. | Method and system for buoyant separation |
| EP3820588A4 (fr) | 2018-07-09 | 2022-04-06 | Akadeum Life Sciences, Inc. | Système et procédé pour le traitement de particules flottantes |
| WO2023028329A1 (fr) | 2021-08-26 | 2023-03-02 | Akadeum Life Sciences, Inc. | Procédé et système pour séparation flottante |
| US12196754B2 (en) | 2022-04-01 | 2025-01-14 | Akadeum Life Sciences, Inc. | Method and system for buoyant-particle-assisted cell therapy |
| CN121511103A (zh) | 2023-02-14 | 2026-02-10 | 爱卡德姆生命科学公司 | 用于部分或完全自动化的浮力辅助分离的方法和系统 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3608742A1 (de) * | 1986-03-15 | 1987-09-17 | Mtm Obermaier Gmbh & Co Kg | Verfahren zum faerben von tier-, pflanzen- oder kunststoffasern |
| IT1197070B (it) * | 1986-08-06 | 1988-11-25 | Foscama Biomed Chim Farma | Procedimento ed impianto per la produzione in continuo di fruttosio-1,6-difosfato mediante utilizzazione di lievito di birra immobilizzato |
| US5308648A (en) * | 1992-09-30 | 1994-05-03 | Union Carbide Chemicals & Plastics Technology Corporation | Spray application of plastics additives to polymers |
| DE19631603A1 (de) * | 1995-10-06 | 1997-04-10 | Amann & Soehne | Verfahren zum Färben eines textilen Substrates |
| ES2135246T3 (es) * | 1995-10-16 | 1999-10-16 | Krupp Uhde Gmbh | Procedimiento y dispositivo para el tratamiento de substratos textiles con fluido supercritico. |
| SE517099E (sv) * | 1996-04-17 | 2004-07-13 | Kvaerner Pulping Tech | System innefattande två pumpar för matning av en sspension till ett tryckkärl |
| US5938794A (en) * | 1996-12-04 | 1999-08-17 | Amann & Sohne Gmbh & Co. | Method for the dyeing of yarn from a supercritical fluid |
| JPH10192670A (ja) * | 1996-12-27 | 1998-07-28 | Inoue Seisakusho:Kk | 超臨界状態を用いた分散方法及び分散装置 |
| US6039470A (en) * | 1997-03-24 | 2000-03-21 | Conwell; Allyn B. | Particulate mixing system |
| JP3645417B2 (ja) * | 1998-04-08 | 2005-05-11 | 三菱化学株式会社 | 液体の移送方法 |
| DE19928405A1 (de) * | 1999-06-22 | 2000-12-28 | Amann & Soehne | Verfahren zum Färben eines textilen Substrates in mindestens einem überkritischen Fluid sowie Färbevorrichtung |
| US6261326B1 (en) * | 2000-01-13 | 2001-07-17 | North Carolina State University | Method for introducing dyes and other chemicals into a textile treatment system |
| US6621326B1 (en) * | 2000-10-26 | 2003-09-16 | Altera Corporation | P-channel negative pumps |
| RU2212482C2 (ru) * | 2001-07-26 | 2003-09-20 | Общество с ограниченной ответственностью "Новые текстильные технологии" | Способ нанесения печатного изображения на тканый материал |
| DE102004013338A1 (de) | 2004-03-17 | 2005-10-06 | Uhde High Pressure Technologies Gmbh | Verfahren zur Suspendierung und Einspeisung von Feststoffen in einen Hochdruckprozeß |
-
2004
- 2004-03-17 DE DE102004013338A patent/DE102004013338A1/de not_active Withdrawn
-
2005
- 2005-03-16 KR KR1020067018903A patent/KR101337155B1/ko not_active Expired - Fee Related
- 2005-03-16 AT AT05735864T patent/ATE556168T1/de active
- 2005-03-16 ES ES05735864T patent/ES2386358T3/es not_active Expired - Lifetime
- 2005-03-16 DE DE112005001140T patent/DE112005001140A5/de not_active Withdrawn
- 2005-03-16 EP EP05735864A patent/EP1725706B1/fr not_active Expired - Lifetime
- 2005-03-16 CA CA002559316A patent/CA2559316A1/fr not_active Abandoned
- 2005-03-16 JP JP2007503189A patent/JP4917532B2/ja not_active Expired - Fee Related
- 2005-03-16 RU RU2006136418/12A patent/RU2353722C2/ru active
- 2005-03-16 PT PT05735864T patent/PT1725706E/pt unknown
- 2005-03-16 CN CN2005800082551A patent/CN101001988B/zh not_active Expired - Fee Related
- 2005-03-16 PL PL05735864T patent/PL1725706T3/pl unknown
- 2005-03-16 UA UAA200610951A patent/UA83735C2/ru unknown
- 2005-03-16 WO PCT/DE2005/000491 patent/WO2005090667A2/fr not_active Ceased
- 2005-03-16 US US10/593,208 patent/US20080034509A1/en not_active Abandoned
- 2005-03-16 AU AU2005224953A patent/AU2005224953A1/en not_active Abandoned
- 2005-03-16 SI SI200531554T patent/SI1725706T1/sl unknown
-
2006
- 2006-09-15 ZA ZA200607729A patent/ZA200607729B/xx unknown
- 2006-10-02 MA MA29360A patent/MA28511B1/fr unknown
Non-Patent Citations (1)
| Title |
|---|
| See references of WO2005090667A2 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102018222883A1 (de) | 2017-12-22 | 2019-06-27 | Thyssenkrupp Ag | Vorrichtung und Verfahren zum kontinuierlichen Hochdruckbehandeln von Schüttgut sowie Verwendung |
| DE102018222881A1 (de) | 2017-12-22 | 2019-06-27 | Thyssenkrupp Ag | Vorrichtung und Verfahren zum kontinuierlichen Hochdruckbehandeln von Schüttgut sowie Verwendung |
| DE102018222874A1 (de) | 2017-12-22 | 2019-06-27 | Thyssenkrupp Ag | Vorrichtung und Verfahren zum kontinuierlichen Hochdruckbehandeln von Schüttgut sowie Verwendung |
Also Published As
| Publication number | Publication date |
|---|---|
| MA28511B1 (fr) | 2007-04-03 |
| KR101337155B1 (ko) | 2013-12-05 |
| RU2006136418A (ru) | 2008-04-27 |
| DE102004013338A1 (de) | 2005-10-06 |
| JP2007529692A (ja) | 2007-10-25 |
| WO2005090667A3 (fr) | 2005-11-24 |
| SI1725706T1 (sl) | 2012-10-30 |
| PT1725706E (pt) | 2012-07-23 |
| CA2559316A1 (fr) | 2005-09-29 |
| CN101001988A (zh) | 2007-07-18 |
| RU2353722C2 (ru) | 2009-04-27 |
| UA83735C2 (ru) | 2008-08-11 |
| WO2005090667A2 (fr) | 2005-09-29 |
| KR20070005623A (ko) | 2007-01-10 |
| ES2386358T3 (es) | 2012-08-17 |
| JP4917532B2 (ja) | 2012-04-18 |
| ATE556168T1 (de) | 2012-05-15 |
| AU2005224953A1 (en) | 2005-09-29 |
| PL1725706T3 (pl) | 2012-10-31 |
| US20080034509A1 (en) | 2008-02-14 |
| CN101001988B (zh) | 2010-05-26 |
| EP1725706B1 (fr) | 2012-05-02 |
| DE112005001140A5 (de) | 2007-05-24 |
| ZA200607729B (en) | 2008-06-25 |
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