EP2047313A1 - Procédé de microscopie à balayage laser et concentrateur de faisceaux - Google Patents
Procédé de microscopie à balayage laser et concentrateur de faisceauxInfo
- Publication number
- EP2047313A1 EP2047313A1 EP07786280A EP07786280A EP2047313A1 EP 2047313 A1 EP2047313 A1 EP 2047313A1 EP 07786280 A EP07786280 A EP 07786280A EP 07786280 A EP07786280 A EP 07786280A EP 2047313 A1 EP2047313 A1 EP 2047313A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- laser scanning
- beam combiner
- lasers
- wavelengths
- scanning microscopy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000004621 scanning probe microscopy Methods 0.000 title claims abstract description 7
- 238000000034 method Methods 0.000 title claims abstract description 6
- 239000000835 fiber Substances 0.000 claims abstract description 13
- 238000005516 engineering process Methods 0.000 claims description 5
- 230000008878 coupling Effects 0.000 claims description 4
- 238000010168 coupling process Methods 0.000 claims description 4
- 238000005859 coupling reaction Methods 0.000 claims description 4
- 239000013307 optical fiber Substances 0.000 claims description 3
- 239000010409 thin film Substances 0.000 claims description 3
- 239000003365 glass fiber Substances 0.000 claims description 2
- 230000003287 optical effect Effects 0.000 abstract description 6
- 238000002347 injection Methods 0.000 abstract 1
- 239000007924 injection Substances 0.000 abstract 1
- 239000000975 dye Substances 0.000 description 11
- 238000001514 detection method Methods 0.000 description 10
- 230000005284 excitation Effects 0.000 description 9
- 238000010521 absorption reaction Methods 0.000 description 7
- 230000005855 radiation Effects 0.000 description 4
- 210000003128 head Anatomy 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000035939 shock Effects 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- WZSUOQDIYKMPMT-UHFFFAOYSA-N argon krypton Chemical compound [Ar].[Kr] WZSUOQDIYKMPMT-UHFFFAOYSA-N 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000004624 confocal microscopy Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 210000001747 pupil Anatomy 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B21/00—Microscopes
- G02B21/0004—Microscopes specially adapted for specific applications
- G02B21/002—Scanning microscopes
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/64—Fluorescence; Phosphorescence
- G01N21/645—Specially adapted constructive features of fluorimeters
- G01N21/6456—Spatial resolved fluorescence measurements; Imaging
- G01N21/6458—Fluorescence microscopy
Definitions
- a laser scanning system In a laser scanning system lasers of different power classes are used. Furthermore, a laser scanning system is characterized by a large number of variable modules that serve as a detector or for illumination. In Fig. 1, a beam path of a laser scanning microscope is shown schematically.
- An LSM is essentially divided into 4 modules as shown in FIG. 1: light source, scanning module, detection unit and microscope. These modules are described in more detail below. Reference is additionally made to DE19702753A1.
- lasers with different wavelengths are used in one LSM. The choice of the excitation wavelength depends on the absorption properties of the dyes to be investigated.
- the excitation radiation is generated in the light source module. Various lasers are used here (argon, argon krypton, TiSa laser).
- the selection of the wavelengths and the adjustment of the intensity of the required excitation wavelength e.g. through the use of an acousto-optic crystal.
- the laser radiation passes through a fiber or a suitable mirror arrangement in the scan module.
- the laser radiation generated in the light source is focused by means of the diffraction-limited diffraction lens via the scanner, the scanning optics and the tube lens into the specimen.
- the focus scans the sample punctiformly in the x-y direction.
- the pixel dwell times when scanning over the sample are usually in the range of less than one microsecond to several 100 microseconds.
- a confocal detection (descanned detection) of the fluorescent light the light which is emitted from the focal plane (specimen) and from the planes above and below passes through the scanners to a dichroic beam splitter (MD). This separates the fluorescent light from the excitation light. Subsequently, the fluorescent light is focused on a diaphragm (confocal aperture / pinhole), which is located exactly in a plane conjugate to the focal plane. As a result, fluorescent light portions outside the focus are suppressed. By varying the aperture size, the optical resolution of the microscope can be adjusted. Behind the aperture is another dichroic block filter (EF) which again suppresses the excitation radiation.
- EF dichroic block filter
- the fluorescent light is measured by means of a point detector (PMT).
- PMT point detector
- the excitation of dye fluorescence occurs in a small volume where the excitation intensity is particularly high. This area is only marginally larger than the detected area using a confocal array. The use of a confocal aperture can thus be dispensed with and the detection can take place directly after the objective (non-descanned detection).
- a descanned detection also takes place, but this time the pupil of the objective is imaged into the detection unit (nonconfocally descanned detection).
- the plane (optical section) which is located in the focal plane of the objective is reproduced by both detection arrangements in conjunction with the corresponding one-photon absorption or multiphoton absorption.
- a three-dimensional image of the sample can then be generated computer-aided.
- the LSM is therefore suitable for the examination of thick specimens.
- the excitation wavelengths are determined by the dye used with its specific absorption properties. Dichroic filters tuned to the emission characteristics of the dye ensure that only the fluorescent light emitted by the respective dye is measured by the point detector.
- connection of the light source modules with the scan module is usually about
- FIG. 1 The invention is shown schematically in FIG. 1
- Tin encapsulated from telecommunication preferably in TTF
- Thin-film technology is suitable for combining the light of, for example, eight light sources, which are brought in via fibers, and, advantageously via a polarization-maintaining glass fiber, for supplying the microscope (scan head) to an LSM.
- Fig. 3 shows a possible embodiment is shown.
- the solution is a compact, encapsulated, fully adjusted assembly that supports the
- Beam combiner contains.
- the laser sources are coupled via fibers and unified output via a fiber, the input and output fibers are fixed, so that no adjustment of a fiber to Strahlverlick as in the state of
- the invention makes possible a compact construction of a beam combiner with the aid of, for example, one of the cubeo-fiber multiplexer or a comparable component.
- the encapsulated assembly provides a rugged construction that is resistant to
- Fiber connector realized, it is easily possible for the customer, a modular design
Landscapes
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Optics & Photonics (AREA)
- Microscoopes, Condenser (AREA)
Abstract
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102006034909A DE102006034909A1 (de) | 2006-07-28 | 2006-07-28 | Verfahren zur Laser-Scanning-Mikroskopie und Strahlvereiniger |
| PCT/EP2007/006549 WO2008012057A1 (fr) | 2006-07-28 | 2007-07-24 | Procédé de microscopie à balayage laser et concentrateur de faisceaux |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| EP2047313A1 true EP2047313A1 (fr) | 2009-04-15 |
Family
ID=38610631
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP07786280A Withdrawn EP2047313A1 (fr) | 2006-07-28 | 2007-07-24 | Procédé de microscopie à balayage laser et concentrateur de faisceaux |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US20090303584A1 (fr) |
| EP (1) | EP2047313A1 (fr) |
| DE (1) | DE102006034909A1 (fr) |
| WO (1) | WO2008012057A1 (fr) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3538941B1 (fr) | 2016-11-10 | 2025-04-23 | The Trustees of Columbia University in the City of New York | Procédés d'imagerie rapide de grands échantillons à haute résolution |
| US12596243B2 (en) * | 2023-09-06 | 2026-04-07 | National Yang Ming Chiao Tung University | Laser scanning microscope with electrical high-order modulation extraction module |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19633185A1 (de) * | 1996-04-16 | 1997-10-23 | Leica Lasertechnik | Punktlichtquelle für ein Laserscanmikroskop und Verfahren zum Einkoppeln von mindestens zwei Lasern unterschiedlicher Wellenlänge in ein Laserscanmikroskop |
| US20010028031A1 (en) * | 2000-04-04 | 2001-10-11 | Johann Engelhardt | Apparatus for combining light and confocal scanning microscope |
| US20060017001A1 (en) * | 2004-07-23 | 2006-01-26 | Paul Donders | Method and apparatus for fluorescent confocal microscopy |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3343276B2 (ja) * | 1993-04-15 | 2002-11-11 | 興和株式会社 | レーザー走査型光学顕微鏡 |
| JP3258821B2 (ja) * | 1994-06-02 | 2002-02-18 | 三菱電機株式会社 | 微小異物の位置決め方法、分析方法、これに用いる分析装置およびこれを用いた半導体素子もしくは液晶表示素子の製法 |
| US5895915A (en) * | 1997-07-24 | 1999-04-20 | General Scanning, Inc. | Bi-directional scanning system with a pixel clock system |
| JP2000199855A (ja) * | 1998-11-02 | 2000-07-18 | Olympus Optical Co Ltd | 走査型光学顕微鏡装置 |
| US6459484B1 (en) * | 1999-10-21 | 2002-10-01 | Olympus Optical Co., Ltd. | Scanning optical apparatus |
| US6570659B2 (en) * | 2001-03-16 | 2003-05-27 | Lightlab Imaging, Llc | Broadband light source system and method and light source combiner |
| JP2004029205A (ja) * | 2002-06-24 | 2004-01-29 | Olympus Corp | レーザ走査型顕微鏡 |
| US7218446B2 (en) * | 2003-08-27 | 2007-05-15 | Biomedical Photometrics Inc. | Imaging system having a fine focus |
| US7280570B2 (en) * | 2003-12-15 | 2007-10-09 | Leica Microsystems | Device for generating a light beam including multiple wavelengths |
| EP1760454A4 (fr) * | 2004-06-24 | 2008-09-03 | Olympus Corp | Dispositif photométrique fluorescent |
| DE102004030669A1 (de) * | 2004-06-24 | 2006-01-19 | Leica Microsystems Cms Gmbh | Mikroskop |
| US7413341B1 (en) * | 2004-08-16 | 2008-08-19 | The Research Foundation Of State University Of New York | Imaging methods |
| US7352458B2 (en) * | 2005-10-26 | 2008-04-01 | President And Fellows Of Harvard College | System and method for high sensitivity vibrational imaging with frequency modulation coherent anti-stokes Raman scattering analyses |
-
2006
- 2006-07-28 DE DE102006034909A patent/DE102006034909A1/de not_active Withdrawn
-
2007
- 2007-07-24 US US12/375,387 patent/US20090303584A1/en not_active Abandoned
- 2007-07-24 EP EP07786280A patent/EP2047313A1/fr not_active Withdrawn
- 2007-07-24 WO PCT/EP2007/006549 patent/WO2008012057A1/fr not_active Ceased
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19633185A1 (de) * | 1996-04-16 | 1997-10-23 | Leica Lasertechnik | Punktlichtquelle für ein Laserscanmikroskop und Verfahren zum Einkoppeln von mindestens zwei Lasern unterschiedlicher Wellenlänge in ein Laserscanmikroskop |
| US20010028031A1 (en) * | 2000-04-04 | 2001-10-11 | Johann Engelhardt | Apparatus for combining light and confocal scanning microscope |
| US20060017001A1 (en) * | 2004-07-23 | 2006-01-26 | Paul Donders | Method and apparatus for fluorescent confocal microscopy |
Non-Patent Citations (1)
| Title |
|---|
| See also references of WO2008012057A1 * |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2008012057A1 (fr) | 2008-01-31 |
| US20090303584A1 (en) | 2009-12-10 |
| DE102006034909A1 (de) | 2008-01-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
| 17P | Request for examination filed |
Effective date: 20090130 |
|
| AK | Designated contracting states |
Kind code of ref document: A1 Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IS IT LI LT LU LV MC MT NL PL PT RO SE SI SK TR |
|
| AX | Request for extension of the european patent |
Extension state: AL BA HR MK RS |
|
| 17Q | First examination report despatched |
Effective date: 20090519 |
|
| DAX | Request for extension of the european patent (deleted) | ||
| STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN |
|
| RAP1 | Party data changed (applicant data changed or rights of an application transferred) |
Owner name: CARL ZEISS MICROSCOPY GMBH Owner name: CUBE OPTICS AG |
|
| 18D | Application deemed to be withdrawn |
Effective date: 20120411 |