EP2687458A1 - Emballage pour films contenant une dose unitaire d' une substance active. - Google Patents

Emballage pour films contenant une dose unitaire d' une substance active. Download PDF

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Publication number
EP2687458A1
EP2687458A1 EP20120005237 EP12005237A EP2687458A1 EP 2687458 A1 EP2687458 A1 EP 2687458A1 EP 20120005237 EP20120005237 EP 20120005237 EP 12005237 A EP12005237 A EP 12005237A EP 2687458 A1 EP2687458 A1 EP 2687458A1
Authority
EP
European Patent Office
Prior art keywords
packaging
packaging material
material element
sealing
layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
EP20120005237
Other languages
German (de)
English (en)
Inventor
Erfindernennung liegt noch nicht vor Die
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LTS Lohmann Therapie Systeme AG
Original Assignee
LTS Lohmann Therapie Systeme AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by LTS Lohmann Therapie Systeme AG filed Critical LTS Lohmann Therapie Systeme AG
Priority to EP20120005237 priority Critical patent/EP2687458A1/fr
Priority to KR20157000819A priority patent/KR20150032702A/ko
Priority to PL13736824T priority patent/PL2874908T3/pl
Priority to AU2013292245A priority patent/AU2013292245B2/en
Priority to CA2878330A priority patent/CA2878330C/fr
Priority to HK15110625.5A priority patent/HK1209713B/xx
Priority to BR112015000813-5A priority patent/BR112015000813B1/pt
Priority to RU2015105053A priority patent/RU2633954C2/ru
Priority to PCT/EP2013/063922 priority patent/WO2014012787A1/fr
Priority to EP13736824.7A priority patent/EP2874908B1/fr
Priority to ES13736824.7T priority patent/ES2605432T3/es
Priority to CN201380044805.XA priority patent/CN104640781B/zh
Priority to MX2015000790A priority patent/MX351124B/es
Priority to JP2015522029A priority patent/JP6422436B2/ja
Publication of EP2687458A1 publication Critical patent/EP2687458A1/fr
Ceased legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
    • A61J1/00—Containers specially adapted for medical or pharmaceutical purposes
    • A61J1/03—Containers specially adapted for medical or pharmaceutical purposes for pills or tablets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B11/00—Wrapping, e.g. partially or wholly enclosing, articles or quantities of material, in strips, sheets or blanks, of flexible material
    • B65B11/50—Enclosing articles, or quantities of material, by disposing contents between two sheets, e.g. pocketed sheets, and securing their opposed free margins
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B61/00—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages
    • B65B61/18—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages for making package-opening or unpacking elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D75/00—Packages comprising articles or materials partially or wholly enclosed in strips, sheets, blanks, tubes or webs of flexible sheet material, e.g. in folded wrappers
    • B65D75/28—Articles or materials wholly enclosed in composite wrappers, i.e. wrappers formed by associating or interconnecting two or more sheets or blanks
    • B65D75/30—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D75/00—Packages comprising articles or materials partially or wholly enclosed in strips, sheets, blanks, tubes or webs of flexible sheet material, e.g. in folded wrappers
    • B65D75/52—Details
    • B65D75/58—Opening or contents-removing devices added or incorporated during package manufacture
    • B65D75/5805—Opening or contents-removing devices added or incorporated during package manufacture for tearing a side strip parallel and next to the edge, e.g. by means of a line of weakness
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D75/00—Packages comprising articles or materials partially or wholly enclosed in strips, sheets, blanks, tubes or webs of flexible sheet material, e.g. in folded wrappers
    • B65D75/52—Details
    • B65D75/58—Opening or contents-removing devices added or incorporated during package manufacture
    • B65D75/5827—Tear-lines provided in a wall portion

Definitions

  • the invention relates to a package for single-dose active substance-containing films, comprising an upper packaging material element and a lower packaging material element, which are connected to each other by means of a circumferential sealing surface or sealing seam, that an all-round enclosed cavity for receiving the film is formed, wherein the upper packaging material element and the lower packaging material element in the region of the sealing surface or the sealing seam each have at least one section which are congruent, and at least one section is crossed by a fold or crease line.
  • TTS Transdermal Therapeutic Systems
  • TTS consist in the simplest case of a very thin backing layer, a pressure-sensitive adhesive polymer layer containing an active ingredient and optionally a removable protective layer which is removed before the application of the TTS.
  • the backing layer and polymer layer must be very thin, so that no foreign body feeling is created when wearing the TTS. This property makes both layers vulnerable to being damaged when the package is torn open.
  • film-shaped oral dosage forms which consist of only one polymer layer.
  • From the DE 10 2004 047 445 A1 is a non-reclosable package for hazardous products, in particular pharmaceutical products comprising a first packaging material element and a second packaging material element known.
  • the two packaging material elements are arranged one above the other and the packaging has at least a first surface portion, at the edge or edges of the two packaging material elements are releasably connected to each other, wherein between the two packaging material elements at least one side enclosed cavity for receiving the packaged goods is formed.
  • the packaging has at least one second surface section which lies outside or adjoins the first surface section and at the edge or edges of which the two packaging material elements are detachably connected to one another and wherein at least one of the two packaging material elements is provided with at least one structure which extends within the second surface portion and which allows tearing of the packaging material element (s).
  • From the DE 10 2006 041 921 A1 is a package for active substance-containing films, which has a carrier layer and a releasably connected to this cover layer known.
  • the package has in a pairwise arrangement two opposite, separated by a web surface areas within which the cover layer is not connected to the carrier layer, whereby two separate, mutually enclosed spaces for pairwise recording of said films are formed.
  • Within said web there is a further surface area in which the carrier layer is not connected to the cover layer, whereby an all-round enclosed cavity is formed and within the web at least one perforation line is present.
  • the upper packaging material element and the lower packaging material element are releasably (peelably) connected to each other.
  • the two packaging material elements are inseparably connected to each other in single-dose packaging. This is preferably done by a heat seal, but can also be done with any other suitable sealing method such as cold sealing, ultrasonic sealing, laser sealing or similar, known in the art foil welding process, as long as a non-detachable sealing seam is obtained.
  • Such a package is for example from the German patent application DE 10 2009 008 217 A1 known.
  • the user must fold over part of the packaging along an imprinted marking line, in order subsequently to open the packaging at a likewise marked location by tearing along a weakening line.
  • the buckling along the printed marking line changes the position of a structure or a cut in the region of the sealing surface or sealing seam of the two packaging material elements to the edge of the packaging and thus allows tearing of the packaging in order to be able to remove the contents from the cavity.
  • the structure or section has a length of about 3 to 5 mm.
  • the printed marker line preferably crosses the pattern or cut at right angles or at a selected angle.
  • the prior art overlooks the fact that the packaging significantly contributes to the stability of the packaged dosage form, because the packaging protects the dosage form from light, moisture, oxygen and microorganisms.
  • the mentioned weakening line weakens the packaging by causing a gap in the seal because the broken seal allows more moisture and oxygen to diffuse into the interior of the package. It should be noted that both water vapor and oxygen are very small molecules and the storage of the drug before use is at least two years, ideally three years or more.
  • the invention is therefore based on the object to provide a generic single-dose packaging, which improves the embodiments described above.
  • This object is achieved in that the section in the upper packaging material element and the congruent cut in the lower packaging material element is formed so that the respective end point of the cuts has a distance from the cavity, which corresponds at least to the width of the sealed seam.
  • the invention thus provides that the end points of the cuts are at least as far away from the cavity as the maximum width of the remaining sealing seams.
  • Each package has sealed seams on at least three sides that take into account a width to prevent or prevent diffusion for the period of maximum storage.
  • the outer layer is preferably printable, so that e.g. Product labels and tear-open aids can be attached.
  • the middle layer consists of a metal foil, preferably aluminum, with a thickness of 9-25 micrometers. This metal layer ensures the tightness of the packaging against moisture and air.
  • the inner layer is a sealable plastic layer, wherein the sealed seam produced by this layer can not be opened again.
  • the upper packaging material element and the lower packaging material element have an identical structure. This has the advantage that only one type of packaging materials for use and thus a confusion is excluded.
  • An expedient development provides that the section in the upper and the cut in the lower Fackstoflelement in the sealed seam is mounted so that it is aligned at right angles to the nearest outer edge of the cavity. This ensures that the cut comes in contact with the peripheral sealing surface or sealing seam at exactly one point, whereas in the known embodiments there is contact over a longer distance.
  • the upper packaging material element and the lower packaging material element are integrally formed and are thereby folded around a bending edge.
  • connection between the two packaging material elements is preferably produced by sealing or welding. Suitable means and methods for producing the sealing surfaces or the sealing seams are known to the person skilled in the art.
  • the seal serves as a diffusion and permeation barrier and is generally impermeable to active substances and atmospheric moisture. Both heat-sealing and cold-sealing methods are possible.
  • a material for sealing layers for example, hot melt adhesives, sealing paints, sieve dispersions or adhesives can be used.
  • packaging 1 according to the invention is shown in plan view.
  • the packaging 1 is a sealed-edge bag made of an upper packaging material element 3 and a lower packaging material element 4. Between the upper packaging material element 3 and the lower packaging material element 4, an active substance-containing film 2 is arranged in a cavity 6 enclosed on all sides.
  • the cavity 6 is generated by a circumferential sealing surface or sealing seam 5, which connects the two packaging material elements 3, 4 inextricably.
  • the cavity 6 and the mirror surface or sealing seam 5 have a common outer edge 6a.
  • In the sealing surface or sealing seam 5 is located in the upper packaging material element 3, a section 7 and in the lower packaging material element 4 a section 8.
  • the two sections 7 and 8 are congruent.
  • the section 7 is crossed by a fold or crease line 10.
  • An imaginary extension of the sections 7 and 8, which is identical to the tear-open edge, has a distance M3 from the nearest edge of the fuel-containing film 2.
  • the distance M3 is 4 to 5 mm.
  • the upper and lower packaging material element 3, 4 is integrally formed and is folded around a bending edge 17. This eliminates the Siegeinaht 5 in this area.
  • Fig. 2 is the construction of the package in a sectional view along the line A - A in Flg. 1 shown.
  • the individual parts are greatly enlarged and drawn separately to illustrate the structure.
  • the upper packaging material element 3 consists of at least one upper, outer layer 11 and a subsequent upper metal layer 13.
  • the lower packaging material layer 4 likewise consists of a lower, outer, layer 12 and a subsequent lower metal layer 14.
  • the metal layers 13, 14 are preferably made of an aluminum foil having a thickness of 9 to 25 microns. This foil ensures that the inserted Product does not come into contact with air and is not exposed to moisture.
  • the upper or lower packaging material element 3, 4 has a sealable layer 9.
  • the sealable layer 9 can also be applied to both the upper and the lower packaging material elements 3, 4. The sealing surface or sealing seam 5 produced by this layer 9 can not be separated again.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Composite Materials (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Packages (AREA)
  • Medical Preparation Storing Or Oral Administration Devices (AREA)
  • Wrappers (AREA)
  • Bag Frames (AREA)
  • Basic Packing Technique (AREA)
EP20120005237 2012-07-17 2012-07-17 Emballage pour films contenant une dose unitaire d' une substance active. Ceased EP2687458A1 (fr)

Priority Applications (14)

Application Number Priority Date Filing Date Title
EP20120005237 EP2687458A1 (fr) 2012-07-17 2012-07-17 Emballage pour films contenant une dose unitaire d' une substance active.
KR20157000819A KR20150032702A (ko) 2012-07-17 2013-07-02 개별 활성물질 함유 필름을 위한 팩 및 상기 팩의 제조 방법
PL13736824T PL2874908T3 (pl) 2012-07-17 2013-07-02 Opakowanie na dozowane pojedynczo, zawierające substancję czynną listki oraz sposób wytwarzania tego opakowania
AU2013292245A AU2013292245B2 (en) 2012-07-17 2013-07-02 Pack for individual active-substance-containing films, and method for producing said pack
CA2878330A CA2878330C (fr) 2012-07-17 2013-07-02 Emballage pour films unidose contenant une substance active et son procede de fabrication
HK15110625.5A HK1209713B (en) 2012-07-17 2013-07-02 Pack for individual active-substance-containing films, and method for producing said pack
BR112015000813-5A BR112015000813B1 (pt) 2012-07-17 2013-07-02 nova embalagem de dose única
RU2015105053A RU2633954C2 (ru) 2012-07-17 2013-07-02 Упаковка для пленок, содержащих однократно дозируемое действующее вещество, и способ ее изготовления
PCT/EP2013/063922 WO2014012787A1 (fr) 2012-07-17 2013-07-02 Emballage pour films unidose contenant une substance active et son procédé de fabrication
EP13736824.7A EP2874908B1 (fr) 2012-07-17 2013-07-02 Emballage pour films contenant une dose unitaire d' une substance active ainsi que le procédé pour fabriquer cet emballage
ES13736824.7T ES2605432T3 (es) 2012-07-17 2013-07-02 Envase para películas que contienen sustancia activa en dosis unitaria y procedimiento para fabricar este envase
CN201380044805.XA CN104640781B (zh) 2012-07-17 2013-07-02 用于单剂的含活性物质的膜的封装件和用于制造该封装件的方法
MX2015000790A MX351124B (es) 2012-07-17 2013-07-02 Empaque para películas individuales que contienen sustancia activa y método para producir dicho empaque.
JP2015522029A JP6422436B2 (ja) 2012-07-17 2013-07-02 新規な単回用量パッケージング

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP20120005237 EP2687458A1 (fr) 2012-07-17 2012-07-17 Emballage pour films contenant une dose unitaire d' une substance active.

Publications (1)

Publication Number Publication Date
EP2687458A1 true EP2687458A1 (fr) 2014-01-22

Family

ID=46640511

Family Applications (2)

Application Number Title Priority Date Filing Date
EP20120005237 Ceased EP2687458A1 (fr) 2012-07-17 2012-07-17 Emballage pour films contenant une dose unitaire d' une substance active.
EP13736824.7A Active EP2874908B1 (fr) 2012-07-17 2013-07-02 Emballage pour films contenant une dose unitaire d' une substance active ainsi que le procédé pour fabriquer cet emballage

Family Applications After (1)

Application Number Title Priority Date Filing Date
EP13736824.7A Active EP2874908B1 (fr) 2012-07-17 2013-07-02 Emballage pour films contenant une dose unitaire d' une substance active ainsi que le procédé pour fabriquer cet emballage

Country Status (12)

Country Link
EP (2) EP2687458A1 (fr)
JP (1) JP6422436B2 (fr)
KR (1) KR20150032702A (fr)
CN (1) CN104640781B (fr)
AU (1) AU2013292245B2 (fr)
BR (1) BR112015000813B1 (fr)
CA (1) CA2878330C (fr)
ES (1) ES2605432T3 (fr)
MX (1) MX351124B (fr)
PL (1) PL2874908T3 (fr)
RU (1) RU2633954C2 (fr)
WO (1) WO2014012787A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022152881A1 (fr) * 2021-01-15 2022-07-21 Lts Lohmann Therapie-Systeme Ag Assemblage de film orodispersible (otf) par couture

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009008217A1 (de) * 2009-02-10 2010-08-19 Lts Lohmann Therapie-Systeme Ag Kindergesicherte, hochinerte Einzelverpackung
DE102014104692A1 (de) * 2014-04-02 2015-10-08 Huhtamaki Flexible Packaging Germany, Zweigniederlassung Der Huhtamaki Flexible Packaging Germany Gmbh & Co. Kg Verpackung
JP2015217970A (ja) * 2014-05-19 2015-12-07 大日本印刷株式会社 包装体

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3809220A (en) * 1972-07-24 1974-05-07 Becton Dickinson Co Child safety package
US5511665A (en) * 1994-10-31 1996-04-30 G. D. Searle & Co. Child-resistant package
DE102004047445A1 (de) 2004-09-30 2006-04-13 Lts Lohmann Therapie-Systeme Ag Nichtwiederverschließbare Verpackung für gesundheitsgefährdende Erzeugnisse, sowie Verfahren zu deren Herstellung
DE102004062864A1 (de) * 2004-12-21 2006-06-22 Boehringer Ingelheim Pharma Gmbh & Co. Kg Folienbehälter
US20060283747A1 (en) * 2005-06-07 2006-12-21 Gloria Lam Family Partnership, Llc Condiment package with advertising for others
DE102006041921A1 (de) 2006-09-07 2008-03-27 Lts Lohmann Therapie-Systeme Ag Verpackung für wirkstoffhaltige Filme und Verfahren für deren Herstellung
DE102009008217A1 (de) 2009-02-10 2010-08-19 Lts Lohmann Therapie-Systeme Ag Kindergesicherte, hochinerte Einzelverpackung
WO2012084216A1 (fr) * 2010-12-23 2012-06-28 Lts Lohmann Therapie-Systeme Ag Emballage de dose individuelle très étanche

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6199698B1 (en) * 1999-12-03 2001-03-13 Alusuisse Technology & Management, Ltd. Pharmaceutical packaging with separation means
JP3984225B2 (ja) * 2002-02-08 2007-10-03 ザ プロクター アンド ギャンブル カンパニー 子供用安全袋
CA2657689A1 (fr) * 2008-03-27 2009-09-27 Bruce D. Detwiler Emballages dechirables pour produit pharmaceutique, et methode
CN101712384A (zh) * 2008-09-30 2010-05-26 三洋电机株式会社 药品包装机

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3809220A (en) * 1972-07-24 1974-05-07 Becton Dickinson Co Child safety package
US5511665A (en) * 1994-10-31 1996-04-30 G. D. Searle & Co. Child-resistant package
DE102004047445A1 (de) 2004-09-30 2006-04-13 Lts Lohmann Therapie-Systeme Ag Nichtwiederverschließbare Verpackung für gesundheitsgefährdende Erzeugnisse, sowie Verfahren zu deren Herstellung
DE102004062864A1 (de) * 2004-12-21 2006-06-22 Boehringer Ingelheim Pharma Gmbh & Co. Kg Folienbehälter
US20060283747A1 (en) * 2005-06-07 2006-12-21 Gloria Lam Family Partnership, Llc Condiment package with advertising for others
DE102006041921A1 (de) 2006-09-07 2008-03-27 Lts Lohmann Therapie-Systeme Ag Verpackung für wirkstoffhaltige Filme und Verfahren für deren Herstellung
DE102009008217A1 (de) 2009-02-10 2010-08-19 Lts Lohmann Therapie-Systeme Ag Kindergesicherte, hochinerte Einzelverpackung
WO2012084216A1 (fr) * 2010-12-23 2012-06-28 Lts Lohmann Therapie-Systeme Ag Emballage de dose individuelle très étanche

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022152881A1 (fr) * 2021-01-15 2022-07-21 Lts Lohmann Therapie-Systeme Ag Assemblage de film orodispersible (otf) par couture

Also Published As

Publication number Publication date
EP2874908A1 (fr) 2015-05-27
AU2013292245B2 (en) 2016-08-18
EP2874908B1 (fr) 2016-09-07
ES2605432T3 (es) 2017-03-14
JP2015524290A (ja) 2015-08-24
HK1209713A1 (en) 2016-04-08
CA2878330A1 (fr) 2014-01-23
MX2015000790A (es) 2015-05-07
WO2014012787A1 (fr) 2014-01-23
JP6422436B2 (ja) 2018-11-14
RU2633954C2 (ru) 2017-10-19
PL2874908T3 (pl) 2017-05-31
BR112015000813B1 (pt) 2021-01-26
CN104640781B (zh) 2016-11-09
RU2015105053A (ru) 2016-09-10
AU2013292245A1 (en) 2015-02-05
CN104640781A (zh) 2015-05-20
CA2878330C (fr) 2020-04-14
MX351124B (es) 2017-10-02
KR20150032702A (ko) 2015-03-27
BR112015000813A2 (pt) 2017-06-27

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