EP2970678A4 - Uv-reflektierende pigmente und verfahren zur herstellung und verwendung davon - Google Patents

Uv-reflektierende pigmente und verfahren zur herstellung und verwendung davon

Info

Publication number
EP2970678A4
EP2970678A4 EP14768336.1A EP14768336A EP2970678A4 EP 2970678 A4 EP2970678 A4 EP 2970678A4 EP 14768336 A EP14768336 A EP 14768336A EP 2970678 A4 EP2970678 A4 EP 2970678A4
Authority
EP
European Patent Office
Prior art keywords
making
same
reflecting pigments
pigments
reflecting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP14768336.1A
Other languages
English (en)
French (fr)
Other versions
EP2970678A1 (de
Inventor
Steven Jones
Markus Rueckel
Thomas Servay
Stefan Dahmen
Geoffrey Johnson
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of EP2970678A1 publication Critical patent/EP2970678A1/de
Publication of EP2970678A4 publication Critical patent/EP2970678A4/de
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • C09C1/0024—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings comprising a stack of coating layers with alternating high and low refractive indices, wherein the first coating layer on the core surface has the high refractive index
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/01—Use of inorganic substances as compounding ingredients characterized by their specific function
    • C08K3/013—Fillers, pigments or reinforcing additives
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
    • C09C1/0051—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings comprising a stack of coating layers with alternating low and high refractive indices, wherein the first coating layer on the core surface has the low refractive index
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/82—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/84—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/1004—Interference pigments characterized by the core material the core comprising at least one inorganic oxide, e.g. Al2O3, TiO2 or SiO2
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/1004—Interference pigments characterized by the core material the core comprising at least one inorganic oxide, e.g. Al2O3, TiO2 or SiO2
    • C09C2200/1016—Interference pigments characterized by the core material the core comprising at least one inorganic oxide, e.g. Al2O3, TiO2 or SiO2 comprising an intermediate layer between the core and a stack of coating layers having alternating refractive indices
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/102—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/10—Interference pigments characterized by the core material
    • C09C2200/102—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin
    • C09C2200/1033—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin comprising an intermediate layer between the core and a stack of coating layers having alternating refractive indices
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/30—Interference pigments characterised by the thickness of the core or layers thereon or by the total thickness of the final pigment particle
    • C09C2200/301—Thickness of the core
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/30—Interference pigments characterised by the thickness of the core or layers thereon or by the total thickness of the final pigment particle
    • C09C2200/302—Thickness of a layer with high refractive material
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
    • C09C2200/30—Interference pigments characterised by the thickness of the core or layers thereon or by the total thickness of the final pigment particle
    • C09C2200/303—Thickness of a layer with low refractive material
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2210/00—Special effects or uses of interference pigments
    • C09C2210/20—Optical properties in the UV-range
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2220/00—Methods of preparing the interference pigments
    • C09C2220/10—Wet methods, e.g. co-precipitation
    • C09C2220/106—Wet methods, e.g. co-precipitation comprising only a drying or calcination step of the finally coated pigment
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C2220/00—Methods of preparing the interference pigments
    • C09C2220/20—PVD, CVD methods or coating in a gas-phase using a fluidized bed

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Laminated Bodies (AREA)
  • Cosmetics (AREA)
  • Optical Elements Other Than Lenses (AREA)
  • Surface Treatment Of Glass (AREA)
EP14768336.1A 2013-03-15 2014-03-12 Uv-reflektierende pigmente und verfahren zur herstellung und verwendung davon Withdrawn EP2970678A4 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361793518P 2013-03-15 2013-03-15
US201361902992P 2013-12-16 2013-12-16
PCT/US2014/024381 WO2014150846A1 (en) 2013-03-15 2014-03-12 Uv reflecting pigments, and method of making and using the same

Publications (2)

Publication Number Publication Date
EP2970678A1 EP2970678A1 (de) 2016-01-20
EP2970678A4 true EP2970678A4 (de) 2016-09-21

Family

ID=51521557

Family Applications (1)

Application Number Title Priority Date Filing Date
EP14768336.1A Withdrawn EP2970678A4 (de) 2013-03-15 2014-03-12 Uv-reflektierende pigmente und verfahren zur herstellung und verwendung davon

Country Status (8)

Country Link
US (1) US20140261084A1 (de)
EP (1) EP2970678A4 (de)
JP (1) JP2016519172A (de)
KR (1) KR20150127090A (de)
CN (1) CN105051117A (de)
BR (1) BR112015023311A2 (de)
RU (1) RU2015144081A (de)
WO (1) WO2014150846A1 (de)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020008341A1 (en) 2018-07-03 2020-01-09 3M Innovative Properties Company Infrared reflective wrap film
JP7456728B2 (ja) * 2019-05-09 2024-03-27 ロレアル 日焼け止め用の多層粒子
FR3095777B1 (fr) * 2019-05-09 2023-09-29 Oreal Materiau multicouches pour filtrer les ultraviolets, composition le comprenant, procede de traitement de matieres keratiniques le mettant en œuvre, et procede de preparation du materiau
US20230357986A1 (en) 2020-10-02 2023-11-09 Tmg Tecidos Plastificados E Outros Revestimentos Para A Industria Automovel Sa Breathable layered flexible material, methods and uses thereof
US12147010B2 (en) 2020-12-17 2024-11-19 Eastman Kodak Company Coating providing ultraviolet scattering
US12454622B2 (en) 2020-12-17 2025-10-28 Eastman Kodak Company Coating providing controlled absorption and scattering
US12240957B2 (en) 2020-12-17 2025-03-04 Eastman Kodak Company Method for fabricating impermeable porous particles
US12428566B2 (en) 2020-12-17 2025-09-30 Eastman Kodak Company Coating providing panchromatic scattering

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050176850A1 (en) * 2004-02-09 2005-08-11 Christoph Schmidt Interference pigments
US20060027140A1 (en) * 2004-07-27 2006-02-09 Kniess Helge B Multilayered interference pigments
US20080274198A1 (en) * 2002-02-01 2008-11-06 Ralf Schweinfurth Use of multilayered pigments in the food and pharmaceuticals sector
US20130045338A1 (en) * 2011-08-16 2013-02-21 Alberto Argoitia Manufacturing of diffractive pigments by fluidized bed chemical vapor deposition

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0657807B2 (ja) * 1988-07-20 1994-08-03 トヨタ自動車株式会社 顔料及びその製造方法
JP3389360B2 (ja) * 1994-01-18 2003-03-24 マツダ株式会社 光干渉材及びそれを含有する塗料
US5584925A (en) * 1995-06-26 1996-12-17 Thiele Kaolin Company Chemically aggregated kaolin clay pigment and process for making the same by phosphate bonding
DE19638708A1 (de) * 1996-09-21 1998-04-16 Merck Patent Gmbh Mehrschichtige Interferenzpigmente
DE19707806A1 (de) * 1997-02-27 1998-09-03 Merck Patent Gmbh Multischicht-Interferenzpigment mit transparenter Mittelschicht
DE19746067A1 (de) * 1997-10-17 1999-04-22 Merck Patent Gmbh Interferenzpigmente
DE19817286A1 (de) * 1998-04-18 1999-10-21 Merck Patent Gmbh Mehrschichtiges Perlglanzpigment auf Basis eines opaken Substrates
JP3650290B2 (ja) * 1999-07-30 2005-05-18 日鉄鉱業株式会社 シアン色粉体およびその製造方法
DE19951869A1 (de) * 1999-10-28 2001-05-03 Merck Patent Gmbh Farbstarke Interferenzpigmente
DE10051062A1 (de) * 2000-10-14 2002-04-18 Merck Patent Gmbh Pigment für Sicherheitsanwendungen
DE10061178A1 (de) * 2000-12-07 2002-06-20 Merck Patent Gmbh Silberfarbenes Glanzpigment
DE10137831A1 (de) * 2001-08-02 2003-02-13 Merck Patent Gmbh Mehrschichtige Interferenzpigmente
JP3986304B2 (ja) * 2001-12-06 2007-10-03 株式会社日本色材工業研究所 積層型干渉性紫外線遮蔽顔料及びそれを配合した化粧料
US6875264B2 (en) * 2003-01-17 2005-04-05 Engelhard Corporation Multi-layer effect pigment
ES2543414T3 (es) * 2005-02-12 2015-08-19 Basf Corporation Pigmento de efecto multicapa goniocromático transparente
KR20100066460A (ko) * 2007-07-31 2010-06-17 바스프 에스이 광학적 가변성 효과 안료
DE102007058601A1 (de) * 2007-12-04 2009-06-10 Merck Patent Gmbh Sicherheitspigment

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080274198A1 (en) * 2002-02-01 2008-11-06 Ralf Schweinfurth Use of multilayered pigments in the food and pharmaceuticals sector
US20050176850A1 (en) * 2004-02-09 2005-08-11 Christoph Schmidt Interference pigments
US20060027140A1 (en) * 2004-07-27 2006-02-09 Kniess Helge B Multilayered interference pigments
US20130045338A1 (en) * 2011-08-16 2013-02-21 Alberto Argoitia Manufacturing of diffractive pigments by fluidized bed chemical vapor deposition

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of WO2014150846A1 *

Also Published As

Publication number Publication date
CN105051117A (zh) 2015-11-11
BR112015023311A2 (pt) 2017-07-18
US20140261084A1 (en) 2014-09-18
JP2016519172A (ja) 2016-06-30
WO2014150846A1 (en) 2014-09-25
KR20150127090A (ko) 2015-11-16
RU2015144081A (ru) 2017-04-24
EP2970678A1 (de) 2016-01-20

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