ES2038559A1 - Metodo de fabricacion de organopolisiloxanos. - Google Patents
Metodo de fabricacion de organopolisiloxanos.Info
- Publication number
- ES2038559A1 ES2038559A1 ES929200287A ES9200287A ES2038559A1 ES 2038559 A1 ES2038559 A1 ES 2038559A1 ES 929200287 A ES929200287 A ES 929200287A ES 9200287 A ES9200287 A ES 9200287A ES 2038559 A1 ES2038559 A1 ES 2038559A1
- Authority
- ES
- Spain
- Prior art keywords
- halide
- hydrocarbon
- making
- making organopolysiloxanes
- phosphonitrile
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 229920001296 polysiloxane Polymers 0.000 title abstract 2
- -1 phosphonitrile halide Chemical class 0.000 abstract 3
- 239000004215 Carbon black (E152) Substances 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- 239000002841 Lewis acid Substances 0.000 abstract 1
- 150000001450 anions Chemical group 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 125000005843 halogen group Chemical group 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 150000007517 lewis acids Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000003961 organosilicon compounds Chemical class 0.000 abstract 1
- 125000004437 phosphorous atom Chemical group 0.000 abstract 1
- SCPYDCQAZCOKTP-UHFFFAOYSA-N silanol Chemical compound [SiH3]O SCPYDCQAZCOKTP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/06—Preparatory processes
- C08G77/08—Preparatory processes characterised by the catalysts used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/12—Polysiloxanes containing silicon bound to hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
- C08G77/16—Polysiloxanes containing silicon bound to oxygen-containing groups to hydroxyl groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
- C08G77/18—Polysiloxanes containing silicon bound to oxygen-containing groups to alkoxy or aryloxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/70—Siloxanes defined by use of the MDTQ nomenclature
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Silicon Polymers (AREA)
Abstract
METODO DE FABRICACION DE ORGANOPOLISILOXANOS EN EL QUE SE PONE EN CONTACTO AL MENOS UNA UNIDAD ROA SIO4-A 2 EN LA QUE RBSO ES HIDROGENO, HIDROXILO, UN GRUPO HIDROCARBURO, HIDROCARBURO SUSTITUIDO O HIDROCARBONOXI C1-18 Y A TIENE UN VALOR QUE VA DESDE 0 A 4 CON UN HALURO DE FOSFONITRILO AB, DONDE A ES UN CATION DE HALURO DE FOSFONITRILO (X(PX2=N)PX3)+, DONDE X ES HALURO Y N ES DE 1 A 8 Y B ES ATOMO P, P. EJ. (MX(V-T+1)R2T). ES PARTICULARMENTE UTIL PARA CONDENSACION DE SILOXANOS BLOQUEADOS EN LOS EXTREMOS CON SILANOL.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB919103666A GB9103666D0 (en) | 1991-02-21 | 1991-02-21 | Method of making organopolysiloxanes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES2038559A1 true ES2038559A1 (es) | 1993-07-16 |
| ES2038559B1 ES2038559B1 (es) | 1994-03-01 |
Family
ID=10690363
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES9200287A Expired - Fee Related ES2038559B1 (es) | 1991-02-21 | 1992-02-12 | Metodo de fabricacion de organopolisiloxanos. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US5210131A (es) |
| JP (1) | JP3297070B2 (es) |
| KR (1) | KR100203251B1 (es) |
| AU (1) | AU645395B2 (es) |
| CA (1) | CA2061004A1 (es) |
| DE (1) | DE4205201B4 (es) |
| ES (1) | ES2038559B1 (es) |
| FR (1) | FR2673186B1 (es) |
| GB (2) | GB9103666D0 (es) |
| IT (1) | IT1256674B (es) |
| NL (1) | NL194442C (es) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4317978A1 (de) * | 1993-05-28 | 1994-12-01 | Wacker Chemie Gmbh | Organosiliciumreste aufweisende Phosphazene, Verfahren zu deren Herstellung und deren Verwendung |
| DE4317909A1 (de) * | 1993-05-28 | 1994-12-01 | Wacker Chemie Gmbh | Verfahren zum Kondensieren und/oder Äquilibrieren von Organosiliciumverbindungen |
| DE4323185C1 (de) * | 1993-07-10 | 1995-01-19 | Nuenchritz Chemie Gmbh | Verfahren zur Herstellung von Polyorganosiloxanen |
| WO1995001983A1 (de) * | 1993-07-10 | 1995-01-19 | Chemiewerk Nünchritz Gmbh | Katalysator zur herstellung von organosiloxanen oder polyorganosiloxanen |
| US5510441A (en) * | 1993-07-15 | 1996-04-23 | General Electric Company | Process for producing octamethyltrisiloxane |
| US5420221A (en) * | 1993-07-15 | 1995-05-30 | General Electric Company | Process for the production of linear organosiloxane polymers by disproportionation |
| US5457220A (en) * | 1994-04-29 | 1995-10-10 | General Electric Company | Process for the production of crosslinked siloxanes by disproportionation |
| DE4422813A1 (de) * | 1994-06-29 | 1996-01-04 | Wacker Chemie Gmbh | Verfahren zum Stabilisieren von Organpolysiloxanen |
| US5698654A (en) * | 1996-07-30 | 1997-12-16 | General Electric Company | Process for preparing hydrogen siloxane copolymers |
| US5753751A (en) * | 1996-10-24 | 1998-05-19 | General Electric Company | Process for preparing self-curable alkenyl hydride siloxane copolymers and coating composition |
| GB9727136D0 (en) * | 1997-12-24 | 1998-02-25 | Dow Corning | Catalyst composition |
| GB9827055D0 (en) | 1998-12-09 | 1999-02-03 | Dow Corning | Method for making a catalyst composition |
| GB9827088D0 (en) * | 1998-12-09 | 1999-02-03 | Dow Corning | Silylating agent |
| GB0018162D0 (en) | 2000-07-26 | 2000-09-13 | Dow Corning Sa | Polymerisation reactor and process |
| EP1498457B1 (de) * | 2003-07-04 | 2005-08-10 | Wacker-Chemie GmbH | Lagerstabile Siliconmassen |
| EP1866376B1 (en) | 2005-04-06 | 2015-05-20 | Dow Corning Corporation | Organosiloxane compositions |
| GB0604583D0 (en) | 2006-03-08 | 2006-04-19 | Dow Corning | Impregnated flexible sheet material |
| EP2061573A2 (en) | 2006-10-10 | 2009-05-27 | Dow Corning Corporation | Silicone foam control agent |
| US9694214B2 (en) | 2008-04-16 | 2017-07-04 | Dow Corning Corporation | Preparation of silicone microemulsions |
| CN102348765B (zh) | 2009-03-10 | 2015-09-09 | 道康宁东丽株式会社 | 水包油硅氧烷乳液组合物 |
| GB0905205D0 (en) | 2009-03-26 | 2009-05-13 | Dow Corning | Preparation of organosiloxane polymer |
| GB0905204D0 (en) | 2009-03-26 | 2009-05-13 | Dow Corning | Preparation of organosiloxane polymers |
| JP5894911B2 (ja) * | 2009-03-31 | 2016-03-30 | ダウ コーニング コーポレーションDow Corning Corporation | 分岐オルガノポリシロキサン |
| GB0905502D0 (en) | 2009-03-31 | 2009-05-13 | Dow Corning | Organopolysiloxane emulsions and their production |
| GB0905507D0 (en) | 2009-03-31 | 2009-05-13 | Dow Corning | Organopol Ysiloxane Compositions Containing An Active Material |
| BR112012010838A2 (pt) | 2009-10-26 | 2016-04-05 | Dow Corning | elastômero pintável |
| JP2013510079A (ja) | 2009-11-03 | 2013-03-21 | ダウ コーニング コーポレーション | ポリシルアルキレンシロキサンの製造プロセス |
| US9029428B2 (en) | 2010-07-02 | 2015-05-12 | Dow Corning Toray Co., Ltd. | Oil-in-water silicone emulsion composition |
| CN108137811A (zh) * | 2015-11-04 | 2018-06-08 | 美国陶氏有机硅公司 | 制备有机聚硅氧烷的方法 |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES371841A1 (es) * | 1968-09-25 | 1971-11-16 | Wacker Chemie Gmbh | Procedimiento para la preparacion de elastomeros de organo-polisiloxanos. |
| US3652711A (en) * | 1968-03-18 | 1972-03-28 | Wacker Chemie Gmbh | Method of polymerizing siloxanes |
| US3706775A (en) * | 1970-12-17 | 1972-12-19 | Wacker Chemie Gmbh | Method of preparing high molecular weight linear organopolysiloxanes |
| US4203913A (en) * | 1975-05-30 | 1980-05-20 | Wacker-Chemie Gmbh | Stabilization of organopolysiloxanes |
| US4725643A (en) * | 1985-07-09 | 1988-02-16 | Wacker-Chemie Gmbh | Process for preparing linear organopolysiloxanes having terminal triorganosiloxy groups |
| US4888405A (en) * | 1987-08-14 | 1989-12-19 | Wacker-Chemie Gmbh | Preparation and processing of mixtures containers organocyclosiloxanes |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB765744A (en) * | 1953-01-13 | 1957-01-09 | Wacker Chemie Gmbh | Process for the polymerisation of substantially diorgano-substituted siloxanes |
| DE1167534B (de) * | 1958-04-10 | 1964-04-09 | Wacker Chemie Gmbh | Verfahren zur Herstellung von hochviskosen und stabilen Organopolysiloxanoelen |
| DE1279019B (de) * | 1967-01-04 | 1968-10-03 | Wacker Chemie Gmbh | Verfahren zur Herstellung von Organohalogensiliciumverbindungen |
| US3449091A (en) * | 1967-01-27 | 1969-06-10 | Du Pont | Halide-modified phosphonitrilic chlorides |
| DE2538818C3 (de) * | 1975-09-01 | 1980-04-30 | Wacker-Chemie Gmbh, 8000 Muenchen | Verfahren zur Förderung von Kondensations- und/oder Äquilibrierungsreaktionen von Organosiliciumverbindungen |
| CA1109636A (en) * | 1977-04-18 | 1981-09-29 | Mark S. Prichard | Metal salt catalyzed polymerization of (npcl.sub.2) oligomers |
| JPS5819604B2 (ja) * | 1978-05-04 | 1983-04-19 | 大塚化学薬品株式会社 | ホスフアゼンオリゴマ−の製造法 |
| US4293675A (en) * | 1980-02-26 | 1981-10-06 | Minnesota Mining And Manufacturing Company | Antimony halide-organic phosphonate ester cationic polymerization catalysts |
| DE3711214A1 (de) * | 1987-04-03 | 1988-10-13 | Wacker Chemie Gmbh | Verfahren zur herstellung von diorganopolysiloxanen mit triorganosiloxygruppen als endstaendigen einheiten |
| DE3725377A1 (de) * | 1987-07-31 | 1989-02-09 | Wacker Chemie Gmbh | Verfahren zum kondensieren und/oder aequilibrieren von organo(poly)siloxanen |
| DE3742068A1 (de) * | 1987-12-11 | 1989-06-22 | Wacker Chemie Gmbh | Verfahren zur herstellung von in den endstaendigen einheiten je eine si-gebundene hydroxylgruppe aufweisenden diorganopolysiloxanen |
| DE3903137A1 (de) * | 1989-02-02 | 1990-08-16 | Wacker Chemie Gmbh | Phosphornitridchloride enthaltende zusammensetzungen |
-
1991
- 1991-02-21 GB GB919103666A patent/GB9103666D0/en active Pending
-
1992
- 1992-02-06 US US07/832,145 patent/US5210131A/en not_active Expired - Lifetime
- 1992-02-07 NL NL9200226A patent/NL194442C/nl not_active IP Right Cessation
- 1992-02-11 CA CA002061004A patent/CA2061004A1/en not_active Abandoned
- 1992-02-12 ES ES9200287A patent/ES2038559B1/es not_active Expired - Fee Related
- 1992-02-14 GB GB9203214A patent/GB2252975B/en not_active Expired - Fee Related
- 1992-02-19 KR KR1019920002459A patent/KR100203251B1/ko not_active Expired - Lifetime
- 1992-02-20 JP JP03343092A patent/JP3297070B2/ja not_active Expired - Lifetime
- 1992-02-20 IT ITTO920136A patent/IT1256674B/it active IP Right Grant
- 1992-02-20 FR FR929201920A patent/FR2673186B1/fr not_active Expired - Lifetime
- 1992-02-20 AU AU11079/92A patent/AU645395B2/en not_active Ceased
- 1992-02-20 DE DE4205201A patent/DE4205201B4/de not_active Expired - Lifetime
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3652711A (en) * | 1968-03-18 | 1972-03-28 | Wacker Chemie Gmbh | Method of polymerizing siloxanes |
| ES371841A1 (es) * | 1968-09-25 | 1971-11-16 | Wacker Chemie Gmbh | Procedimiento para la preparacion de elastomeros de organo-polisiloxanos. |
| US3706775A (en) * | 1970-12-17 | 1972-12-19 | Wacker Chemie Gmbh | Method of preparing high molecular weight linear organopolysiloxanes |
| US4203913A (en) * | 1975-05-30 | 1980-05-20 | Wacker-Chemie Gmbh | Stabilization of organopolysiloxanes |
| US4725643A (en) * | 1985-07-09 | 1988-02-16 | Wacker-Chemie Gmbh | Process for preparing linear organopolysiloxanes having terminal triorganosiloxy groups |
| US4888405A (en) * | 1987-08-14 | 1989-12-19 | Wacker-Chemie Gmbh | Preparation and processing of mixtures containers organocyclosiloxanes |
Also Published As
| Publication number | Publication date |
|---|---|
| NL194442B (nl) | 2001-12-03 |
| US5210131A (en) | 1993-05-11 |
| ITTO920136A1 (it) | 1993-08-20 |
| GB9203214D0 (en) | 1992-04-01 |
| KR100203251B1 (ko) | 1999-06-15 |
| FR2673186B1 (fr) | 1993-08-20 |
| IT1256674B (it) | 1995-12-12 |
| JPH04320423A (ja) | 1992-11-11 |
| NL194442C (nl) | 2002-04-04 |
| DE4205201B4 (de) | 2004-09-16 |
| ES2038559B1 (es) | 1994-03-01 |
| NL9200226A (nl) | 1992-09-16 |
| DE4205201A1 (de) | 1992-08-27 |
| AU1107992A (en) | 1992-08-27 |
| KR920016510A (ko) | 1992-09-24 |
| JP3297070B2 (ja) | 2002-07-02 |
| FR2673186A1 (fr) | 1992-08-28 |
| GB2252975B (en) | 1994-11-30 |
| CA2061004A1 (en) | 1992-08-22 |
| AU645395B2 (en) | 1994-01-13 |
| ITTO920136A0 (it) | 1992-02-20 |
| GB9103666D0 (en) | 1991-04-10 |
| GB2252975A (en) | 1992-08-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD1A | Patent lapsed |
Effective date: 20040916 |