ES2042905T3 - Procedimiento para preparar acrilatos o metacrilatos de alto punto de ebullicion. - Google Patents
Procedimiento para preparar acrilatos o metacrilatos de alto punto de ebullicion.Info
- Publication number
- ES2042905T3 ES2042905T3 ES89115066T ES89115066T ES2042905T3 ES 2042905 T3 ES2042905 T3 ES 2042905T3 ES 89115066 T ES89115066 T ES 89115066T ES 89115066 T ES89115066 T ES 89115066T ES 2042905 T3 ES2042905 T3 ES 2042905T3
- Authority
- ES
- Spain
- Prior art keywords
- methacrylates
- high boiling
- procedure
- preparing high
- acrylates
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 150000002734 metacrylic acid derivatives Chemical class 0.000 title abstract 3
- 238000009835 boiling Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 title 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 abstract 1
- 150000001252 acrylic acid derivatives Chemical class 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 150000005846 sugar alcohols Polymers 0.000 abstract 1
- 238000005809 transesterification reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
EL INVENTO SE REFIERE A UN PROCEDIMIENTO PARA PRODUCIR ACRILATOS CON ELEVADOS PUNTOS DE EBULLICION Y CON PEQUEÑOS INDICES DE COLOR. DICHO PROCEDIMIENTO CONSISTE EN TRATAR METACRILATOS (ACRILATOS) CON ALCOHOLES PRIMARIOS, SECUNDARIOS O TERCIARIOS SEGUN METODOS CONOCIDOS SE CARACTERIZA POR SEPARAR EL PRODUCTO OBTENIDO DE LOS CATALIZADORES EMPLEADOS Y SOMETER AL PRODUCTO SEPARADO A UNA EVAPORACION RAPIDA Y CORTA A UNA PRESION DE 0,01 A 10 MBAR Y A UNA TEMPERATURA ENTRE 110 Y 170 C.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3836093A DE3836093A1 (de) | 1988-10-22 | 1988-10-22 | Verfahren zur herstellung von hochsiedenden acrylaten bzw. methacrylaten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2042905T3 true ES2042905T3 (es) | 1993-12-16 |
Family
ID=6365733
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES89115066T Expired - Lifetime ES2042905T3 (es) | 1988-10-22 | 1989-08-16 | Procedimiento para preparar acrilatos o metacrilatos de alto punto de ebullicion. |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4983761A (es) |
| EP (1) | EP0365777B1 (es) |
| JP (1) | JPH02157246A (es) |
| AT (1) | ATE77361T1 (es) |
| DE (2) | DE3836093A1 (es) |
| ES (1) | ES2042905T3 (es) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5498751A (en) * | 1993-09-03 | 1996-03-12 | Cps Chemical Company, Inc. | Organotin catalyzed transesterification |
| US5606103A (en) * | 1993-09-03 | 1997-02-25 | Cps Chemical Company, Inc. | Organotin catalyzed transesterification |
| DE19930721C2 (de) * | 1999-07-05 | 2001-12-20 | Roehm Gmbh | Verfahren zur Herstellung und Prozeßinhibierung von Isobornylmethacrylat |
| WO2002055472A1 (de) * | 2000-12-18 | 2002-07-18 | Basf Aktiengesellschaft | Verfahren zur herstellung von höheren (meth)acrylsäureestern |
| WO2005040088A1 (ja) * | 2003-10-24 | 2005-05-06 | Mitsubishi Rayon Co., Ltd. | (メタ)アクリル酸エステルの製造方法 |
| EP2045233B1 (de) * | 2007-10-04 | 2012-11-28 | Celanese Chemicals Europe GmbH | Verfahren zur Farbverbesserung von Oligoglykolcarbonsäureestern |
| DE102009002861A1 (de) * | 2009-05-06 | 2010-11-18 | Evonik Röhm Gmbh | Verfahren und Anlage zur Aufreinigung von Monomeren |
| KR20150016133A (ko) | 2013-08-02 | 2015-02-11 | 주식회사 엘지화학 | 광반응성 화합물의 정제 방법 및 광반응성 화합물 |
| EP3072879A1 (en) | 2015-03-26 | 2016-09-28 | Nitto Europe N.V | Method for prevention of premature polymerization |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1568376B2 (de) * | 1966-03-29 | 1973-12-06 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Verfahren zum Umestern von Estern der Acryl oder Methacrylsäure |
| GB1174148A (en) * | 1967-08-11 | 1969-12-10 | Nii Monomerov Dlya Sint Kauchu | Method of producing Acrylic and Methacrylic Esters |
| FR2049944A5 (es) * | 1969-06-05 | 1971-03-26 | Japan Gas Chemical Co | |
| DE2317226C3 (de) * | 1973-04-06 | 1980-10-30 | Deutsche Texaco Ag, 2000 Hamburg | Verfahren zur Herstellung von höhermolekularen Alkylacrylaten bzw. -methacrylaten |
| DE2744641B2 (de) * | 1977-10-04 | 1979-08-02 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Verfahren zur Herstellung von Estern der Methacrylsäure |
| FR2584711B1 (fr) * | 1985-07-11 | 1987-10-30 | Organo Synthese Ste Fse | Procede de preparation d'esters methacrylique par transesterification |
-
1988
- 1988-10-22 DE DE3836093A patent/DE3836093A1/de not_active Withdrawn
-
1989
- 1989-08-16 ES ES89115066T patent/ES2042905T3/es not_active Expired - Lifetime
- 1989-08-16 EP EP89115066A patent/EP0365777B1/de not_active Expired - Lifetime
- 1989-08-16 AT AT89115066T patent/ATE77361T1/de not_active IP Right Cessation
- 1989-08-16 DE DE8989115066T patent/DE58901685D1/de not_active Expired - Lifetime
- 1989-10-05 US US07/417,558 patent/US4983761A/en not_active Expired - Fee Related
- 1989-10-23 JP JP1273910A patent/JPH02157246A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| EP0365777A1 (de) | 1990-05-02 |
| EP0365777B1 (de) | 1992-06-17 |
| US4983761A (en) | 1991-01-08 |
| DE3836093A1 (de) | 1990-04-26 |
| DE58901685D1 (de) | 1992-07-23 |
| JPH02157246A (ja) | 1990-06-18 |
| ATE77361T1 (de) | 1992-07-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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