ES2054185T3 - Procedimiento para la preparacion de 3-ciano-3,5,5'-trimetil-1-ciclohexanona. - Google Patents
Procedimiento para la preparacion de 3-ciano-3,5,5'-trimetil-1-ciclohexanona.Info
- Publication number
- ES2054185T3 ES2054185T3 ES90117995T ES90117995T ES2054185T3 ES 2054185 T3 ES2054185 T3 ES 2054185T3 ES 90117995 T ES90117995 T ES 90117995T ES 90117995 T ES90117995 T ES 90117995T ES 2054185 T3 ES2054185 T3 ES 2054185T3
- Authority
- ES
- Spain
- Prior art keywords
- trimetil
- ciano
- preparation
- reaction
- ciclohexanona
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 abstract 4
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 abstract 2
- 238000010992 reflux Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/08—Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds
- C07C253/10—Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds to compounds containing carbon-to-carbon double bonds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
LA PRESENTE INVENCION TRATA UN PROCESO PARA LA PREPARACION DE 3-CIANO-3, 5, 5''-TRIMETIL-1-CICLOHEXANORA POR MEDIO DE LA REACCION DE ISOFORONA CON UN CIANURO ALKALINO. LA REACCION ES REALIZADA PARTIENDO DE CANTIDADES IGUALES DE ISOFORONA Y DE CIANURO DISUELTOS EN UNA SOLUCION HOMOGENEA ACUOSO/ORGONICO A UNA TEMPERATURA COMPRENDIDA ENTRE 20 C, Y LA TEMPERATURA DE REFLUJO MANTENIENDO UN PH ENTRE 14 Y 8 POR MEDIOS DE LA ADICION GRADUAL DE UN ACIDO INORGANICO DURANTE LA REACCION.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT02224689A IT1236969B (it) | 1989-11-02 | 1989-11-02 | Procedimento di preparazione di 3-ciano-3,5,5'-trimetil-1-cicloesanone. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2054185T3 true ES2054185T3 (es) | 1994-08-01 |
Family
ID=11193611
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES90117995T Expired - Lifetime ES2054185T3 (es) | 1989-11-02 | 1990-09-19 | Procedimiento para la preparacion de 3-ciano-3,5,5'-trimetil-1-ciclohexanona. |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US5142090A (es) |
| EP (1) | EP0425806B1 (es) |
| JP (1) | JPH03153656A (es) |
| DE (1) | DE69009394T2 (es) |
| ES (1) | ES2054185T3 (es) |
| IT (1) | IT1236969B (es) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4203456A1 (de) * | 1992-02-07 | 1993-08-12 | Basf Ag | Verfahren zur kontinuierlichen herstellung von 3-cyano-3,5,5-trimethylcyclohexanon |
| US5235089A (en) * | 1992-02-27 | 1993-08-10 | Hampshire Chemical Corp. | Process for the preparation of 3-cyano-3,5,5-trimethylcyclohexanone |
| US5183915A (en) * | 1992-03-05 | 1993-02-02 | Elf Atochem North America, Inc. | Catalyst and process for the production of 3-cyano-3,5,5-trialkylcyclohexanone |
| DE4407487A1 (de) * | 1994-03-07 | 1995-09-14 | Basf Ag | Verfahren zur Herstellung von 3-Cyano-3,5,5-trimethylcyclohexanon |
| DE102010062603A1 (de) | 2010-12-08 | 2012-06-14 | Evonik Degussa Gmbh | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin |
| DE102011077681A1 (de) | 2011-06-17 | 2012-12-20 | Evonik Degussa Gmbh | Verfahren zur Herstellung von 3-Cyano-3,5,5-trimethylcyclohexanon |
| CN106977422B (zh) * | 2017-03-06 | 2018-12-04 | 万华化学集团股份有限公司 | 一种连续生产异佛尔酮腈的方法 |
| CN117843527A (zh) * | 2023-12-14 | 2024-04-09 | 万华化学集团股份有限公司 | 一种异佛尔酮腈的制备方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH371440A (fr) * | 1957-05-31 | 1963-08-31 | Rohm & Haas | Procédé de préparation de cyanocétones carbocycliques |
| DE1229078B (de) * | 1961-10-18 | 1966-11-24 | Hibernia Chemie Ges Mit Beschr | Verfahren zur Herstellung von 3-(Aminomethyl)-3, 5, 5-trimethylcyclohexylderivaten |
| DE1240854B (de) * | 1964-10-24 | 1967-05-24 | Scholven Chemie Ag | Verfahren zur Herstellung von 3-Cyan-3, 5, 5-trimethylcyclohexanon aus Isophoron undBlausaeure |
| FR2468584A1 (fr) * | 1979-10-26 | 1981-05-08 | Ugine Kuhlmann | Procede de preparation de cyano-3-trimethyl-3,5,5-cyclohexanone |
-
1989
- 1989-11-02 IT IT02224689A patent/IT1236969B/it active IP Right Grant
-
1990
- 1990-09-19 EP EP90117995A patent/EP0425806B1/en not_active Expired - Lifetime
- 1990-09-19 ES ES90117995T patent/ES2054185T3/es not_active Expired - Lifetime
- 1990-09-19 DE DE69009394T patent/DE69009394T2/de not_active Expired - Fee Related
- 1990-09-20 US US07/585,240 patent/US5142090A/en not_active Expired - Fee Related
- 1990-11-02 JP JP2298751A patent/JPH03153656A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| IT8922246A1 (it) | 1991-05-02 |
| JPH03153656A (ja) | 1991-07-01 |
| DE69009394T2 (de) | 1994-12-22 |
| IT8922246A0 (it) | 1989-11-02 |
| US5142090A (en) | 1992-08-25 |
| IT1236969B (it) | 1993-05-07 |
| DE69009394D1 (de) | 1994-07-07 |
| EP0425806B1 (en) | 1994-06-01 |
| EP0425806A1 (en) | 1991-05-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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