ES2061332T3 - Procedimiento para purificar monoterc-butil-hidroquinona. - Google Patents

Procedimiento para purificar monoterc-butil-hidroquinona.

Info

Publication number
ES2061332T3
ES2061332T3 ES92901049T ES92901049T ES2061332T3 ES 2061332 T3 ES2061332 T3 ES 2061332T3 ES 92901049 T ES92901049 T ES 92901049T ES 92901049 T ES92901049 T ES 92901049T ES 2061332 T3 ES2061332 T3 ES 2061332T3
Authority
ES
Spain
Prior art keywords
butyl hydroquinone
monoterc
hidroquinona
butil
purify
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES92901049T
Other languages
English (en)
Inventor
James Ronald Hilderbrand
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eastman Chemical Co
Original Assignee
Eastman Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eastman Chemical Co filed Critical Eastman Chemical Co
Application granted granted Critical
Publication of ES2061332T3 publication Critical patent/ES2061332T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/685—Processes comprising at least two steps in series
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/72—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

SE SUMINISTRA UN PROCESO PARA LA PRODUCCION DE HIDROQUINONA BUTIL TERCIARIA DE GRADO DE ALIMENTACION A PARTIR DE HIDROQUINONA BUTIL MONOTERCIARIA IMPURA. LOS CRISTALES DE HIDROQUINONA BUTIL MONOTERCIARIA IMPURA SON AGITADOS A UNA TEMPERATURA ELEVADA MIENTRAS SE ENCUENTRAN EN CONTACTO CON UN DISOLVENTE NO POLAR BAJO CONDICIONES DE EXTRACCION DE LA MAYORIA DE LAS IMPUREZAS SEGUIDA MEDIANTE UNA SEPARACION DE LOS CRISTALES DE HIDROQUINONA BUTIL MONOTERCIARIA PURIFICADA A PARTIR DEL DISOLVENTE A UNA TEMPERATURA POR ENCIMA DEL PUNTO DE CRISTALIZACION DE LAS IMPUREZAS.
ES92901049T 1990-12-05 1991-11-26 Procedimiento para purificar monoterc-butil-hidroquinona. Expired - Lifetime ES2061332T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/622,453 US5087771A (en) 1990-12-05 1990-12-05 Process for the purification of monotertiarybutyl hydroquinone

Publications (1)

Publication Number Publication Date
ES2061332T3 true ES2061332T3 (es) 1994-12-01

Family

ID=24494224

Family Applications (1)

Application Number Title Priority Date Filing Date
ES92901049T Expired - Lifetime ES2061332T3 (es) 1990-12-05 1991-11-26 Procedimiento para purificar monoterc-butil-hidroquinona.

Country Status (9)

Country Link
US (1) US5087771A (es)
EP (1) EP0561929B1 (es)
JP (1) JPH06503326A (es)
AT (1) ATE112253T1 (es)
CA (1) CA2095110A1 (es)
DE (1) DE69104379T2 (es)
DK (1) DK0561929T3 (es)
ES (1) ES2061332T3 (es)
WO (1) WO1992010456A1 (es)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6271424B1 (en) 2000-06-16 2001-08-07 Eastman Chemical Company Process for the purification of monotertiarybutyl hydroquinone
CN102838454B (zh) * 2012-09-25 2014-07-30 厦门大学 一种叔丁基对苯二酚的提纯方法
CN104072341B (zh) * 2014-06-23 2016-01-06 华南理工大学 一种2,5-二叔丁基对苯二酚精制方法
CN106770705A (zh) * 2016-11-22 2017-05-31 青岛舜宇恒平仪器有限公司 对易氧化物质进行在线柱后还原检测的装置和分析方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2722556A (en) * 1952-03-19 1955-11-01 Eastman Kodak Co Preparation of tertiary butyl hydroquinone
DE2606364C3 (de) * 1976-02-18 1988-05-26 Basf Ag, 6700 Ludwigshafen Verfahren zur Stofftrennung aus einem flüssigen Gemisch durch fraktionierte Kristallisation
US4507244A (en) * 1982-06-02 1985-03-26 Walter Rau Lebensmittelwerke Gmbh & Co. Kg Method for crystallizing a substance from a solution
US4447655A (en) * 1982-11-24 1984-05-08 General Electric Company Purification of bisphenol-A
US4536292A (en) * 1984-03-26 1985-08-20 Calgon Corporation Carboxylic/sulfonic/quaternary ammonium polymers for use as scale and corrosion inhibitors
JPS60221607A (ja) * 1984-04-17 1985-11-06 Babcock Hitachi Kk 分割セル型流動層燃焼装置
US4720570A (en) * 1986-03-14 1988-01-19 Celanese Corporation Rate of crystallizing diphenylisophthalate/diphenylterephthalate monomer
US4861919A (en) * 1988-02-29 1989-08-29 The Dow Chemical Company Countercurrent multi-stage water crystallization of aromatic compounds

Also Published As

Publication number Publication date
EP0561929A1 (en) 1993-09-29
US5087771A (en) 1992-02-11
DK0561929T3 (da) 1994-10-24
WO1992010456A1 (en) 1992-06-25
EP0561929B1 (en) 1994-09-28
ATE112253T1 (de) 1994-10-15
DE69104379D1 (de) 1994-11-03
CA2095110A1 (en) 1992-06-06
JPH06503326A (ja) 1994-04-14
DE69104379T2 (de) 1995-02-09

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