ES2067115T3 - Procedimiento para la preparacion de esteres de acido 3-oxocarboxilico. - Google Patents
Procedimiento para la preparacion de esteres de acido 3-oxocarboxilico.Info
- Publication number
- ES2067115T3 ES2067115T3 ES91117470T ES91117470T ES2067115T3 ES 2067115 T3 ES2067115 T3 ES 2067115T3 ES 91117470 T ES91117470 T ES 91117470T ES 91117470 T ES91117470 T ES 91117470T ES 2067115 T3 ES2067115 T3 ES 2067115T3
- Authority
- ES
- Spain
- Prior art keywords
- esters
- oxocarboxilico
- procedure
- preparation
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000002253 acid Substances 0.000 title abstract 2
- 230000010933 acylation Effects 0.000 abstract 2
- 238000005917 acylation reaction Methods 0.000 abstract 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract 1
- 150000004729 acetoacetic acid derivatives Chemical class 0.000 abstract 1
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- -1 carboxylic acid chlorides Chemical class 0.000 abstract 1
- 230000008030 elimination Effects 0.000 abstract 1
- 238000003379 elimination reaction Methods 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 239000011777 magnesium Substances 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
- C07C67/333—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton
- C07C67/343—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cephalosporin Compounds (AREA)
- Medicinal Preparation (AREA)
- Heterocyclic Compounds Containing Sulfur Atoms (AREA)
- Furan Compounds (AREA)
- Pyridine Compounds (AREA)
Abstract
LOS 3 ESTERES DE ACIDO DE OXOCARBONO SE ELABORAN MEDIANTE LA ACILACION DE MAGNESIOMENOLATE DE ESTERES DE ACIDO ACETACETICO CON CLORIDOS DE ACIDO DE CARBONO Y SU DIVISION DE GRUPOS DE ACETILO DE LOS ESTERES DE ACIDO ACETACETICO DE ACILO, FORMADOS POR PRODUCTOS INTERMEDIOS. DEBIDO AL AÑADIDO DE UNA MINA TERCIARIA EN LA ACILACION, SE CONSIGUE UNA MEJOR LIMPIEZA Y RENDIMIENTO DE LOS PRODUCTOS.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH330190 | 1990-10-15 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2067115T3 true ES2067115T3 (es) | 1995-03-16 |
Family
ID=4253029
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES91117470T Expired - Lifetime ES2067115T3 (es) | 1990-10-15 | 1991-10-14 | Procedimiento para la preparacion de esteres de acido 3-oxocarboxilico. |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US5144057A (es) |
| EP (1) | EP0481395B1 (es) |
| JP (1) | JPH04264054A (es) |
| AT (1) | ATE117669T1 (es) |
| CA (1) | CA2053487A1 (es) |
| DE (1) | DE59104393D1 (es) |
| DK (1) | DK0481395T3 (es) |
| ES (1) | ES2067115T3 (es) |
| NO (1) | NO174802B (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3251525B2 (ja) * | 1996-05-24 | 2002-01-28 | 高砂香料工業株式会社 | 3−オキソカルボン酸エステルの製造方法 |
| US5965767A (en) * | 1997-04-10 | 1999-10-12 | Procter & Gamble Company | Beta ketoester compositions and method of manufacture |
| JP2001199935A (ja) * | 2000-01-14 | 2001-07-24 | Takasago Internatl Corp | ピバロイル酢酸エステルの製造方法 |
| US6545165B1 (en) * | 2000-02-04 | 2003-04-08 | Roche Colorado Corporation | Synthesis of 3,6-dialkyl-5,6-dihydro-4-hydroxy-pyran-2-one |
| AT409376B (de) * | 2000-07-12 | 2002-07-25 | Dsm Fine Chem Austria Gmbh | Verfahren zur herstellung von 3-oxocarbonsäureestern |
| JP2002332259A (ja) * | 2001-05-08 | 2002-11-22 | Konica Corp | α位に電子吸引性基を有するβ−ケトカルボン酸エステル誘導体の製造方法 |
| WO2003082929A1 (en) * | 2002-04-03 | 2003-10-09 | Dainippon Ink And Chemicals, Inc. | Photoinitiator, novel compound, and photocurable composition |
| CN100398510C (zh) * | 2003-12-03 | 2008-07-02 | 上海化学试剂研究所 | β-二酮酯的制备方法 |
| CN1318382C (zh) * | 2003-12-10 | 2007-05-30 | 上海化学试剂研究所 | 丙酰乙酸乙酯的制备方法 |
| CN100335456C (zh) * | 2003-12-10 | 2007-09-05 | 上海化学试剂研究所 | 脂肪族β-酮酸酯的制备方法 |
| US20060149094A1 (en) * | 2004-12-30 | 2006-07-06 | Zoeller Joseph R | Process for generating pivaloylacetate esters via carbonylation of chloropinacolone |
| CN102285900B (zh) * | 2011-07-11 | 2013-10-02 | 上海赫腾精细化工有限公司 | 3-(2,6-二氯苯基)-2,3-二氧丙酸乙酯-2-(4-氯苯基)腙的制备方法 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5770837A (en) * | 1980-10-20 | 1982-05-01 | Yoshitomi Pharmaceut Ind Ltd | Preparation of carboxylic acid derivative |
-
1991
- 1991-10-11 JP JP3263917A patent/JPH04264054A/ja not_active Withdrawn
- 1991-10-11 US US07/774,876 patent/US5144057A/en not_active Expired - Fee Related
- 1991-10-14 EP EP91117470A patent/EP0481395B1/de not_active Expired - Lifetime
- 1991-10-14 DK DK91117470.4T patent/DK0481395T3/da active
- 1991-10-14 ES ES91117470T patent/ES2067115T3/es not_active Expired - Lifetime
- 1991-10-14 NO NO914035A patent/NO174802B/no unknown
- 1991-10-14 DE DE59104393T patent/DE59104393D1/de not_active Expired - Fee Related
- 1991-10-14 AT AT91117470T patent/ATE117669T1/de not_active IP Right Cessation
- 1991-10-15 CA CA002053487A patent/CA2053487A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| EP0481395B1 (de) | 1995-01-25 |
| EP0481395A3 (en) | 1992-09-16 |
| JPH04264054A (ja) | 1992-09-18 |
| DK0481395T3 (da) | 1995-04-03 |
| NO914035L (no) | 1992-04-21 |
| DE59104393D1 (de) | 1995-03-09 |
| ATE117669T1 (de) | 1995-02-15 |
| NO914035D0 (no) | 1991-10-14 |
| NO174802C (es) | 1994-07-13 |
| CA2053487A1 (en) | 1992-04-16 |
| US5144057A (en) | 1992-09-01 |
| EP0481395A2 (de) | 1992-04-22 |
| NO174802B (no) | 1994-04-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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