ES2067258T3 - Procedimiento para la preparacion de dioxido de titanio finamente dividido, y dioxido de titanio finamente dividido. - Google Patents

Procedimiento para la preparacion de dioxido de titanio finamente dividido, y dioxido de titanio finamente dividido.

Info

Publication number
ES2067258T3
ES2067258T3 ES92101653T ES92101653T ES2067258T3 ES 2067258 T3 ES2067258 T3 ES 2067258T3 ES 92101653 T ES92101653 T ES 92101653T ES 92101653 T ES92101653 T ES 92101653T ES 2067258 T3 ES2067258 T3 ES 2067258T3
Authority
ES
Spain
Prior art keywords
titanium dioxide
titanium
finally divided
dioxide
divided titanium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES92101653T
Other languages
English (en)
Inventor
Lothar Dr Elfenthal
Edgar Dr Klein
Franz Dr Rosendahl
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kronos Titan GmbH
Original Assignee
Kronos Titan GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kronos Titan GmbH filed Critical Kronos Titan GmbH
Application granted granted Critical
Publication of ES2067258T3 publication Critical patent/ES2067258T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00Compounds of titanium
    • C01G23/04Oxides; Hydroxides
    • C01G23/047Titanium dioxide
    • C01G23/053Producing by wet processes, e.g. hydrolysing titanium salts
    • C01G23/0536Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/36Compounds of titanium
    • C09C1/3607Titanium dioxide
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/36Compounds of titanium
    • C09C1/3607Titanium dioxide
    • C09C1/3653Treatment with inorganic compounds
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/84Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/10Particle morphology extending in one dimension, e.g. needle-like
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/54Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/60Optical properties, e.g. expressed in CIELAB-values

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Geology (AREA)
  • Physics & Mathematics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Composite Materials (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Medicinal Preparation (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Cosmetics (AREA)

Abstract

LA INVENCION ALUDE A UN PROCESO PARA LA PRODUCCION DE BIOXIDO DE TITANIO DE PARTICULAS FINAS Y BIOXIDO DE TITANIO DE PARTICULAS FINAS. EL BIOXIDO DE TITANIO ES A LA LUZ ESENCIALMENTE TRANSPARENTE Y TAMBIEN ABSORBENTE DE LA RADIACION ULTRAVIOLETA. PARA SU PRODUCCION SE UTILIZARA DIOXIDO DE ESTAÑO EN PARTICULAS FINAS, CUYO TAMAÑO DE PARTICULA ES DE 1 HASTA 10 NM, ESENCIALMENTE ES DE 1 HASTA 4 NM, EN UNA CANTIDAD DE 0,5 HASTA 10 DE PORCENTAJE DE PESO, REFERIDO A TIO SUB 2. MEDIANTE LA ADICION DE DIOXIDO DE ESTAÑO SE AJUSTARA EL TAMAÑO CONSEGUIDO DE LA PARTICULA DEL DIOXIDO DE TITANIO. MEDIANTE UNA MALEABILIDAD DE 300 HASTA 800 GRADOS C, LAS PARTICULAS CON FORMA DE AGUJA SERAN REDONDEADAS. POR MEDIO DE UN TRATAMIENTO POSTERIOR, LAS PARTICULAS PUEDEN SER RECUBIERTAS CON CAPAS DE SUSTANCIAS INORGANICAS Y/O ORGANICAS. EL DIOXIDO DE TITANIO DE PARTES FINAS, PUEDE SER PRODUCIDO SOBRE SODIOTITANATO POR DESCOMPOSICION CON ACIDO CLORHIDRICO O MEDIANTE UNA HIDROLISIS PROPIA DE UNA COMBINACION DE TITANIOTETRAVALENTE, LA CUAL LLEVA A UNA FORMACION DE RUTILO. EL DIOXIDO DE ESTAÑO SE APLICA PREFERENTEMENTE COMO UNA SOLUCION COLOIDAL, QUE SE CONSIGUE MEDIANTE LA REACCION DEL TETRACLORURO DE ESTAÑO CON AGUA, CONFORMADA EN UN MAXIMO DE 22 GRADOS C.
ES92101653T 1991-02-21 1992-02-01 Procedimiento para la preparacion de dioxido de titanio finamente dividido, y dioxido de titanio finamente dividido. Expired - Lifetime ES2067258T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4105345A DE4105345A1 (de) 1991-02-21 1991-02-21 Verfahren zur herstellung von feinteiligem titandioxid und feinteiliges titandioxid

Publications (1)

Publication Number Publication Date
ES2067258T3 true ES2067258T3 (es) 1995-03-16

Family

ID=6425519

Family Applications (1)

Application Number Title Priority Date Filing Date
ES92101653T Expired - Lifetime ES2067258T3 (es) 1991-02-21 1992-02-01 Procedimiento para la preparacion de dioxido de titanio finamente dividido, y dioxido de titanio finamente dividido.

Country Status (11)

Country Link
US (1) US5215580A (es)
EP (1) EP0499863B1 (es)
JP (1) JP3307667B2 (es)
CN (1) CN1064285A (es)
BR (1) BR9200366A (es)
CA (1) CA2059688A1 (es)
DE (2) DE4105345A1 (es)
ES (1) ES2067258T3 (es)
FI (1) FI101311B (es)
MX (1) MX9200587A (es)
NO (1) NO306261B1 (es)

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DE4222905A1 (de) * 1992-07-11 1994-01-13 Kronos Titan Gmbh Subpigmentäres Titandioxid mit verbesserter Photostabilität
US5720805A (en) * 1993-04-13 1998-02-24 Southwest Research Institute Titanium-tin-oxide nanoparticles, compositions utilizing the same, and the method of forming the same
US5391609A (en) * 1993-06-09 1995-02-21 Mobil Oil Corp. Transparent films providing a barrier to the transmission of ultra-violet light
AU675000B2 (en) * 1993-10-22 1997-01-16 Ishihara Sangyo Kaisha Ltd. Dendrite or asteroidal titanium dioxide micro-particles and process for producing the same
US5534056A (en) * 1993-10-28 1996-07-09 Manfred R. Kuehnle Composite media with selectable radiation-transmission properties
US5527386A (en) * 1993-10-28 1996-06-18 Manfred R. Kuehnle Composite media with selectable radiation-transmission properties
US5601807A (en) * 1995-05-19 1997-02-11 Asaoka; Hisatoshi Ceramic type sunscreens
WO1997015526A1 (en) * 1995-10-27 1997-05-01 E.I. Du Pont De Nemours And Company Hydrothermal process for making ultrafine metal oxide powders
DE19543204C2 (de) * 1995-11-20 1997-09-18 Bayer Ag Verfahren zur Herstellung von nanodispersem Titandioxid und seine Verwendung
CA2259281C (fr) * 1996-07-08 2002-09-17 Rhodia Chimie Particules de dioxyde de titane, leur procede de preparation et leur utilisation dans les cosmetiques, vernis et lasures
US6933331B2 (en) 1998-05-22 2005-08-23 Nanoproducts Corporation Nanotechnology for drug delivery, contrast agents and biomedical implants
US5997890A (en) * 1997-05-23 1999-12-07 The Procter & Gamble Company Skin care compositions and method of improving skin appearance
US5972359A (en) * 1997-05-23 1999-10-26 The Procter & Gamble Company Skin care compositions and method of improving skin appearance
US6174533B1 (en) 1997-05-23 2001-01-16 The Procter & Gamble Company Skin care compositions and method of improving skin appearance
US6013270A (en) * 1998-04-20 2000-01-11 The Procter & Gamble Company Skin care kit
JP4220020B2 (ja) * 1998-07-16 2009-02-04 チタン工業株式会社 超微粒子酸化チタン及びその製造方法並びにその応用
US6743286B2 (en) * 2001-07-30 2004-06-01 Millennium Inorganic Chemicals, Inc. Inorganic particles and methods of making
US7285162B2 (en) * 2001-07-30 2007-10-23 Millennium Inorganic Chemicals, Inc. Titanium dioxide pigment having improved light stability
US6855426B2 (en) 2001-08-08 2005-02-15 Nanoproducts Corporation Methods for producing composite nanoparticles
SE0103528D0 (sv) * 2001-10-21 2001-10-21 Jan Faergeman Topiska kompositioner med förstärkt effekt
DE10205920A1 (de) 2002-02-12 2003-08-21 Itn Nanovation Gmbh Nanoskaliger Rutil, sowie Verfahren zu dessen Herstellung
GB0211780D0 (en) * 2002-05-22 2002-07-03 Itri Ltd Nano-particulate tin products
KR20020063532A (ko) * 2002-06-07 2002-08-03 이종국 티탄산나트륨 휘스커의 나트륨 용출에 의한 티타니아휘스커 제조법
WO2004003070A1 (de) * 2002-06-28 2004-01-08 Merck Patent Gmbh Härtung und trocknung von lacksystemen und druckfarben
US7708974B2 (en) 2002-12-10 2010-05-04 Ppg Industries Ohio, Inc. Tungsten comprising nanomaterials and related nanotechnology
US6838494B2 (en) * 2002-12-30 2005-01-04 Ferro Corporation Light reflecting polymeric compositions
US6913830B2 (en) * 2003-08-14 2005-07-05 Ppg Industries Ohio, Inc. Coating compositions containing semiconductor colorants
JP4851685B2 (ja) * 2003-10-31 2012-01-11 三井化学株式会社 ルチル型酸化チタン超微粒子の製造方法
KR100809758B1 (ko) * 2004-06-29 2008-03-04 미쓰이 가가쿠 가부시키가이샤 주석 변성 루틸형 산화티탄 미립자
US7265176B2 (en) * 2005-01-31 2007-09-04 E. I. Du Pont De Nemours And Company Composition comprising nanoparticle TiO2 and ethylene copolymer
ATE385508T1 (de) * 2005-02-04 2008-02-15 Du Pont Zusammensetzungen fluorkohlenstoff-gepfropfte polysiloxane aufweisend
JP4641212B2 (ja) * 2005-04-25 2011-03-02 三井化学株式会社 複合酸化物超微粒子およびその製造法
JP4673664B2 (ja) * 2005-04-27 2011-04-20 三井化学株式会社 コーティング用高屈折率樹脂組成物
CN100333830C (zh) * 2005-04-30 2007-08-29 东南大学 锐钛矿型二氧化钛溶胶的制备方法
US20080194009A1 (en) * 2007-02-13 2008-08-14 Marentis Rodger T Novel HVAC pathogen neutralization system
US7704470B2 (en) * 2007-04-24 2010-04-27 Haydock Consulting Services, Lc Removal of contaminants from by-product acids
JP5851102B2 (ja) * 2011-03-02 2016-02-03 石原産業株式会社 ルチル型酸化チタンナノ粒子及びその製造方法
JP6076019B2 (ja) * 2011-10-06 2017-02-08 多木化学株式会社 アルカリ性ルチル型酸化チタンゾル
TWI613261B (zh) 2012-06-29 2018-02-01 克洛諾斯國際有限公司 將無機色素粒子作表面處理的方法
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CN107216686A (zh) * 2017-06-01 2017-09-29 宁海仁元电子材料有限公司 一种导电钛白粉生产工艺
CN109250753A (zh) * 2018-12-10 2019-01-22 攀钢集团攀枝花钢铁研究院有限公司 制备纳米锐钛矿型二氧化钛的方法
CN111864084B (zh) * 2020-07-24 2022-03-01 武汉理工大学 一种稳定高效钙钛矿太阳能电池的制备方法
CN114349042A (zh) * 2022-01-05 2022-04-15 中国科学技术大学 金红石相掺氢金属氧化物、稳定无缺陷的金红石相金属氧化物及其制备方法

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Also Published As

Publication number Publication date
BR9200366A (pt) 1992-11-10
JPH05186221A (ja) 1993-07-27
US5215580A (en) 1993-06-01
MX9200587A (es) 1992-08-01
DE59201108D1 (de) 1995-02-16
NO920682L (no) 1992-08-24
NO306261B1 (no) 1999-10-11
DE4105345A1 (de) 1992-08-27
EP0499863A1 (de) 1992-08-26
FI101311B1 (fi) 1998-05-29
EP0499863B1 (de) 1995-01-04
CN1064285A (zh) 1992-09-09
FI101311B (fi) 1998-05-29
FI920731A0 (fi) 1992-02-20
CA2059688A1 (en) 1992-08-22
FI920731L (fi) 1992-08-22
JP3307667B2 (ja) 2002-07-24
NO920682D0 (no) 1992-02-20

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