ES2078465T3 - Procedimiento y dispositivo para medir la adsorcion y la desorcion de un gas adsorbido por una muestra solida asi como su utilizacion. - Google Patents

Procedimiento y dispositivo para medir la adsorcion y la desorcion de un gas adsorbido por una muestra solida asi como su utilizacion.

Info

Publication number
ES2078465T3
ES2078465T3 ES91401164T ES91401164T ES2078465T3 ES 2078465 T3 ES2078465 T3 ES 2078465T3 ES 91401164 T ES91401164 T ES 91401164T ES 91401164 T ES91401164 T ES 91401164T ES 2078465 T3 ES2078465 T3 ES 2078465T3
Authority
ES
Spain
Prior art keywords
measure
circuit
gas
desorption
pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES91401164T
Other languages
English (en)
Inventor
Hubert Ajot
Jean-Francois Joly
Dominique Albert Garnier
Felix Marny
Francis Raatz
Colette Russmann
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Application granted granted Critical
Publication of ES2078465T3 publication Critical patent/ES2078465T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/088—Investigating volume, surface area, size or distribution of pores; Porosimetry
    • G01N15/0893—Investigating volume, surface area, size or distribution of pores; Porosimetry by measuring weight or volume of sorbed fluid, e.g. B.E.T. method

Landscapes

  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Pathology (AREA)
  • General Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Dispersion Chemistry (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCESO Y A UN DISPOSITIVO PARA MEDIR LA ABSORCION Y EVENTUALMENTE LA DESORCION DE UN GAS ABSORBIDO POR UNA MUESTRA, ASI COMO SU UTILIZACION: TE LA FASE DE ABSORCION O UN AUMENTO DE PRESION DEL GAS, DURANTE LA FASE DE DESORCION, EN EL CIRCUITO DEPOSITO (I) DE 0,1 A 0,7 PA POR MINUTO GRACIAS A AL MENOS UNA VALVULA DE REGULACION VP SUB 1 DE ABERTURA PROPORCIONAL, DE MANERA A TRANSFERIR UN VOLUMEN SENSIBLEMENTE CONSTANTE DE GAS HACIA LA MUESTRA Y SE MIDE LA PRESION DEL GAS EN EL CIRCUITO DEPOSITO (2) Y EN EL CIRCUITO DE MEDIDA (1) POR CAPTORES DE PRESION (C SUB 2, C SUB 1) A INTERVALOS DE TIEMPO. SE DETERMINA FINALMENTE, POR MEDIOS DE TRATAMIENTO (14), EL ISOTERMO DE ABSORCION Y DE DESORCION, A PARTIR DEL VOLUMEN DEL CIRCUITO DEPOSITO, DE LA CANTIDAD DE GAS TRANSFERIDO, DE LA PRESION DEL GAS EN EL CIRCUITO DE MEDIDA Y DEL VOLUMEN DEL CIRCUITO DE MEDIDA. EN PARTICULAR, DE LA SUPERFICIE ESPECIFICA DE UN CATALIZADOR.
ES91401164T 1990-05-09 1991-05-02 Procedimiento y dispositivo para medir la adsorcion y la desorcion de un gas adsorbido por una muestra solida asi como su utilizacion. Expired - Lifetime ES2078465T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9005871A FR2661990B1 (fr) 1990-05-09 1990-05-09 Procede et dispositif pour mesurer l'adsorption et la desorption d'un gaz absorbe par un echantillon solide ainsi que son utilisation.

Publications (1)

Publication Number Publication Date
ES2078465T3 true ES2078465T3 (es) 1995-12-16

Family

ID=9396496

Family Applications (1)

Application Number Title Priority Date Filing Date
ES91401164T Expired - Lifetime ES2078465T3 (es) 1990-05-09 1991-05-02 Procedimiento y dispositivo para medir la adsorcion y la desorcion de un gas adsorbido por una muestra solida asi como su utilizacion.

Country Status (10)

Country Link
US (1) US5239482A (es)
EP (1) EP0456559B1 (es)
JP (1) JP3154066B2 (es)
KR (1) KR0171213B1 (es)
AU (1) AU648075B2 (es)
CA (1) CA2042156C (es)
DE (1) DE69111886T2 (es)
ES (1) ES2078465T3 (es)
FR (1) FR2661990B1 (es)
ZA (1) ZA913496B (es)

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JP3326278B2 (ja) * 1994-06-24 2002-09-17 三洋電機株式会社 気体吸蔵特性の測定装置
JP2779913B2 (ja) * 1995-01-30 1998-07-23 稔 竹内 細孔分布測定装置および定量注入器
JP2784476B2 (ja) * 1995-03-07 1998-08-06 稔 竹内 細孔分布測定装置
US5646335A (en) * 1995-08-24 1997-07-08 Coulter Corporation Wickless temperature controlling apparatus and method for use with pore volume and surface area analyzers
CA2207149C (fr) * 1997-05-22 2009-02-10 Hydro-Quebec Appareils pour la titration des gaz et le cyclage d'un materiau absorbant ou adsorbant
RU2149381C1 (ru) * 1999-06-29 2000-05-20 Институт катализа им. Г.К. Борескова Сибирского отделения РАН Способ одновременного определения адсорбционной и десорбционной ветвей изотерм адсорбции азота и устройство для его осуществления
US6387704B1 (en) * 2000-04-17 2002-05-14 Quantachrome Corporation Method for compensating for the time-dependent change in coolant level during gas sorption analysis
RU2196319C2 (ru) * 2000-09-25 2003-01-10 Закрытое акционерное общество "МЕТА" Способ измерения удельной поверхности дисперсных и пористых материалов
US6618687B2 (en) * 2001-10-16 2003-09-09 The United States Of America As Represented By The Secretary Of The Navy Temperature-based estimation of remaining absorptive capacity of a gas absorber
KR20020062233A (ko) * 2002-04-18 2002-07-25 한국문화기술연구원(주) 다공성 물질의 승온탈착과 반응 특성 측정을 위한 기상흡착장치 및 측정 방법
US7429358B1 (en) 2002-05-20 2008-09-30 Hy-Energy, Llc Method and apparatus for measuring gas sorption and desorption properties of materials
US6964191B1 (en) * 2002-10-15 2005-11-15 Murthy Tata Apparatus and technique for measuring permeability and permeant sorption
US7320224B2 (en) * 2004-01-21 2008-01-22 Brooks Automation, Inc. Method and apparatus for detecting and measuring state of fullness in cryopumps
US20060027014A1 (en) * 2004-08-03 2006-02-09 Quantachrome Corporation Apparatus and method for water sorption measurement
RU2447423C1 (ru) * 2010-12-22 2012-04-10 Государственное образовательное учреждение высшего профессионального образования "Уфимский государственный нефтяной технический университет" Способ определения реакционной поверхности углеродных материалов
US8881587B2 (en) * 2011-01-27 2014-11-11 Schlumberger Technology Corporation Gas sorption analysis of unconventional rock samples
CN102901803B (zh) * 2012-10-24 2014-10-08 河南理工大学 受载含瓦斯煤不同含水率吸附-解吸实验的方法
CN103115844B (zh) * 2013-01-28 2014-04-16 中国石油大学(华东) 一种煤页岩等温吸附/解吸曲线的测定方法
CN103471975B (zh) * 2013-09-18 2015-07-01 山东科技大学 复杂条件下瓦斯渗透实验装置
CN104502224B (zh) * 2014-08-14 2016-04-20 中国石油大学(华东) 饱和水条件下煤岩等温解吸曲线测定装置及方法
CN104655522A (zh) * 2015-02-02 2015-05-27 王思波 一种页岩气现场解吸附分析仪
US10156507B2 (en) * 2015-04-01 2018-12-18 Schlumberger Technology Corporation Determination of free volume of a rock sample using high pressure adsorption data
CN104863579B (zh) * 2015-05-27 2017-06-06 中国地质大学（北京） 一种损失气量测定方法及损失气量测定系统
CN104819910A (zh) * 2015-05-27 2015-08-05 辽宁工程技术大学 常压条件下测定大样量煤样吸附气体量的实验装置和方法
CN106168565A (zh) * 2015-07-17 2016-11-30 中国石油天然气股份有限公司 一种测量页岩基质含气量的装置及方法
ES2561707B1 (es) * 2015-12-21 2017-02-20 Universitat D'alacant / Universidad De Alicante Dispositivo para mantener constante la temperatura de un porta-muestras y uso del dispositivo en analizadores de sorción
US10222312B2 (en) * 2016-06-28 2019-03-05 Anton Paar Quantatec, Inc. Cryogenic temperature controller for volumetric sorption analyzers
US10514332B1 (en) * 2016-12-14 2019-12-24 Micromeritics Instrument Corporation Systems and methods for providing a profile of a material property using multiple analysis stations
CN107367440B (zh) * 2017-06-19 2023-08-01 金华职业技术学院 一种用于乙炔吸附测量的方法
CN109991043B (zh) * 2017-12-31 2022-07-05 中国人民解放军63653部队 基于高温管式气氛炉的差压式取气测量系统
CN108535134A (zh) * 2018-03-27 2018-09-14 西南石油大学 注氮气吞吐煤层压力监测及甲烷解吸效率评价装置与方法
CN108627415A (zh) * 2018-04-13 2018-10-09 河南理工大学 一种深部开采受载煤体瓦斯吸附-解吸实验系统及方法
CN108732062B (zh) * 2018-07-27 2024-12-27 上海海事大学 一种精确测量吸附剂开式吸附水蒸气的装置及方法
US11650139B2 (en) * 2018-08-08 2023-05-16 Panasonic Holdings Corporation Detection method for detection device, control system, detection system, and program
CN113340765B (zh) * 2021-06-25 2023-06-27 西藏大学 一种分子筛材料吸附性能检测装置及方法
CN115993430B (zh) * 2023-02-28 2026-02-06 健帆生物科技集团股份有限公司 一种检测吸附剂吸附性能的方法

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US4566326A (en) * 1984-07-09 1986-01-28 Quantachrome Corporation Automatic volumetric sorption analyzer
USRE33567E (en) * 1986-02-25 1991-04-09 Micromeritics Instrument Corporation Temperature controlling apparatus for use with pore volume and surface area analyzers
US4693124A (en) * 1986-02-25 1987-09-15 Micromeritics Instrument Co. Temperature controlling apparatus for use with pore volume and surface area analyzers
US4762010A (en) * 1987-04-02 1988-08-09 Mobil Oil Corporation Apparatus and method for adsorption and desorption studies, particularly for characterization of catalysts
US5058442A (en) * 1989-02-15 1991-10-22 Gas Research Institute Apparatus for measuring liquid vapor adsorption and desorption characteristics of a sample
JP2881242B2 (ja) * 1990-02-27 1999-04-12 富士シリシア化学株式会社 吸脱着量測定用装置及び吸脱着量測定方法

Also Published As

Publication number Publication date
AU648075B2 (en) 1994-04-14
FR2661990A1 (fr) 1991-11-15
EP0456559A1 (fr) 1991-11-13
ZA913496B (en) 1992-12-30
DE69111886D1 (de) 1995-09-14
KR910020435A (ko) 1991-12-20
KR0171213B1 (ko) 1999-05-15
JPH04230831A (ja) 1992-08-19
EP0456559B1 (fr) 1995-08-09
DE69111886T2 (de) 1995-12-07
CA2042156A1 (fr) 1991-11-10
FR2661990B1 (fr) 1992-07-24
CA2042156C (fr) 1999-11-09
US5239482A (en) 1993-08-24
JP3154066B2 (ja) 2001-04-09
AU7644491A (en) 1991-11-14

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