ES2083048T3 - Procedimiento para fabricar 2-nitro-5-fluoro- o bien -5-cloro-fenol. - Google Patents
Procedimiento para fabricar 2-nitro-5-fluoro- o bien -5-cloro-fenol.Info
- Publication number
- ES2083048T3 ES2083048T3 ES92117009T ES92117009T ES2083048T3 ES 2083048 T3 ES2083048 T3 ES 2083048T3 ES 92117009 T ES92117009 T ES 92117009T ES 92117009 T ES92117009 T ES 92117009T ES 2083048 T3 ES2083048 T3 ES 2083048T3
- Authority
- ES
- Spain
- Prior art keywords
- procedure
- nitro
- fluoride
- chlorine
- phenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- IXIJRPBFPLESEI-UHFFFAOYSA-N 1,2-difluoro-3-nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC(F)=C1F IXIJRPBFPLESEI-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910000000 metal hydroxide Inorganic materials 0.000 abstract 1
- 150000004692 metal hydroxides Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
LA INVENCION PRESENTADA CONCIERNE A UN PROCEDIMIENTO PARA LA OBTENCION DE 2 LIBRES DE ISOMEROS, EN EL CUAL SE TRANSFORMA 2,4 DIFLUORONITROBENCENO O 2,4 NES ACUOSAS DE HIDROXIDO DE METAL ALCALINO O DE METAL ALCALINO-TERREO, EN PRESENCIA DE DISOLVENTES ORGANICOS O DE OTRAS SUSTANCIAS MEDIADORAS DE LA SOLUBILIDAD, A TEMPERATURAS DE ENTRE 20 (GRADOS) C A CERCA DE 190 (GRADOS) C, LA MEZCLA DE LA REACCION SE SITUA POR MEDIO DE LA ADICION DE ACIDO, EN UN RH DE APROXIMADAMENTE 1 HASTA CERCA DE 6, EL PRODUCTO ORIGINADO ES DESTILADO POR VAPOR DE AGUA Y DESPUES DEL ENFRIADO ES AISLADO DEL DESTILADO.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4133447 | 1991-10-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2083048T3 true ES2083048T3 (es) | 1996-04-01 |
Family
ID=6442350
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES92117009T Expired - Lifetime ES2083048T3 (es) | 1991-10-09 | 1992-10-06 | Procedimiento para fabricar 2-nitro-5-fluoro- o bien -5-cloro-fenol. |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US5227535A (es) |
| EP (1) | EP0537592B1 (es) |
| JP (1) | JP3229386B2 (es) |
| CA (1) | CA2080208A1 (es) |
| DE (1) | DE59205092D1 (es) |
| ES (1) | ES2083048T3 (es) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4030263A1 (de) * | 1990-09-25 | 1992-03-26 | Hoechst Ag | Verfahren zur herstellung von 2,3-difluor-6-nitrophenol |
| IN180375B (es) * | 1992-12-17 | 1998-01-24 | Hoechst Ag | |
| CN106045861B (zh) * | 2016-05-26 | 2019-04-19 | 山东润博生物科技有限公司 | 一种连续化生产5-氟-2-硝基苯酚的方法及其系统 |
| CN106083536B (zh) * | 2016-06-14 | 2018-10-30 | 浙江永太科技股份有限公司 | 一种安塞曲匹关键中间体的制备方法 |
| CN107935858B (zh) * | 2016-10-12 | 2020-09-08 | 利尔化学股份有限公司 | 5-氟-2-硝基苯酚的制备方法 |
| CN107459464A (zh) * | 2017-08-23 | 2017-12-12 | 连云港世杰农化有限公司 | 一种合成2‑(5‑氟‑2‑硝基‑苯氧基)乙酸甲酯的方法 |
| CN114031503A (zh) * | 2021-12-15 | 2022-02-11 | 启东东岳药业有限公司 | 同时合成5-氟-2-硝基苯酚和3-氟-4-硝基苯酚的方法 |
| CN116514662B (zh) * | 2022-12-12 | 2025-03-04 | 山东京博农化科技股份有限公司 | 一种5-氟-2-硝基苯酚的制备方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3461173A (en) * | 1963-11-12 | 1969-08-12 | Sun Oil Co | Preparation of substituted o-nitrophenols |
| FR2224440B1 (es) * | 1973-04-06 | 1976-06-11 | Rhone Progil | |
| DE2733682A1 (de) * | 1977-07-26 | 1979-02-08 | Bayer Ag | Verfahren zur herstellung von trifluormethylphenolen |
| DE2935629A1 (de) * | 1979-09-04 | 1981-03-12 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung von 5-chlor-2-nitrophenol. |
| US4596893A (en) * | 1984-01-31 | 1986-06-24 | Budapesti Vegyimuvek | 2-trifluoromethyl-4,6-dinitro-phenol and derivatives thereof, process for the preparation thereof and herbicidal, acaricidal and crop regulation compositions containing same |
| DE4030263A1 (de) * | 1990-09-25 | 1992-03-26 | Hoechst Ag | Verfahren zur herstellung von 2,3-difluor-6-nitrophenol |
-
1992
- 1992-10-06 ES ES92117009T patent/ES2083048T3/es not_active Expired - Lifetime
- 1992-10-06 EP EP92117009A patent/EP0537592B1/de not_active Expired - Lifetime
- 1992-10-06 DE DE59205092T patent/DE59205092D1/de not_active Expired - Fee Related
- 1992-10-07 JP JP26889992A patent/JP3229386B2/ja not_active Expired - Fee Related
- 1992-10-07 US US07/957,674 patent/US5227535A/en not_active Expired - Fee Related
- 1992-10-08 CA CA002080208A patent/CA2080208A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| DE59205092D1 (de) | 1996-02-29 |
| EP0537592B1 (de) | 1996-01-17 |
| JP3229386B2 (ja) | 2001-11-19 |
| CA2080208A1 (en) | 1993-04-10 |
| JPH05294900A (ja) | 1993-11-09 |
| EP0537592A1 (de) | 1993-04-21 |
| US5227535A (en) | 1993-07-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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