ES2088605T3 - Procedimiento de varias etapas para la obtencion continua de poliisocianatos organicos. - Google Patents
Procedimiento de varias etapas para la obtencion continua de poliisocianatos organicos.Info
- Publication number
- ES2088605T3 ES2088605T3 ES93105635T ES93105635T ES2088605T3 ES 2088605 T3 ES2088605 T3 ES 2088605T3 ES 93105635 T ES93105635 T ES 93105635T ES 93105635 T ES93105635 T ES 93105635T ES 2088605 T3 ES2088605 T3 ES 2088605T3
- Authority
- ES
- Spain
- Prior art keywords
- organic polyisocyanates
- procedure
- several stages
- continuous obtaining
- continuous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 2
- 229920001228 polyisocyanate Polymers 0.000 title abstract 2
- 239000005056 polyisocyanate Substances 0.000 title abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 abstract 1
- 238000003776 cleavage reaction Methods 0.000 abstract 1
- 125000005442 diisocyanate group Chemical group 0.000 abstract 1
- 229920000768 polyamine Polymers 0.000 abstract 1
- 239000004814 polyurethane Substances 0.000 abstract 1
- 229920002635 polyurethane Polymers 0.000 abstract 1
- 230000007017 scission Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/82—Post-polymerisation treatment
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/04—Preparation of derivatives of isocyanic acid from or via carbamates or carbamoyl halides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
EL OBJETO DE LA INVENCION ES UN PROCEDIMIENTO EN VARIAS ETAPAS PARA LA PRODUCCION ININTERRUMPIDA DE POLIISOCIANATOS ORGANICOS COMO DIISOCIANATOS ALIFATICOS O CICLOALIFATICOS A TRAVES DE LA TRANSFORMACION LA POLIAMINA ORGANICA CORRESPONDIENTE EN POLIURETANO MONOMERO, AL TRATAR DICHA POLIAMINA CON DERIVADOS DE ACIDO CARBONICO Y ALCOHOLES; EN MONOMEROS DE POLIURETANO Y LA DESGREGACION SE SEPARAN EL POLIISOCIANATO PRODUCIDO EN ETAPAS DE REACCION DETERMINADAS Y EL RESIDUO NO APROVECHABLE Y SE CONDUCE EL PRODUCTO SECUNDARIO APROVECHABLE RESULTANTE DE LA DISGREGACION TERMICA A LA ETAPA PREVIA DE PRODUCCION DE POLIISOCIANATO.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4213099A DE4213099A1 (de) | 1992-04-21 | 1992-04-21 | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von organischen Polyisocyanaten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2088605T3 true ES2088605T3 (es) | 1996-08-16 |
Family
ID=6457162
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES93105635T Expired - Lifetime ES2088605T3 (es) | 1992-04-21 | 1993-04-06 | Procedimiento de varias etapas para la obtencion continua de poliisocianatos organicos. |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US5386053A (es) |
| EP (1) | EP0566925B1 (es) |
| JP (1) | JP3382289B2 (es) |
| KR (1) | KR100251900B1 (es) |
| AT (1) | ATE139994T1 (es) |
| CA (1) | CA2094484C (es) |
| DE (2) | DE4213099A1 (es) |
| DK (1) | DK0566925T3 (es) |
| ES (1) | ES2088605T3 (es) |
Families Citing this family (50)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4342426A1 (de) * | 1993-12-13 | 1995-06-14 | Bayer Ag | Verfahren zur Herstellung von Diurethanen und ihre Verwendung zur Herstellung von Diisocyanaten |
| DE4439421A1 (de) * | 1994-11-04 | 1996-05-09 | Huels Chemische Werke Ag | Neue harnstoffgruppenhaltige Polyamine und Verfahren zu ihrer Herstellung |
| DE19523386A1 (de) * | 1995-06-23 | 1997-01-09 | Bayer Ag | Verfahren zur Entfernung von Nebenprodukten aus Diurethanen |
| DE59705128D1 (de) * | 1996-03-15 | 2001-12-06 | Bayer Ag | Verfahren zur thermischen Spaltung von Carbamidsäureestern |
| DE19813107A1 (de) | 1998-03-25 | 1999-09-30 | Basf Ag | Verfahren zur Herstellung von Polyurethanschaumstoffen |
| DE19907648A1 (de) * | 1999-02-23 | 2000-08-24 | Basf Ag | Verfahren zur Herstellung von Isocyanaten durch Spaltung von Urethanen |
| DE10260092A1 (de) | 2002-12-19 | 2004-07-01 | Basf Ag | Verfahren zur Reinigung von Isocyanaten |
| DE10338509A1 (de) * | 2003-08-22 | 2005-03-17 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE10338508A1 (de) * | 2003-08-22 | 2005-03-17 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE10338511A1 (de) * | 2003-08-22 | 2005-03-17 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102004022626A1 (de) * | 2004-05-07 | 2005-12-15 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102004026451A1 (de) * | 2004-05-29 | 2005-12-15 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102004036499A1 (de) * | 2004-07-28 | 2006-03-23 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102005043799A1 (de) * | 2005-09-13 | 2007-04-12 | Basf Ag | Verfahren zur Herstellung von Isocyanaten |
| CN101374802B (zh) | 2006-01-13 | 2013-07-17 | 巴斯夫欧洲公司 | 制备异氰酸酯的方法 |
| EP2049675A1 (de) | 2006-08-01 | 2009-04-22 | Basf Se | Verfahren zur herstellung von pentamethylen-1,5-diisocyanat |
| EP2069292A1 (de) * | 2006-08-31 | 2009-06-17 | Basf Se | Verfahren zur herstellung von isocyanaten |
| TWI361179B (en) * | 2006-11-17 | 2012-04-01 | Asahi Kasei Chemicals Corp | A process for producing isocyanates |
| WO2008074645A1 (de) * | 2006-12-20 | 2008-06-26 | Basf Se | Verfahren zur herstellung von 2-methylpentan-1,5-diisocyanat aus methylglutarsäuredinitril |
| TW200844080A (en) | 2007-01-11 | 2008-11-16 | Asahi Kasei Chemicals Corp | Process for producing isocyanate |
| CN101652344B (zh) | 2007-03-30 | 2014-06-04 | 旭化成化学株式会社 | 使用含有氨基甲酸酯和芳香族羟基化合物的组合物制造异氰酸酯的方法、以及氨基甲酸酯输送用和储藏用组合物 |
| JP5313164B2 (ja) | 2007-11-19 | 2013-10-09 | 旭化成ケミカルズ株式会社 | イソシアネートおよび芳香族ヒドロキシ化合物の製造方法 |
| KR20130127550A (ko) * | 2008-05-15 | 2013-11-22 | 아사히 가세이 케미칼즈 가부시키가이샤 | 이소시아네이트의 제조 방법 |
| US8895774B2 (en) * | 2008-05-15 | 2014-11-25 | Asahi Kasei Chemicals Corporation | Process for producing isocyanates using diaryl carbonate |
| DE102008002002A1 (de) | 2008-05-27 | 2009-12-03 | Evonik Degussa Gmbh | Chlor armes mehrstufiges Verfahren zur Herstellung von cycloaliphatischen Diisocyanaten |
| WO2011015541A1 (de) | 2009-08-04 | 2011-02-10 | Basf Se | Verfahren zur herstellung von isocyanaten |
| KR101332485B1 (ko) | 2009-08-21 | 2013-11-26 | 아사히 가세이 케미칼즈 가부시키가이샤 | N-치환 카르밤산 에스테르의 제조 방법 및 상기 n-치환 카르밤산 에스테르를 사용하는 이소시아네이트의 제조 방법 |
| US8859805B2 (en) | 2009-09-22 | 2014-10-14 | Basf Se | Process for preparing isocyanates |
| EP2503878B1 (de) | 2009-11-27 | 2015-01-28 | Basf Se | Dendritischer polyharnstoff zur solubilisierung schwerlöslicher wirkstoffe |
| US8835673B2 (en) | 2009-12-04 | 2014-09-16 | Basf Se | Process for preparing isocyanates |
| DE102009054749A1 (de) | 2009-12-16 | 2011-06-22 | Evonik Degussa GmbH, 45128 | Zusammensetzung aus (cyclo)aliphatischen Diisocyanaten und aromatischen Säurehalogeniden |
| US9000219B2 (en) | 2009-12-24 | 2015-04-07 | Mitsui Chemicals, Inc. | Method for treatment of isocyanate residue, and method for treatment of carbonate |
| JP5563816B2 (ja) * | 2009-12-24 | 2014-07-30 | 三井化学株式会社 | イソシアネート残渣の処理方法 |
| JP5563886B2 (ja) * | 2010-05-11 | 2014-07-30 | 三井化学株式会社 | イソシアネート残渣の処理方法 |
| JP5643517B2 (ja) * | 2010-02-04 | 2014-12-17 | 三井化学株式会社 | 触媒処理方法 |
| EP2679575B1 (en) | 2011-02-21 | 2019-04-10 | Asahi Kasei Kabushiki Kaisha | Process for producing carbonyl compounds |
| EP2714649A2 (de) | 2011-05-30 | 2014-04-09 | Basf Se | Verfahren zur herstellung von polyisocyanaten |
| US8871969B2 (en) | 2011-05-30 | 2014-10-28 | Basf Se | Process for the production of polyisocyanates |
| JP2014521797A (ja) | 2011-08-05 | 2014-08-28 | ビーエイエスエフ・ソシエタス・エウロパエア | 超分岐ポリマーに基づく会合性増粘剤 |
| US8772527B2 (en) | 2012-04-27 | 2014-07-08 | Basf Se | Process for isomerization of cis-2-pentenenitrile to 3-pentenenitriles |
| DE102012219324A1 (de) | 2012-10-23 | 2014-04-24 | Evonik Industries Ag | Zusammensetzungen umfassend alkoxysilanhaltige Isocyanateund saure Stabilisatoren |
| WO2014082910A1 (de) * | 2012-11-28 | 2014-06-05 | Basf Se | Verfahren zur herstellung von polyisocyanaten |
| KR101745229B1 (ko) | 2013-04-03 | 2017-06-08 | 미쓰이 가가쿠 가부시키가이샤 | 자일릴렌 다이아이소사이아네이트의 제조 방법 및 자일릴렌 다이아이소사이아네이트의 제조 장치 |
| EP3459931A1 (en) | 2017-09-26 | 2019-03-27 | Covestro Deutschland AG | Multistep process for the preparation of diisocyanates |
| EP3459930A1 (en) | 2017-09-26 | 2019-03-27 | Covestro Deutschland AG | Multistep process for the preparation of hexamethylene diisocyanate, pentamethylene diisocyanate or toluene diisocyanate |
| CN110872481B (zh) * | 2018-08-30 | 2022-02-18 | 万华化学集团股份有限公司 | 一种无醛胶合板用胶黏剂及其制备方法,胶合板及其制备方法 |
| US20240425448A1 (en) | 2021-11-08 | 2024-12-26 | Asahi Kasei Kabushiki Kaisha | Method for producing isocyanate compound, method for producing carbamate compound, method for recovering amine compound, and isocyanate composition |
| CN114249671B (zh) * | 2021-11-19 | 2023-03-10 | 美瑞新材料股份有限公司 | 一种以脂肪族二胺混合物为原料制备脂肪族二异氰酸酯的方法 |
| CN115350660B (zh) * | 2022-07-05 | 2024-11-12 | 中国科学院过程工程研究所 | 一种非光气法制备1,5-戊二异氰酸酯的装置和方法 |
| CN115611776A (zh) * | 2022-09-29 | 2023-01-17 | 四川元理材料科技有限公司 | Ipdi粗品纯化的工业化方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3047898A1 (de) * | 1980-12-19 | 1982-07-15 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen thermischen spaltung von carbamidsaeureestern und die verwendung von hierbei anfallenden isocyanate und carbamidsaeureester aufweisenden gemischen zur herstellung von isocyanaten |
| DE3215591A1 (de) * | 1982-04-27 | 1983-10-27 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen thermischen spaltung von carbamidsaeureestern |
| DE3314788A1 (de) * | 1983-04-23 | 1984-10-25 | Basf Ag, 6700 Ludwigshafen | Mehrstufenverfahren zur herstellung von hexamethylendiisocyanat-1,6 und/oder isomeren aliphatischen diisocyanaten mit 6 kohlenstoffatomen im alkylenrest |
| DE3314790A1 (de) * | 1983-04-23 | 1984-10-25 | Basf Ag, 6700 Ludwigshafen | Mehrstufenverfahren zur herstellung von 3-isocyanatomethyl-3,5,5-trimethyl-cyclohexylisocyanat |
| DE3339300A1 (de) * | 1983-10-29 | 1985-05-09 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von isocyanaten durch thermische spaltung von urethanen |
| DE3828033A1 (de) * | 1988-08-18 | 1990-03-08 | Huels Chemische Werke Ag | Kreislaufverfahren zur herstellung von (cyclo)aliphatischen diisocyanaten |
| IT1244476B (it) * | 1990-12-21 | 1994-07-15 | Enichem Sintesi | Procedimento continuo per la preparazione di isociamati |
-
1992
- 1992-04-21 DE DE4213099A patent/DE4213099A1/de not_active Withdrawn
-
1993
- 1993-03-08 US US08/028,009 patent/US5386053A/en not_active Expired - Lifetime
- 1993-03-26 JP JP06800093A patent/JP3382289B2/ja not_active Expired - Lifetime
- 1993-04-06 DE DE59303105T patent/DE59303105D1/de not_active Expired - Lifetime
- 1993-04-06 DK DK93105635.2T patent/DK0566925T3/da active
- 1993-04-06 EP EP93105635A patent/EP0566925B1/de not_active Expired - Lifetime
- 1993-04-06 AT AT93105635T patent/ATE139994T1/de active
- 1993-04-06 ES ES93105635T patent/ES2088605T3/es not_active Expired - Lifetime
- 1993-04-20 CA CA002094484A patent/CA2094484C/en not_active Expired - Fee Related
- 1993-04-21 KR KR1019930007023A patent/KR100251900B1/ko not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0566925A2 (de) | 1993-10-27 |
| JP3382289B2 (ja) | 2003-03-04 |
| CA2094484C (en) | 1997-10-07 |
| EP0566925A3 (en) | 1993-12-08 |
| DE59303105D1 (de) | 1996-08-08 |
| CA2094484A1 (en) | 1993-10-22 |
| KR100251900B1 (ko) | 2000-04-15 |
| KR930021675A (ko) | 1993-11-22 |
| US5386053A (en) | 1995-01-31 |
| JPH0625136A (ja) | 1994-02-01 |
| EP0566925B1 (de) | 1996-07-03 |
| DE4213099A1 (de) | 1993-10-28 |
| DK0566925T3 (da) | 1996-07-29 |
| ATE139994T1 (de) | 1996-07-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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