ES2089733T3 - Proceso para preparar esteres y amidas de acidos grasos de sales de acido sulfonico. - Google Patents
Proceso para preparar esteres y amidas de acidos grasos de sales de acido sulfonico.Info
- Publication number
- ES2089733T3 ES2089733T3 ES93307155T ES93307155T ES2089733T3 ES 2089733 T3 ES2089733 T3 ES 2089733T3 ES 93307155 T ES93307155 T ES 93307155T ES 93307155 T ES93307155 T ES 93307155T ES 2089733 T3 ES2089733 T3 ES 2089733T3
- Authority
- ES
- Spain
- Prior art keywords
- amides
- fatty acids
- fatty acid
- acid salts
- sulphonic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 235000014113 dietary fatty acids Nutrition 0.000 title abstract 6
- 229930195729 fatty acid Natural products 0.000 title abstract 6
- 239000000194 fatty acid Substances 0.000 title abstract 6
- 150000004665 fatty acids Chemical class 0.000 title abstract 4
- 150000001408 amides Chemical class 0.000 title abstract 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical class OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 title 1
- -1 Fatty acid esters Chemical class 0.000 abstract 2
- 230000015556 catabolic process Effects 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 238000000354 decomposition reaction Methods 0.000 abstract 1
- 238000006731 degradation reaction Methods 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/32—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of salts of sulfonic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Steroid Compounds (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
LOS ESTERES DE ACIDO GRASO DE HIDROXIALQUILSULFONATOS Y AMIDAS DE ACIDO GRASO DE AMINOALQUILSULFONATOS SE PREPARAN AL CALENTAR UN EXCESO DE ACIDOS GRASOS CON EL SULFONATO ANTES DE QUE SE DISIPE LA CONDENSACION DE AGUA. EL EXCESO DE ACIDOS GRASOS SE ELIMINA EN LA DESTILACION Y EL PRODUCTO DE ESTER DE ACIDO GRASO AISLADO O AMIDA SE ENFRIA RAPIDA Y DIRECTAMENTE PARA MINIMIZAR LA DESCOMPOSICION Y DEGRADACION DEL COLOR.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/946,269 US5300665A (en) | 1992-09-16 | 1992-09-16 | Process for preparing fatty acid esters and amides of sulfonic acid salts |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2089733T3 true ES2089733T3 (es) | 1996-10-01 |
Family
ID=25484234
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES93307155T Expired - Lifetime ES2089733T3 (es) | 1992-09-16 | 1993-09-10 | Proceso para preparar esteres y amidas de acidos grasos de sales de acido sulfonico. |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US5300665A (es) |
| EP (1) | EP0594297B1 (es) |
| JP (1) | JPH06192211A (es) |
| AT (1) | ATE137742T1 (es) |
| AU (1) | AU659567B2 (es) |
| BR (1) | BR9303776A (es) |
| CA (1) | CA2105418A1 (es) |
| DE (1) | DE69302557T2 (es) |
| ES (1) | ES2089733T3 (es) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5384421A (en) * | 1992-08-21 | 1995-01-24 | Hoechst Celanese Corporation | Process for making sodium acylisethionates |
| US5434276A (en) * | 1993-12-27 | 1995-07-18 | Finetex, Inc. | Process for making N-acyl taurides |
| US5496959A (en) * | 1994-05-23 | 1996-03-05 | Hoechst Celanese Corporation | Preparation of N-acyl taurates |
| US5837668A (en) * | 1996-04-30 | 1998-11-17 | Rhodia Inc. | Acyloxyalkane sulfonate and amphoteric surfactant blend compositions and methods for preparing same |
| US6069262A (en) * | 1997-10-06 | 2000-05-30 | Finetex, Inc. | Fatty acid esters of hydroxyalkyl sulfonate salts and process for producing same |
| US6562874B1 (en) * | 1999-12-07 | 2003-05-13 | Unilever Home & Personal Care Usa Division Of Conopco, Inc. | Compositions comprising combination of DEFI and modified DEFI and methods of making |
| US6362145B1 (en) | 2000-11-14 | 2002-03-26 | Clariant International Ltd. | Clear soap bar comprising metal catalyst sodium cocoyl isethionate |
| US20050020680A1 (en) * | 2001-09-14 | 2005-01-27 | Falck John R | Hydroxyfattysulfonic acid analogs |
| MXPA04002390A (es) * | 2001-09-14 | 2004-11-22 | Taisho Pharma Co Ltd | Analogos del acido hidroxigrasosulfonico. |
| US20060089279A1 (en) * | 2004-10-26 | 2006-04-27 | Brennan Michael A | Mild acyl isethionate toilet bar composition |
| US7737096B2 (en) * | 2004-10-26 | 2010-06-15 | Unilever Home & Personal Care Usa Division Of Conopco, Inc. | Mild acyl isethionate toilet bar composition |
| WO2008075366A2 (en) * | 2006-12-20 | 2008-06-26 | Medwell Laboratories Ltd. | Novel conjugates of polyunsaturated fatty acids with amines and therapeutic uses thereof |
| CN102584642B (zh) * | 2011-01-13 | 2013-04-03 | 吉林伊捷思化学有限公司 | 羟乙基磺酸钠脂肪酸酯的制备方法 |
| US10376456B2 (en) | 2015-03-16 | 2019-08-13 | Galaxy Surfactant | Concentrated and self-preserving compositions of mild surfactants for transparent and skin-pH personal care formulations |
| CN113896661B (zh) * | 2020-06-22 | 2023-09-19 | 万华化学集团股份有限公司 | 一种椰油基羟乙基磺酸钠的制备方法 |
| CN116103053B (zh) * | 2022-08-11 | 2025-07-11 | 广州天赐高新材料股份有限公司 | 一种表面活性剂组合物及其制备方法 |
| CN115626884B (zh) * | 2022-12-20 | 2023-04-07 | 江苏奥洁生物科技有限公司 | 一种合成n-酰基氨基酸表面活性剂的方法 |
Family Cites Families (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2316719A (en) * | 1943-04-13 | Purification of organic substances | ||
| USRE23823E (en) * | 1954-05-04 | Detergent and method of making | ||
| US2303582A (en) * | 1938-10-08 | 1942-12-01 | Colgate Palmolive Peet Co | Treatment of organic sulphates |
| US2307953A (en) * | 1940-07-05 | 1943-01-12 | Colgate Palmolive Peet Co | Purification of organic compounds |
| US2820818A (en) * | 1954-04-12 | 1958-01-21 | Dow Chemical Co | Preparation of salts of hydroxy aliphatic sulfonic acids |
| US2857370A (en) * | 1954-11-22 | 1958-10-21 | Gen Aniline & Film Corp | Process of preparing ester and amide type anionic surface active agents |
| NL95122C (es) * | 1954-11-22 | |||
| US2810747A (en) * | 1955-08-22 | 1957-10-22 | Dow Chemical Co | Continuous production of salts of hydroxy aliphatic sulfonic acids |
| BE559684A (es) * | 1956-08-10 | |||
| US2898352A (en) * | 1957-07-29 | 1959-08-04 | Gen Aniline & Film Corp | Ester type surface active agents |
| US2974154A (en) * | 1958-12-30 | 1961-03-07 | Gen Aniline & Film Corp | Process of preparing salt-free n-acyl taurines |
| US2974153A (en) * | 1958-12-30 | 1961-03-07 | Gen Aniline & Film Corp | Process of preparing salt-free n-acyl taurines |
| US3151136A (en) * | 1959-07-29 | 1964-09-29 | Koczorowski Eduard | Process of preparing fatty acid esters of hydroxyalkane sulfonic acids |
| US3150156A (en) * | 1959-08-04 | 1964-09-22 | Lever Brothers Ltd | Catalytic process for preparing nu-acyl taurates |
| US3004049A (en) * | 1959-12-01 | 1961-10-10 | Gen Aniline & Film Corp | Production of ester type anionic surface active agents |
| US3232968A (en) * | 1959-12-01 | 1966-02-01 | Gen Aniline & Film Corp | Process for preparing n-acyl taurates using hypophosphorous acid as catalyst |
| US3234247A (en) * | 1962-05-17 | 1966-02-08 | Armour & Co | Preparation of n-acyl taurates |
| US3320292A (en) * | 1963-09-05 | 1967-05-16 | Lever Brothers Ltd | Preparation of sulfonated fatty acid ester surface-active agents |
| US3383396A (en) * | 1963-10-30 | 1968-05-14 | Lever Brothers Ltd | Preparation of surface-active agents using a dissolved zirconium catalyst |
| US3394155A (en) * | 1964-05-22 | 1968-07-23 | Lever Brothers Ltd | Preparation of surface-active agents |
| US3420858A (en) * | 1964-12-11 | 1969-01-07 | Lever Brothers Ltd | Process for the production of fatty acid esters of hydroxy sulfonates |
| US3420857A (en) * | 1964-12-11 | 1969-01-07 | Lever Brothers Ltd | Process for the continuous production of fatty acid esters of hydroxy sulfonates |
| US3429136A (en) * | 1964-12-11 | 1969-02-25 | Lever Brothers Ltd | Process for preparing hydroxy sulfonate esters |
| US3745181A (en) * | 1971-06-28 | 1973-07-10 | Us Agriculture | Process for the preparation of surfactants |
| US3880897A (en) * | 1973-09-13 | 1975-04-29 | Gillette Co | Method of making acyl esters of hydroxy alkane sulfonates |
| US4476055A (en) * | 1982-07-06 | 1984-10-09 | Westvaco Corporation | C21-Dicarboxylic acid isethionates as primary anionic surfactants |
| US4515721A (en) * | 1982-09-27 | 1985-05-07 | Jordan Chemical Company | Process for the production of fatty acid esters of hydroxyalkyl sulfonate salts |
| US4537724A (en) * | 1983-05-11 | 1985-08-27 | Ethyl Corporation | Alkanoyloxybenzenesulfonate salt production |
| US4536338A (en) * | 1983-11-09 | 1985-08-20 | Lever Brothers Company | Process for manufacture of fatty acid esters of hydroxy sulfonates |
| US5121611A (en) * | 1990-10-25 | 1992-06-16 | Liquid Carbonic Corporation | Refrigeration apparatus and method of refrigeration |
-
1992
- 1992-09-16 US US07/946,269 patent/US5300665A/en not_active Expired - Fee Related
-
1993
- 1993-08-31 JP JP5215314A patent/JPH06192211A/ja active Pending
- 1993-09-02 CA CA002105418A patent/CA2105418A1/en not_active Abandoned
- 1993-09-10 EP EP93307155A patent/EP0594297B1/en not_active Expired - Lifetime
- 1993-09-10 DE DE69302557T patent/DE69302557T2/de not_active Expired - Fee Related
- 1993-09-10 ES ES93307155T patent/ES2089733T3/es not_active Expired - Lifetime
- 1993-09-10 AT AT93307155T patent/ATE137742T1/de not_active IP Right Cessation
- 1993-09-13 BR BR9303776A patent/BR9303776A/pt not_active Application Discontinuation
- 1993-09-16 AU AU47405/93A patent/AU659567B2/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| JPH06192211A (ja) | 1994-07-12 |
| EP0594297B1 (en) | 1996-05-08 |
| EP0594297A1 (en) | 1994-04-27 |
| CA2105418A1 (en) | 1994-03-18 |
| ATE137742T1 (de) | 1996-05-15 |
| BR9303776A (pt) | 1994-07-26 |
| DE69302557D1 (de) | 1996-06-13 |
| DE69302557T2 (de) | 1996-09-19 |
| AU4740593A (en) | 1994-03-24 |
| AU659567B2 (en) | 1995-05-18 |
| US5300665A (en) | 1994-04-05 |
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Legal Events
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|---|---|---|---|
| FG2A | Definitive protection |
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